3150 Dodd Rd - Old Oasis Market - Tank Removal Soil Sampling gco� P��r��3z�-�� `
� �� � C�NL.�L(CK-w�� �VK.�lTN��r�I
Main OffiCe-ll303 Excelsior Blvd.-Hopkins,MN 55343
Phone:(952)933-4800-Fax:(952)939-0418
www.pump-meter.com
— � Email:pump-meter@pump-meter.com
�� o� i
Pum and Meter Service, Inc. SERVICE . saLEs • INSTALLATION
Bejin Pump ServiCe-A division of Pump&Meter Service,Inc. Duluth BranCh
3497 129th Street-Chippewa Falls,WI 54729 Phone:(218)389-6359-Fax:(218)389-6359
Phone:(715)723-8223-Fax:(715)723-7242
September 9, 2015
HI & A PROPERTIES LLC
ATTN: YOUSEF ABUMAYALEH
520 BLAKE ROAD NORTH
HOPKINS, MN 55343
RE: Tank Removal Soil Sampling
OLD OASIS MARKET
315 0 DODD RO.A.D
EAGAN,MN 55121
To Whom It May Concern:
Enclosed Is a copy of the chemistry report on the soil samples
taken during the removal of the (4) 10, 000 gallon underground
storage tanks at the above location. Results of the data indicate
non-detect.
Thank you.
Sincerely,
PUMP & METER SERVICE, INC.
RON SMITH
Enc.
Fueling Systems - Electronic Gauging& y��'� Self-Serv Equipment - Compressors
Inventory Controls - Fiberg/ass Tanks&Pipe r Auto Lifts&Parts - Service Station Pumps
gEUM EQpIPMENT INS�
Line Testing - Tank Testing Card Contro/Systems - Canopies
f y
Pace Analytical Services,inc.
aceAnalytical� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
www.pacelabs.com (612)607-1700
September 08, 2015
Mr. Ron Smith
Pump & Meter
11303 Excelsior Blvd.
Hopkins, MN 55343
RE: Project: OASIS EAGAN
Pace Project No.: 10320026
Dear Mc Smith: i
Enclosed are the analytical results for sample(s) received by the laboratory on August 27, 2015. The '
results relate only to the samples included in this report. Results reported herein conform to the I,
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless I
otherwise noted in the body of the report. �
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
-���
Timothy Sandager
timothy.sandager@pacelabs.com
Project Manager
Enclosures
Q ptCRF�.
_� � REPORT OF LABORATORY ANALYSIS
� ��°
This report shall not be reproduced,except in full,
� without the written consent of Pace Analytical Services,Inc.. Page 1 Of 11
980 �1 Q`"
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Pace Analytical Services,lnc.
aceAnaly�ical� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
www.��raa�.� �s�z�so�-noo
CERTIFICATIONS
Project: OASIS EAGAN
Pace Project No.: 10320026
Minnesota Certification IDs
1700 Elm Street SE Suite 200,Minneapolis,MN 55414 Minnesota Certification#:027-053-137
A2LA Certification#:2926.01 Mississippi Certification#:Pace
Alaska Certification#:UST-078 Montana Certification#:MT0092
Alaska Certification#MN00064 Nevada Certification#:MN 00064
Alabama Certification#40770 Nebraska Certification#:Pace
Arizona Certification#:AZ-0014 New Jersey Certification#:MN-002
Arkansas Certification#:88-0680 New York Certification#:11647
California Certification#:01155CA North Carolina Certification#:530
Colorado Certification#Pace North Carolina State Public Health#:27700
Connecticut Certification#:PH-0256 North Dakota Certification#:R-036
EPA Region 8 Certification#:8TMS-L Ohio EPA#:4150
Florida/NELAP Certification#:E87605 Ohio VAP Certification#:CL101
Guam Certification#:14-008r Oklahoma Certification#:9507
Georgia Certification#:959 Oregon Certification#:MN200001
Georgia EPD#:Pace Oregon Certification#:MN300001
Idaho Certification#:MN00064 Pennsylvania Certification#:68-00563
Hawaii Certification#MN00064 Puerto Rico Certification
Illinois CertificaGon#:200011 Saipan(CNMI)#:MP0003
Indiana Certification#C-MN-01 South Carolina#:74003001
lowa Certification#:368 Texas Certification#:T104704192
Kansas Certification#:E-10167 Tennessee Certification#:02818
Kentucky Dept of Envi.Protection-DW#90062 Utah Certification#:MN000642013-4
Kentucky Dept of Envi.Protection-WW#:90062 �rginia DGS Certification#:251
Louisiana DEQ Certification#:3086 �rginia/VELAP Certification#:Pace I
Louisiana DHH#:LA140001 Washington Certification#:C486
Maine Certification#:2013011 West Virginia Certification#:382
Maryland Certification#:322 West Virginia DHHR#:9952C
Michigan DEPH Certification#:9909 Wisconsin Certification#:999407970
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analyticai Services,Inc.. Page 2 of 11
7 . . .. . . .. . .. . . . . . . . . . . .
Pace Analyticai Services,Inc.
1700 Eim Street-Suite 200
aceAnalytical Minneapolis,MN 55414
www.pace►aas.eom (s12)so7-1700
SAMPLE SUMMARY
Project: OASIS EAGAN
Pace Project No.: 10320026
Lab ID Sample ID Matrix Date Collected Date Received
10320026001 DISPENSER#6 Solid 08/27/15 12:00 08/27/15 12:58
REPORT OF LABORATORY ANALYSIS
This report shali not be reproduced,except in full,
without the written consent of Pace Analyticai Services,Inc.. Page 3 of 11
. . ..r . . . . . �
r
Pace Analytical Services,lnc.
aceAnalytica!� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
�Pa�a�� (612)607-1700
SAMPLE ANALYTE COUNT
Project: OASIS EAGAN
Pace Project No.: 10320026
Analytes
Lab ID Sample ID Method Analysts Reported
10320026001 DISPENSER#6 WI MOD DRO MT 2
ASTM D2974 JDL 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in fuil,
without the written consent of Pace Analytical Services,Inc.. Page 4 of 11
. .T .. . . . . . . . . .... .. . .
1
Pace Analytical Services,Inc.
aceAnalytical� 170M nt eapol s,MN 55414
www.pacela6s.com (612)607-1700
ANALYTICAL RESULTS
Project: OASIS EAGAN
Pace Project No.: 10320026
Sample: DISPENSER#6 Lab ID: 10320026001 Collected: 08/27/15 12:00 Received: O8/27/15 12:58 Matrix:Solid
Resu/ts reporfed on a"dry weight"basis and are adjusted for percent moisture,sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIDRO GCS Analytical Method:WI MOD DRO Preparation Method:WI MOD DRO
WDRO C10-C28 ND mg/kg 10.6 1 09/02/15 06:04 09J03/15 13:54
Surrogates
n-Triacontane(S) 77 %. 50-150 1 09/02/15 06:04 09/03/15 13:54 638-68-6 D5
Dry Weight Analytical Method:ASTM D2974
Percent Moisture 5.7 % 0.10 1 09/03/15 70:48
REPORT OF LABORATORY ANALYSIS
This report shali not be reproduced,except in fuli,
Date:09/08/2015 08:36 AM without the written consent of Pace Analylical Services,Inc.. Page 5 of 11
} �
Pace Analytical Services,lnc.
aceAnalytical� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
www.pace►a6s.com �s�z�sm-noo
QUALITY CONTROL DATA
Project: OASIS EAGAN
Pace Project No.: 10320026
QC Batch: MPRP/57469 Analysis Method: ASTM D2974
QC Batch Method: ASTM D2974 Analysis Description: Dry WeighUPercent Moisture
Associated Lab Samples: 10320026001
SAMPLE DUPLICATE: 2068004
1252270001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 12.3 11.5 6 30
SAMPLE DUPLICATE: 2068005
10320571005 Dup Max '
Parameter Units Result Resuit RPD RPD Qualifiers
Percent Moisture "/a 10.0 7.g 25 30
Results presented on this page are in the units indieated by the"Units"cotumn except where an attemate unit(s presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This repoA shall not be reproduced,except in fuli,
Date:09/08/2015 08:36 AM without the written consent of Pace Analytical Services,Inc.. Page 6 Of 11
t
!
Pace Analytical Services,Inc.
� 1700 Elm Street-Suite 200
aceAnalytical Minneapolis,MN 55414
www.pacela6s.com (612)607-1700
QUALITY CONTROL DATA
Project: OASIS EAGAN
Pace Project No.: 10320026
QC Batch: OEXT/30622 Analysis Method: WI MOD DRO
QC Batch Method: WI MOD DRO Analysis Description: WIDRO GCS
Associated Lab Samples: 10320026001
METHOD BLANK: 2066853 Matrix: Solid
Associated Lab Samples: 10320026001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
WDRO C10-C28 mg/kg ND 10.0 09/03/15 11:53
n-Triacontane(S) %. 73 50-150 09/03/15 11:53
LABORATORY CONTROL SAMPLE&LCSD: 2066854 2066855
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units Conc. Result Resuit %Rec %Rec Limits RPD RPD Qualifiers
WDRO C10-C28 mg/kg 80 61.7 64.7 77 81 70-120 5 20
n-Triacontane(S) %. 80 80 50-150
Results presented on this page are in the units indicated by the"Units"column except where an altemate unit Is presented to the right of the resutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:09/08/2015 08:36 AM without the written consent of Pace Analytical Services,Inc.. Page 7 of 11
` «
Pace Analytical Services,Inc.
aceAnalytical� 170M nineapol st,MN'S5414
www.pacelabs.00m (612)607-1700
QUALIFIERS
Project: OASIS EAGAN
Pace Project No.: 10320026
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
N-Nitrosodiphenyiamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANA�YTE QUALIFIERS
D5 The sample was re-weighed into a new container because the sample weight in the original container exceeded the
method specifications.
REPORT OF LABORATORY ANALYSIS
This repoR shail not be reproduced,except in full,
Date:09/08/2015 08:36 AM without the written consent of Pace Anatytical Services,Inc.. Page 8 of 11
r . . . . . . . . . . .. .
Pace Analytical Services,Inc.
aceAnaly�ical� 1700 Eim Street-Suite 200
Minneapolis,MN 55414
www.pacelabs.com (612)607-1700
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: OASIS EAGAN
Pace Project No.: 10320026
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
10320026001 DISPENSER#6 WI MOD DRO OEXT/30622 WI MOD DRO GCSV/16612
10320026001 DISPENSER#6 ASTM D2974 MPRP/57469
REPORT OF LABORATORY ANALYSIS
This report shali not be reproduced,except in full,
Date:09l08/2015 08:36 AM without the written consent of Pace Analyticai Senrices,Inc.. Page 9 of 11
� �
Pace Analytical Services,Inc.
aceAnalJ�ical� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
www.pacelabs.com �s�2>so�-noo
August 31, 2015
Mr. Ron Smith
Pump & Meter
11303 Excelsior Blvd.
Hopkins, MN 55343
RE: Pro'ect: OASIS A�D£AC'�u I
1
Pace Project No.: 10319106
Dear Mr. Smith:
Enclosed are the analytical results for sample(s) received by the laboratory on August 20, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
---��.��___-
Timothy Sandager
timothy.sandager@pacelabs.com
Project Manager
Enclosures
p«FO
2 a` REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
9g0
without the written consent of Pace Analytical Services,Inc.. Page 1 of 13
� '
Pace Analytical Services,Inc.
aceAnalytica!� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
�•Pa�(a�.� (612)607-1700
CERTIFICATIONS
Project: OASIS MARKED
Pace Project No.: 10319106
Minnesota Certification IDs
1700 Elm Street SE Suite 200,Minneapolis,MN 55414 Minnesota Certification#:027-053-137
A2LA Certification#:2926.01 Mississippi Certification#:Pace
Alaska Certification#:UST-078 Montana Certification#:MT0092
Alaska Certification#MN00064 Nevada Certfication#:MN 00064
Alabama Certification#40770 Nebraska Certification#:Pace
Arizona Certification#:AZ-0014 New Jersey Certification#:MN-002
Arkansas Certification#:88-0680 New York Certification#:11647
California Certification#:01155CA North Carolina Certification#:530
Colorado Certification#Pace North Carolina State Public Health#:27700
Connecticut Certification#:PH-0256 North Dakota Certification#:R-036
EPA Region 8 Certification#:8TMS-L Ohio EPA#:4150
Florida/NELAP Certification#:E87605 Ohio VAP Certification#:CL101
Guam Certification#:14-008r Oklahoma Certification#:9507
Georgia Certification#:959 Oregon Certification#:MN200001
Georgia EPD#:Pace Oregon Certification#:MN300001
Idaho Certification#:MN00064 Pennsylvania Certification#:68-00563
Hawaii Certification#MN00064 Puerto Rico Certification
Illinois Certification#:200011 Saipan(CNMI)#:MP0003
Indiana Certification#C-MN-01 South Carolina#:74003001
lowa Certification#:368 Texas Certification#:T704704192
Kansas Certification#:E-10167 Tennessee Certification#:02818
Kentucky Dept of Envi.Protection-DW#90062 Utah Certification#:MN000642013-4
Kentucky Dept of Envi.Protection-VWV#:90062 Vrginia DGS Certification#:251
Louisiana DEQ Certification#:3086 �rginiaNELAP Certification#:Pace
Louisiana DHH#:LA140001 Washington CertificaGon#:C486
Maine Certification#:2013011 West Virginia Certification#:382
Maryland Certification#:322 West Vrginia DHHR#:9952C
Michigan DEPH Certification#:9909 Wisconsin Certification#:999407970
REPORT OF LABORATORY ANA�YSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,inc.. Page 2 of 13
� �
Pace Anaiytical Services,Inc.
aceAnaly�icai� 170 M n'eapol st,MN 55414
www.pacelabs.com
(612)607-1700
SAMPLE SUMMARY
Project: OASIS MARKED
Pace Project No.: 10319106
Lab ID Sample ID Matrix Date Collected Date Received
10319106001 DISPENSEN#1 Solid 08/19/15 02:05 08/20/15 11:50
10319106002 DISPENSEN#2 Solid 08/19/15 02:45 08/20/15 11:50
10319106003 DISPENSEN#3 Solid 08/19/15 02:35 08/20/15 71:50
10319106004 DISPENSEN#4 Solid 08/19/15 02:15 08/20/15 11:50
10319106005 DISPENSEN#5 Solid 08/19/15 04:45 08/20/15 11:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in fuii,
without the written consent of Pace Analytical Services,Inc.. Page 3 of 13
Pace Analytical Services,inc.
aceAnalytical� 1700 Elm Street-Suite 200
Minneapolis.MN 55414
www.pacelabs.com �s�2�so�-noo
SAMPLE ANALYTE COUNT
Project: OASIS MARKED
Pace Project No.: 10319106
Analytes
Lab ID Sample ID Method Analysts Reported
10319106001 DISPENSEN#1 WI MOD GRO CMB 2
10319106002 DISPENSEN#2 WI MOD GRO CMB 2
10319106003 DISPENSEN#3 WI MOD GRO CMB 2
10319106004 DISPENSEN#4 WI MOD GRO CMB 2
10319106005 DISPENSEN#5 WI MOD DRO MT 2
ASTM D2974 JDL 7
REPORT OF LABORATORY ANALYSIS
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0
t
Pace Analytical Services,Inc.
aceAnaly�ical� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
www.pacela6s.com (612)607-1700
ANALYTICAL RESULTS
Project: OASIS MARKED
Pace Project No.: 10319106
Sample: DISPENSEN#1 Lab ID: 10319106001 Collected: 08/19/15 02:05 Received: 08/20/1511:50 Matrix:Solid
Results reported on a"wet-weight"basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method:WI MOD GRO Preparation Method:EPA 5030 Medium Soil
Gasoline Range Organics ND mg/kg 10.0 1 08/25/1511:58 08/26/15 18:57
Surrogates
a,a,a-Trifluorotoluene(S) 96 %. 80-150 1 08/25/75 11:58 OS/26/1518:57 98-08-8
Sample: DISPENSEN#2 Lab ID: 10319106002 Collected: 08/19/15 02:45 Received: 08/20/15 11:50 Matrix:Solid
Resu/ts reported on a"wet-weight"basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method:WI MOD GRO Preparation Method:EPA 5030 Medium Soii
Gasoline Range Organics ND mg/kg 9.9 1 08/25/15 11:58 08l26/15 21:41
Surrogates
a,a,a-Trifluorotoluene(S) 95 %. 80-150 1 08/25/1511:58 08/26/15 21:41 98-08-8
Sample: DISPENSEN#3 Lab ID: 10319106003 Collected: 08/19/15 02:35 Received: 08/20/15 11:50 Matrix:Solid
Resu/ts reported on a"wet-weight"basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method:WI MOD GRO Preparation Method:EPA5030 Medium Soil
Gasotine Range Organics ND mg/kg 10.2 1 08/25/1511:58 08/26/15 22:03
Surrogates
a,a,a-Trifluorotoluene(S) 97 %. 80-150 1 08/25/15 11:58 08l26/15 22:03 98-08-8
Sample: DISPENSEN#4 Lab ID: 10319106004 Collected: 08l19/15 02:15 Received: 08/20/15 11:50 Matrix:Solid
Resu/ts reported on a"wet-weight"basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method:WI MOD GRO Preparation Method:EPA 5030 Medium Soil
Gasoline Range Organics ND mgJkg 10.3 1 08/25/15 11:58 08/26/15 23:55
Surrogates
a,a,a-Trifluorotoluene(S) 94 %. 80-150 1 08/25/15 11:58 08/26/15 23:55 98-08-8
Sample: DISPENSEN#5 Lab ID: 10319106005 Collected: 08/19/15 04:45 Received: 08/20/15 11:50 Matrix:Solid
Resu/ts reported on a"dry weight"basis and are adjusted for percent moisture,sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIDRO GCS Analytical Method:WI MOD DRO Preparation Method:WI MOD DRO
WDRO C10-C28 223 mg/kg 59.8 10 O8/24/15 12:00 08/26/15 16:39
REPORT OF LABORATORY ANALYSIS
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(
Pace Analytical Services,inc.
aceAnalytical� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
www.pace�aas.com (s1z)so7-noo
ANALYTICAL RESULTS
Project: OASIS MARKED
Pace Project No.: 10319106
Sample: DISPENSEN#5 Lab ID: 10319106005 Collected: 08/19/15 04:45 Received: 08/20l15 11:50 Matrix:Solid
Resu/ts reported on a"dry weight"basis and are adjusted for percent moisture,sample size and any dilutions.
Parameters Resuits Units Report Limit DF Prepared Analyzed CAS No. Qual
WIDRO GCS Analytical Method:WI MOD DRO Preparation Method:WI MOD DRO
Surrogates
n-Triacontane(S) 73 %. 50-150 10 08/24/15 12:00 08l26/15 16:39 638-68-6
Dry Weight Analytical Method:ASTM D2974
Percent Moisture 4.8 % 0.10 1 08/24/15 14:09
REPORT OF LABORATORY ANALYSIS
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, � '
Pace Analytical Services,Inc.
aceAnalytical� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
www.pace/abs.com , (612)607-1700
QUALITY CONTROL DATA '
Project: OASIS MARKED
Pace Project No.: 10319106 '
QC Batch: GCV/14300 Analysis Method: WI MOD GRO
QC Batch Method: EPA 5030 Medium Soil Analysis Description: WIGRO Solid GCV '
Associated Lab Samples: 10319106001,10319106002,10319106003,10319106004 '
METHOD BLANK: 2058679 Matrix: Solid '
Associated Lab Samples: 10319106007,10319106002,10319106003,10319106004 '
Blank Reporting '
Parameter Units Result Limit Analyzed Qualifiers ',
Gasoline Range Organics mg/kg ND 10.0 08/26/15 15:55 I',
a,a,a-Trifluorotoluene(S) °/a. 99 80-150 08/26/15 15:55 �
LABORATORY CONTROL SAMPLE&LCSD: 2058680 2058681 '
Spike LCS LCSD LCS LCSD %Rec ', Max
Parameter Units Conc. Result Result %Rec %Rec Limits RPD ' RPD Qualifiers
Gasoline Range Organics mg/kg 50 46.6 45.0 93 90 80-120 3 ' 20
a,a,a-Trifluorotoluene(S) %. 103 100 80-150
MATRIX SPIKE SAMPLE: 2058682 '
10318705001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Gasoline Range Organics mg/kg ND 52.9 48.9 90 80-120
a,a,a-Trifluorotoluene(S) %. 101 80-150
SAMPLE DUPLICATE: 2058683 '
10318705002 Dup Max
Parameter Units Result Result RPD RPD Qualjfiers
Gasoline Range Organics mg/kg ND 5.2� 20 ,
a,a,a-Trifluorotoluene(S) %. 99 g7 0
Results presented on this page are in the units indicated by the"Untts"column except where an altemate unit is presented to the rlght of the result.
REPORT OF LABORATORY ANALYSIS '
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,
�
Pace Analytical Services,Inc.
aceAnaly�ieal� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
�wn+!Pacetebs.com (612)607-1700
QUAUTY CONTROL DATA
Project: OASIS MARKED
Pace Project No.: 10319106
QC Batch: MPRP/57218 Analysis Method: ASTM D2974
QC Batch Method: ASTM D2974 Analysis Description: Dry WeighUPercent Moisture
Associated Lab Samples: 10319106005
SAMPLE DUPLICATE: 2058431
10319261002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 9.3 8.8 4 30
SAMPLE DUPLICATE: 2058671
10319106005 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 4.8 5.2 9 30
Results presented on this page are in the units indicated by the"Units"eolumn except where an altemate unH is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:08/31/2015 03:08 PM without the written consent of Pace Analyticai Services,Inc.. Page 8 Of 13
�
r
Pace Analytical Services,Inc.
� 1700 Elm Street-Suite 200
aceAnalytical Minneapolis,MN 55414
www.pacelabs.com (612)607-1700
QUALITY CONTROL DATA
Project: OASIS MARKED
Pace Project No.: 10319106
QC Batch: OEXT/30525 Analysis Method: WI MOD DRO
QC Batch Method: WI MOD DRO Analysis Description: WIDRO GCS
Associated Lab Samples: 10319106005
METHOD BLANK: 2059627 Matrix: Solid
Associated Lab Samples: 10319106005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
WDRO C10-C28 mg/kg ND 10.0 08/26/15 13:56
n-Triacontane(S) %. 78 50-150 08/26/15 13:56
IABORATORY CONTROL SAMPLE&LCSD: 2059628 2059629
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers
WDRO C10-C28 mg/kg 80 70.3 69.2 88 86 70-120 2 20
n-Triacontane(S) %. 80 80 50-150
Results presented on this page are tn the units Indicated by the"Units"column except where an attemate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in fuli,
Date:08l31/2015 03:08 PM without the written consent of Pace Analyticai Services,lnc.. Page 9 of 13
�
Pace Analytical Services,Inc.
aceAnalytical� 170Min eapol st,MN'55414
www.pacelabs.com (612)607-1700
QUALIFIERS
Project: OASIS MARKED
Pace Project No.: 10319106
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
J-Estimated concentration above the adjusted method detection timit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate°/a recovery and RPD values.
LCS(Dj-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,inc.
1700 Elm Street-Suite 200
aceAnaly�ical Minneapolis,MN 55414
�+•Pe��� (612)607-1700
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: OASIS MARKED
Pace Project No.: 10319106 ,
Analytical i
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch �
70319106005 DISPENSEN#5 WI MOD DRO OEXT/30525 WI MOD DRO GCSV/16543
10319106001 DISPENSEN#1 EPA 5030 Medium Soil GCW14300 WI MOD GRO GCV/14321
10319106002 DISPENSEN#2 EPA 5030 Medium Soil GCV/14300 WI MOD GRO GCV/14321
10319106003 DISPENSEN#3 EPA 5030 Medium Soii GCV/14300 WI MOD GRO GCV/14321
10319706004 DISPENSEN#4 EPA5030 Medium Soil GCV/14300 WI MOD GRO GCV/14321
10319106005 DISPENSEN#5 ASTM D2974 MPRP/57218
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♦ �
Pace Analyticai Services,loc.
aceAnalytical� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
www.pacela6s.com
(612)607-1700
August 31, 2015
Mr. Ron Smith
Pump & Meter
11303 Excelsior Blvd.
Hopkins, MN 55343
RE: Project: OASIS EAGAN
Pace Project No.: 10319107
Dear Mr. Smith:
Enclosed are the analytical results for sample(s) received by the laboratory on August 20, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
--��.�`_—
Timothy Sandager
timothy.sandager@pacelabs.com
Project Manager
Enclosures
a��o
_� m-a' REPORT OF LABORATORYANALYSIS
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Pace Analyticai Services,Inc.
aceAnaJytical� 170Minl eapol st,MN155414
www.pacetabs.com (612)607-1700
CERTIFICATIONS
Project: OASIS EAGAN
Pace Project No.: 10319107
Minnesota Certification IDs
1700 Elm Street SE Suite 200,Minneapolis,MN 55474 Minnesota Certification#:027-053-137
A2LA Certification#:2926.01 Mississippi Certification#:Pace
Alaska Certification#:UST 078 Montana Certification#:MT0092
Alaska Certification#MN00064 Nevada Certification#:MN 00064
Alabama Certification#40770 Nebraska Certification#:Pace
Arizona Certification#:AZ-0014 New Jersey Certification#:MN-002
Arkansas CertificaUon#:88-0680 New York Certification#:11647
California Certification#:01155CA North Carolina Certification#:530
Colorado Certification#Pace North Carolina State Public Health#:27700
Connecticut Certification#:PH-0256 North Dakota Certification#:R-036
EPA Region 8 Certification#:8TMS-L Ohio EPA#:4150
Florida/NELAP Certification#:E87605 Ohio VAP Certification#:CL101
Guam Certification#:14-008r Oklahoma Certification#:9507
Georgia Certification#:959 Oregon Certification#:MN200001
Georgia EPD#:Pace Oregon Certification#:MN300001
Idaho Certification#:MN00064 Pennsylvania Certification#:68-00563
Hawaii Certification#MN00064 Puerto Rico Certification
Illinois Certification#:200011 Saipan(CNMI)#:MP0003
Indiana Certification#C-MN-01 South Carolina#:74003001
lowa Certification#:368 Texas Certification#:T104704192
Kansas Certification#:E-10167 Tennessee Certification#:02818
Kentucky Dept of Envi.Protection-DW#90062 Utah Certification#:MN000642013-4
Kentucky Dept of Envi.Prot�ction-WW#:90062 �rginia DGS CertificaGon#:251
Louisiana DEQ Certification#:3086 VirginiaNELAP Certification#:Pace
Louisiana DHH#:LA140001 Washington Certification#:C486
Maine Certification#:2013011 West Virginia Certification#:382
Maryland Certification#:322 West vrginia DHHR#:9952C
Michigan DEPH Certification#:9909 Wisconsin Certification#:999407970
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Pace Analytical Services,Inc.
aceAnalytical� 170 M nlneapol st,MN155414
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SAMPLE SUMMARY
Project: OASIS EAGAN
Pace Project No.: 10319107
Lab ID Sample ID Matrix Date Cotlected Date Received
10379107001 10K DIESEL TANK 1A Solid 08/19/1512:15 08/20/15 11:50
10319107002 10K DIESEL TANK 18 Solid O8/19/15 12:3U O8/20/1511:50
10319107003 10K PREM TANK 2A Solid OS/19/15 01:35 08/20J15 11:50
70319107004 10K PREM TANK 2B Solid 08/19/15 01:45 08/20/15 11:50
10319107005 10K MID GRADE 3A Solid 08/19/15 02:30 08/20/1511:50
10319107006 10K MID GRADE 36 Solid 08/19/15 02:50 08/20/15 11:50
10319107007 10K REG TANK 4A Solid 08/19/15 03:40 08/20/15 11:50
10319107008 70K REG TANK 46 Solid 08/19/15 03:50 08/20/1511:50
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' Pace Analytical Services,Inc. '
aceAnalytical� ,�oo E�m St�eet_S��te zoo
Mianeapoiis,MN 55414
www.pacelans.com (s12)so7-1700 �
SAMPLE ANALYTE COUNT II
Project: OASIS EAGAN II
Pace Project No.: 10319107
Analytes
Lab ID Sample ID Method Analysts Reported
10319107001 10K DIESEL TANK 1A WI MOD DRO MT 2
ASTM D2974 JDL 1
10319107002 10K DIESEL TANK 1B WI MOD DRO MT 2
ASTM D2974 JDL 1
10319107003 10K PREM TANK 2A WI MOD GRO CMB 2
10319107004 10K PREM TANK 26 WI MOD GRO CMB 2
10319107005 10K MID GRADE 3A WI MOD GRO CMB 2
10319107006 10K MID GRADE 3B WI MOD GRO CMB 2
10319107007 10K REG TANK 4A WI MOD GRO CMB 2
10319107008 10K REG TANK 4B WI MOD GRO CMB 2
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,Inc.
aceAnaly�ical� 1700 Elm Street-Suite 200
Minneapoiis,MN 55414
►nnuPece�ebs.com (612)607-1700
ANALYTICAL RESULTS
Project: OASIS EAGAN
Pace Project No.: 10319107
Sample: 10K DIESEL TANK 1A Lab ID: 10319107001 Collected: 08/19/15 12:15 Received: 08/20/15 11:50 Matrix:Solid
Resu/ts reported on a"dry weigbt"basis and are adjusted for percent moisture,sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIDRO GCS Analytical Method:WI MOD DRO Preparation Method:WI MOD DRO
WDRO C10-C28 ND mg/kg 9.2 1 08/24/15 12:00 08/26/15 14:10
Surrogates
n-Triacontane(S) 83 %. 50-150 1 08/24/15 12:00 08/26/15 14:10 638-68-6
Dry Weight Analytical Method:ASTM D2974
Percent Moisture 18.5 % 0.10 1 08/24/15 14:10
Sample: 10K DIESEL TANK 1 B Lab ID: 10319107002 Collected: 08/19/15 12:30 Received: 08/20/1511:50 Matrix:Solid
Resu/ts reported on a"dry weighY'basis and are adjusted for percent moisture,sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIDRO GCS Analytical Method:WI MOD DRO Preparation Method:WI MOD DRO
WDRO C10-C28 9.8 mg/kg 8.3 1 08/24/15 12:00 08/26/1514:17 T6
Surrogates
n-Triacontane(S) 76 °/a. 50-150 1 08/24/15 12:00 08/26/15 14:17 638-68-6 '
Dry Weight Analytical Method:ASTM D2974
Percent Moisture 17.6 % 0.10 1 08/24(1514:10
Sample: 10K PREM TANK 2A Lab ID: 10319107003 Collected: 08/19/15 01:35 Received: 08/20/15 11:50 Matrix:Solid
Results reported on a"wet-weight"basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method:WI MOD GRO Preparation Method:EPA 5030 Medium Soil
Gasoline Range Organics ND mg/kg 9.8 1 08/25/15 11:58 08/27/15 00:17
Surrogates
a,a,a-Trifluorotoluene(S) 95 %. 80-150 1 08/25/15 11:58 08/27/15 00:17 98-08-8
Sample: 10K PREM TANK 2B Lab ID: 10319107004 Collected: 08/19/15 01:45 Received: 08/20/15 11:50 Matrix:Solid
Results reported on a"wet-weight"basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method:WI MOD GRO Preparation Method:EPA 5030 Medium Soii
Gasoline Range Organics NO mg/kg 9.8 1 08/25/15 11:58 OS/27/15 00:39
Surrogafes
a,a,a-Trifluorotoluene(S) 96 %. 80-150 1 08/25/15 11:58 08/27/15 00:39 98-08-8
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,Inc.
aceAnaly�ical� 170M nlneapol st,MN'S541�4
www.pacelabs.com
(612)607-1700
ANALYTICAL RESULTS
Project: OASIS EAGAN
Pace Project No.: 10319107
Sample: 10K MID GRADE 3A Lab ID: 10319107005 Collected: 08/19/15 02:30 Received: 08/20/15 11:50 Matrix:Solid
Resu/ts reported on a"wet-weight"basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method:WI MOD GRO Preparation Method:EPA 5030 Medium Soil
Gasoline Range Organics ND mg/kg 10 1 08/25/15 11:58 08/27/15 01:02
Surrogates
a,a,a-Trifluorotoluene(S) 95 %. 80-150 1 08/25/1511:58 OS/27/15 01:02 9&08-8
Sample: 10K MID GRADE 36 Lab ID: 10319107006 Collected: O8/19/15 02:50 Received: 08/20/1511:50 Matrix:Solid
Resu/ts reported on a"wet-weight"basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method:WI MOD GRO Preparation Method:EPA 5030 Medium Soil
Gasoline Range Organics ND mg/kg 9.8 1 08/25/1511:58 08/27/15 02:54
Surrogates
a,a,a-Trifluorotoluene(S) 97 %. 80-150 1 08/25/15 11:58 08/27/15 02:54 98-08-8
Sample: 10K REG TANK 4A Lab ID: 10319107007 Collected: 08/19/15 03:40 Received: 08/20/15 11:50 Matrix:Solid
Resu/ts reported on a"wet weight"basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method:WI MOD GRO Preparation Method:EPA 5030 Medium Soil
Gasoline Range Organics ND mg/kg 10.2 1 08/25/15 11:58 08/27/15 01:24
Surrogates
a,a,a-Trifluorotoluene(S) 95 %. 80-150 1 08/25/15 11:58 08/27/15 01:24 98-08-8
Sample: 10K REG TANK 4B Lab ID: 10319107008 Collected: O8/19/15 03:50 Received: 08/20/15 11:50 Matrix:Solid
Results reported on a"wet-weight"basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method:WI MOD GRO Preparation Method:EPA 5030 Medium Soil
Gasoline Range Organics ND mg/kg 10.1 1 08/25/1511:58 08/27/15 01:47
Surrogates
a,a,a-Trifluorotoluene(S) 95 %. 80-150 1 08/25/15 11:58 08/27/15 01:47 98-08-8
REPORT OF LABORATORY ANALYSIS
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T
1
Pace Analytical Services,Inc.
aceAnalyticai� 170M nl eapol st,MN155414
wwx<pacelabacom (612)607-4700
QUALITY CONTROL DATA
Project: OASIS EAGAN
Pace Project No.: 10319107
QC Batch: GCV/14300 Analysis Method: WI MOD GRO
QC Batch Method: EPA 5030 Medium Soil Analysis Description: WIGRO Solid GCV
Associated Lab Samples: 10319107003,10319107004,10319107005,10319107006,10319107007,10319107008
METHOD BLANK: 2058679 Matrix: Solid
Associated Lab Samples: 10319107003,10319107004,10319107005,10319107006,10319107007,10319107008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Gasoline Range Organics mg/kg ND 10.0 08/26/15 15:55
a,a,a-Trifluorototuene(S) %. 99 80-150 08/26/15 15:55
LABORATORY CONTROL SAMPLE&LCSD: 2058680 2058681
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units Conc. Result Resuit %Rec %Rec Limits RPD RPD Qualifiers
Gasoline Range Organics mg/kg 50 46.6 45.0 93 90 80-120 3 20
a,a,a-Trifluorotoluene(S) %. 103 100 80-150
MATRIX SPIKE SAMPLE: 2058682
10318705001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Gasoline Range Organics mg/kg ND 52.9 48.9 90 80-120
a,a,a-Trifluorotoluene(S) %. 101 80-150
SAMPLE DUPLICATE: 2058683
10318705002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Gasoline Range Organics mg/kg ND 5.2J 20
a,a,a-Trifluorotoluene(S) %. 99 97 0
Resutts presented on this page are tn the units tndicated by the"Units"column except where an aitemate untt is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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l �
Pace Analytical Services,lnc.
aceAnaly�ical� 170 Minl eapol st,MN'554/4
www.pacelabs.com (612)607-1700
QUALITY CONTROL DATA
Project: OASIS EAGAN
Pace Project No.: 10319107
QC Batch: MPRP/57218 Analysis Method: ASTM D2974
QC Batch Method: ASTM D2974 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 10319107001,10319107002
SAMPLE DUPLICATE: 2058431
10319261002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 9•3 8.8 4 30
SAMPLE DUPLICATE: 2058671
10319106005 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 4.8 5.2 9 30
Results presented on this page are in the units indicated by the"Units"column except where an altemate unk is presented to the�ight of the resulk
REPORT OF LABORATORY ANALYSIS
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Pace Analyticai Services,Inc.
aceAnalytical� 1700 Elm Street-Suite 200
Minneapolis,MN 55414
www.pacefa6s.com (612)607-1700
QUALITY CONTROL DATA
Project: OASIS EAGAN
Pace Project No.: 10319107
QC Batch: OEXT/30525 Analysis Method: WI MOD DRO
QC Batch Method: WI MOD DRO Analysis Description: WIDRO GCS
Associated Lab Samples: 10319107001,10319107002
METHOD BLANK: 2059627 Matrix: Solid
Associated Lab Samples: 10319107001,10319107002
Blank Reporting
Parameter Units Resuit Limit Analyzed Qualifiers
WDRO C10-C28 mg/kg ND 10.0 08/26/15 13:56
n-Triacontane(S) °/a. 78 50-150 08/26/15 13:56
LABORATORY CONTROL SAMPLE&LCSD: 2059628 2059629
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers
WDRO C10-C28 mg/kg 80 70.3 69.2 88 86 70-120 2 20
n-Triacontane(S) %. 80 80 50-150
Results presented on this page are in the untts iadicated by the"Units"column except where an a�temate unk is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,Inc.
1700 Elm Street-Suite 200
aceAnalytical Minneapolis,MN 55414
www.pacelabs.com (612)607-1700
QUALIFIERS
Project: OASIS EAGAN
Pace Project No.: 10319107
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(0)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Dupticate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
T6 High boiling point hydrocarbons are present in the sample.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,Inc.
aceAnalytical� 1700 Eim Street-Suite 200
Minneapolis,MN 55414
www.pacefabs.com (612)607-1700
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: OASIS EAGAN
Pace Project No.: 10319107
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
10319107001 10K DIESEL TANK 1A WI MOD DRO OEXT/30525 WI MOD DRO GCSV/16543
10319107002 10K DIESEL TANK 16 WI MOD DRO OEXT/30525 WI MOD DRO GCSV/16543
10319107003 10K PREM TANK 2A EPA 5030 Medium Soil GCV/14300 WI MOD GRO GCV/14321
10319107004 10K PREM TANK 26 EPA 5030 Medium Soil GCV/14300 WI MOD GRO GCV/14321
10319107005 10K MID GRADE 3A EPA 5030 Medium Soil GCV/14300 WI MOD GRO GCV/14327
10319107006 10K MID GRADE 3B EPA5030 Medium Soil GCV/14300 WI MOD GRO GCV/14321
10319107007 10K REG TANK 4A EPA 5030 Medium Soil GCV/14300 WI MOD GRO GCV/14321
10319107008 10K REG TANK 4B EPA 5030 Medium Soil GCV/14300 WI MOD GRO GCV/14321
10319107001 10K DIESEL TANK 1A ASTM D2974 MPRP/57218
10319107002 10K DIESEL TANK 1 B ASTM D2974 MPRP/57218
REPORT OF LABORATORY ANALYSIS
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