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1534 Lone Oak Rd - Soil EvaluationsRAUN°N INTERTEC November 22, 1995 Mr. 7eff Luehrs Dakota County Environmental Management Department 14955 Galaxie Avenue Apple Valley, MN 551248579 Deaz Mr. Luehrs: Braun Intertec CerpowKon 1345 NorThland Orive Mendom Haighh, Minnewta 551241141 612b83.8700 Fmc:683-8888 Enginears and Scienlisfs Serving rhe Built and Naturaf EnvironmenM Project No. C1viXI{-95-0722 Re: Subsurface Investigation, Rubber Disposal Site, 1534 Lone Oak Road, Eagan, MN As authorized by Dakota County, Braun Intertec Corporation conducted a subsurface investigation at the refecenced site during October 1995. Our tesults aze provided in the attached report. Should you have any questions regazding the contents of this report, please contact me at (612) 683-8756. Sincerely, ? Patricia M. Terhaar, CPG Supervisor, Hydmgeologic Investigations Table of Contents I. Introduction . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . 1 II. Scope of Work . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 III. Results ............................................ 2 ; A. Site Geology and Hydrogeology . . . . . . . . . . . . . . . . . . . . . . . . . . 2 ' B. Waste Characteristics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 C. Analytical Resuits for Soil and Groundwater . . . . . . . . . . . . . . . . . . 3 D. Vapor Monitoring Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 IV. Conclusions and Recommendations . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 V. General ............................................ 5 Tables 1. Aaalytical Results for Waste Samples 2. Analytical Results for Soil Sunple 3. Analytical Results for Groundwater Samples Figures 1. Site Map 2. Groundwater Contour Map Appendices A. Boring Logs and Well Construction Diagrams B. Laboratory Reports I. Introduction Braun Intertec was authorized by Dakota Counry to conduct a subsurface investigation at 1534 Lone Oak Road in Eagan, Minnesota. The azea to be investigated was usaci as a disposal site for rubber col}ected at Fort Snelling during World Waz II. The purpose of this investigauon was to assess subsurface conditions and confirm the absence of potentially hazardous waste. The site is located in a residential azea, and several houses overlie or aze adjacent to the fill azea. A seismic survey conducted previousty indicated that the waste ranges in thiclmess from a few feet to approximately 30 feet and is overlain by 0 to 14 feet of soil. II. Scope of Work The following tasks were performed by Braun Intertec for this project. A Site-Specific Safety Plan was prepazed. A hollow-stem auger boring was conducted through the waste at the location specified as VW-1 on the attached site map. The boring was advanced ihrough the waste until native soils were encountered at approximately 23 feet. Samples of the waste were collectefl from an approximate depth of 10 feet and from 20 feet for analysis of RCRA metals and ubestos. The borehole was monitored for methane, and the cuttings were screened for organic vapors using a photoionization detector (PID). At the termination of the boring, a split-barrel soil sample was collected. The soIl was screened for organic vapors using jaz headspace procedures, and a sample was collected for analysis of volatile organic compounds (VOCs) using MDH Method 466A, polynuclear azomatic hydrocarbons (PAHs) by Method SW-846 8270 and RCRA metals. A vapor monitoring well was installed to a depth of 20 feet in the boring. A consizuction diagram is provided in Appendix A. Approximately 24 hours and 48 hours after instailation, methane concentrations in the vapor well were measured. An air sample was also collected using a chazcoal tube for analysis of VOCs. Dakota County Project No. CMA,Y-45-0722 November 22, 1995 Page 2 • Three additional soIl borings were conducted for installadon of temporary monitoring wells. These temporary wells were labeled PZ-1 through PZ-3. Localions aze shown on the attached site map. Well construction diagrams aze provided in Append'u A. • After purging three well volumes, groundwater samples were collected from each of the temporary wells and analyzed for the following pazameters: Field pH Total RCRA metals VOCs by IvIDH 465E Dissoived RCRA metals PAHs by EPA 610 Total Alkaiinity Ammonia as Nitrogen Sufide Potassium Ca hazdness Nitrate as Niuogen Sulfate Sodium A duplicate sample pabeled PZ-A) from PZ-3 and a field blank were also colleaed and analyzed. Ail analytical samples were placed in a cooler and transported to our laboratory following standazd chain-0f-custody procedures. • The wells were removed and the boreholes were sealed after sampling was compieted. • Waste cuttings were placed in drums and are being stored temporarily az Braun Intertec. Foc disposal purposes, a sample of the waste cuttings was analyzed for RCRA metais using TCLP. As requested by Dakota County, we aze coordinating disposal with USPCI. M. Results A. Site Geology and Hydrogeology As indicated by the boring logs (Appendix A), all borings encountered 3 to 4 feet of topsofl. At VW-1 and PZ-3, the topsoil (not native) was underlain by rubber debris to depths of 23 feet and 21 feet, respectively. Siz to 7 feet of clayey sand was encountered in PZ-2 and PZ-3 at different horizons. The remaining soils consisted of silty sand and poorly graded sand. •t Dakota Counry Project No. CMXX-95-0722 November 22, 1995 Page 3 The water table occurs az a depth of about 25 feet at the locarion of PZ-3. At PZ-1 and PZ-2, which are located at the base of a hill, the water table was about 2.5 feet and 0.2 feet below the surface, respectively. The groundwater flow direction is southwesterly, consisteirt with topography (Figure 2). B. Waste Characteristics The waste rubber observed in the soil borings was shredded and chopped into small to medium pieces. It appeared to consisi primarily of clothing remnants such as boots or raincoats. Chemical analysis of tlte waste for RCRA metals indicated high concentrations of azsenic, bazium, cadmium and lead (Table 1). No asbestos was detected in the samgles. Laboratory reports are contained in Appendix B. TCI.P analysis of RCRA metals was performed on a sample of the waste cuttings. Results are included in Appead'u B. Concentrations are below the limits established for the toxicity characteristic. Therefore, the waste is not considered to be hazardous. C. Analytical Resuits for Soil and Groundwater The soil sample collected from beneath the waste in VW-1 contained relatively low concentrations of azsenic, bazium and chromium (Table 2). No other RCRA metals, VOCs or PAHs were detected. Groundwater analyticai results are summarized in Table 3. Two VOCs, bromodichloromethane and chloroform, were detected in at least one well; however, concentrations were below the Minnesota Department of Health, Health Aisk Limit (HRL). Two PAHs, benzo(k)fluoranthene and benzo(a)pyrene, were detected in PZ-3 at relatively low conceirtrations. No HRL has been established for these compounds, but for comparison, they are below the Maximum Contaminant Levels (MCis) established for public drinking water supplies. The first extraction for the PAH analysis did not work, and therefore, the sample had to be re-ectracted past the EPA recommended holding time. The quality of the resulting data is not believed to have been significandy affectefl. The tota( RCRA metals concentrations for the groundwatec samples are high. This is likely a resuit of sediment in the samples since the dissolved conceatrations are relatively low or were not detected. If the weiis had been rigorously developed and allowed to set longcr, the total metals concentrations would likely have been much lower. Dakota Counry Project No. CrXX-95-0722 November 22, 1995 Page 4 D. Vapor Monitoring Results No VOCs were detected in the air sample collected from the vapor monitoring well (Appendix B). Very lugh methane concentrations (169b gas by volume) were measured in the vapor monitoring well both one and two days after instailation. _ IV. Conclusions and Recommendations Two of the borings at the site encountered waste rubber at 3 ro 4 feet below ground surface. The thickness of the waste at these locations was 18 m 19 feet. Analysis of the waste indicated high concentrations of inetals, particulazly bazium and lead. Results of TCLP analysis indicate that the waste is not hazardous under the toxicity chazacteristic. Based on water levels measured in the temporary monitoring wells, groundwater at the site is flowing southwest, consistent with topography. Concentrations of total metals in the groundwater aze high. However, since dissolved metal concentrations are, for the most part, below detection limits, the total metal concentrations aze likely due to sediment and not a reflection of groundwater quality. A soi] sample collected from unmediately below the waste did not indicate elevated levels of inetals in the soils. The major environmentai concem at this site is the presence of explosive gas (methane) in ihe subsurface. The source and lateral exteat of the methane is unknown. We did not observe any significant organic material in the waste rubber which would be likely to produce high concentrations of inethane. It is unlikely that the cubber itself wouid produce explosive gas. Other potential sources for the methane are: leaking natural gas lines, abandoned septic systems, sewers, or other unknown deposits of degrading waste. The porous nature of the shredded rubber may provide a conduit or a repository for the methane. The aznount of inethane detected in the vapor monitoring well is over three times the lower exptosive timit (200 percent of the lower explosive limit is 5 percent gas by volume). These levels aze considered high and may present a significant risk to the safety of nearby residences if gas enters the dwelling or other confined spaces at explosive concentrations. As we discussed with Dakota Counry personnel during monitoring of the vapor well on October 13, 2995, the basemenu of the three houses closesi to VW-1 should be monitored for methane and methane alarms should be installed. In addition, vapor monitoring points should be installed next to the foundaUOns of the houses. . ?€ Dakom counry Projea No. OIIGY-95-0722 November ZZ, 1995 Page 5 We recommend that the potendal sources of tiLe metfiane be imesagated. At a m;n?TMnm. dtis could include: . discussions with the locai ;as compaay, including potenriai sampiing and "fingerPrinting" of dte gas; • monitoring of nearby. sewess for expiosive aas; and . interviews with adjacent home owners ro obtain informacion oa rhe location of old sepdc systems, composs piles or other nearby disposal sices. Based on the informarion obtained, addiuonal smdies shouid be perfoffied ro determine the extent of the methane and to evaluate potendal coaecrive measures. V. General In performing its services, Braun Tn[ectec used diaz degree of care and skill ordiaarily exercised under similaz circumstances by reputable membecs of its profession practicing in the same locality. No orher warranty is made or imended. r:\wpr,=\==\9so722Xom.AOi , I? ? r : T i I Tabie 1 Analytical Results for Waste Samples (mB/KB) Pazametes - 110 feet ' 20 feef Arsenic, Total 25 42 Barium, Total 540 1600 Cadmium, Total 58 25 Chromium, Total 16 25 Lead, Total 1600 4400 Mercury, Total ND ND Selenium, Total ND ND Silver, Total 1•2 NM Asbestos ND Nm 11 ND = Not Derected f:\wpfi1eskmxz95\07 2 210 7 22.T Table 2 Analytical Results for Soil Sample (25') Pacametes mgtK VOCs None Detected PAHs None Detected Arsenic, Total 6.4 Barium, Total 24 Cadmium, Total ND Chromium, Total 6.8 Lead, Total ND Mercury, Total ND Selenium, Total ND Silver, Total ND ND = Not Da[ected f:lwpfilesMmxx19510722\0722.T Table 3 Analytical Results for Groundwater Samples ? (µg/L unless otherwise indicated) ?Pm?eter ?'?:., _ :F .-PZ:L -, _ . • M_?-:: PZ.3: Bromodichlotomethane ND 1.5 ND (ND) 6 Chlorofotm ND 5.2 3.6 (ND) 60 Benzo(k)fluoranthena ND ND 0.04 (0.06) NA Beuzo(a)pyrene ND ND 0.10 (0.14) NA Alkalinity, Total mg1L 450 410 480 (460) NA Sulfate mg/L 49 3.7 51(52) NA Sulfide, Total mg/L 1.4 2.8 3(1.0) NA Nitogen, Ammonia mg/L 0.03 0.63 1.2 (0.99) NA Nitrogen, Nitrate mg/L 1.1 0.11 028 (0.29) 10,000 Arsenic, Total 430 ND 1400 (I100) NA Barium, Total 1400 2400 8800 (8900) 2000 Cad¢uum, ToW ND ND ND (ND) 4 Chromium, Total 360 340 1100 (1000) 20.000 Hazdness, Calcium mgEq/L 1500 1900 850 (870) NA Lead, Total 120 160 5200 (5300) NA Mucury, Totsl 1.6 1.6 7.9 (8.4) NA Potassium, Total 17,000 21,000 42,000 (41,000) NA Selenium, Tota( ND ND ND (ND) 30 Silvu, Total ND ND ND (ND) 30 Sodium, Total 27,000 72.0D0 89,000 (98,000) NA Arsenic, Dissolved ND ND ND NA Barium. Dissolved 59 76 270 (260) 2000 Cadmium, Dissolved ND ND ND ND 4 Chromium. Dissolved ND ND ND ND 20,000 Lead, Dissolved ND ND ND ND NA Mercury, Dissolved 0.5 ND ND ND NA Selenium, Dissolved ND ND ND ND 30 Silver, Diseolved ND ND ND ND 30 NA = No[ Appliwble ND = No[ DeutlW ' HRL = NIDH Halth Rut Limit Dupliate sample taultr slmwa m puwthaa No VOCs werc detated m the field bladc f: \wpfileskmxx\95W72210722.T Y LONE OAK ROAD - --^ - - --T - - - - Tr- - R.o.w. - -1 -- - -- I --- ?? 1 ? ? ? I . . ? 1534 I . \ 1 iI \ ?APPROXIMA'fE LOCAl10N OF7 I I 1 1 VAPOR MONITORING WELL J I ? 1 ? 1 I \ . 1 GROUNDWATER ? I 1 FLOW DIREC710N 1 ? PZ? 3 i I N 1. 796.10 PZ-2 1 `96 9? I 1 25' 0 50' 96) I 4-? >9 0 SCALE 1"= 50' a'Sp 9B I 1 •3 ) O I i cncrun , 91T l0 - - PROPERTY L1NE 1 pZS'? }? I} PIEZOMETER ? I ? CROUNDWATER CONTOUR ELEVAl10N (FT.) 795.77 GROUNDWATER ELEVAl10N (fT.) ? ? . \ B RAY Nr INTERTEC GROUNDWATER CONTOUR MAP DAKOTA COUNTY 7534 LONE OAK ROAD EAGAN, MINNESOTA INT RENSION SHEET oanvm er. JqG it-13-95 APP'D BY: PMT 11-13-95 oF doe No. CMXX-95-0722 owc. NO. MX50722 FIGURE N0. Sc? 7"- 50' z R W O . . . LONE OAK RITA. - - - - - - --?- - - - - R . 0 . W. - - - T - - - - - - - ? - ? ` ? s - T { - / / . . . 7534 t• 1 \ 1 ? i APPROXIMATE LOCATION 7 ? OF VENT WELL ? 1 Z / . . PZ-2 1 1 1 + 1 1 , ? 1 1 1 1 1 l ?. : PZ-1? . F / 1 / ? LEGEND , PROPERTY IINE PIEZOMETER I \ 30' 0 gp' SCAI,E 1"= 80' ? - -{ ?- - - - - - - -T- ?l i I , ? o ? ? ; I ? I LT -..-..- -..-.._ ?..? .- ?..-..-.._..?.. i ? i / I I -n INT OATE c oeavm ev: JAG 11-3-95 SITE MAP r ? APP'D BY: pMT 11-13-95 DAKOTA COUNTY BRAUN o .ros N0. CMXX-95-0722 7534 LONE OAK ROAD -. DWC.NO. MX50722 1 SHEET OF EAGAN, MINNESOTA I NT E RTE C SCaIE 1"= fi0' Appendix A Borimg Logs and Well Construction Diagrams LOG OF BORING PROJECT: CD'LY7L-95-0722 BORING: P/-1 LOCATION: Dakota County See site map. 7534 Lone Oak Road Eagan ATinnesota , DATE: 10110/95 SCALE: 1" = 4' Elev. Depth ASTM Description of Macerials - 798.0 0.0 Symbol (ASTM D2488) BPF Tesks or Notes • TOPSOIL: Organic Clay, black, moist. 794.0 40 (Topsoil) SP POORLY GRADED SAND with SII.T, fine SM grained, brown, waterbearing, laose. 20 (Alluvium) 790.0 8.0 SM SILTY SAND, fiue grained, brownish grey, 789.0 9.0 waterbearing. SP (Alluvium) 22 . POpRLy GRADED SAND, fine to medium grained, brawn, waterbeacing, medium deuse to very loose. (Alluvium) 82.5 15. 2 END OF BORING Set screen from S to 15 feet. ChCLX-95•0722 Hraun Inmrtec PZ-I page 1 oE t LOG OF BORING PROJECT: ChLYX-95-0722 BORING: . PZ-2 LOCATION: See site map. Dakota County 1534 Lone Oak Road Edg811, MIMPSOfB DATE: 10/10/95 SCAI.E: 1" = 4' Elev. Depth ASTM Description of Materials - B PF Tests or Notes 796.3 0.0 Symbol (ASTM D2488) ^ TOPSOII,: Organic Clay, black, moist. ^ • (Topsoil) SC : CLAYEY SAND, fine grained, yellowish bmwn, water6earing, loose. 4 (Alluvium) SP POORLY GRADED SAND, fine to medium ' grained, brown, waterbearing. (Alluvium) 781.3 15.0 END OF BORING Screen set from 5 to 15 feet. PZ-2 oage ( of 1 CMX7C-95-0722 unun wenec LOG OF BORING PROJEGT: CMXY-95-0722 BORING: P'j,-3 LOCATION: Dakota County See site map. 1534 Lone Oak Road Eagan MinnesoW , DAT'E: SCAI.E: 1" = 4' Elev. Depth ASTM Description of Materials ' I 822.0 0.0 Symbol (ASTM D2488) BPF WL Tests or Notes ^ TOPSOIL: Silty Sand, fine grained, moist. (TaPsail) 819.0 3.0 Rubber de6ris. 801.0 71.0 9 SC :. CLAYEY SAND, fine grained, grey, moist, medium dense. (Alluvium) 13 794.0 28.0 SP POORLY GRADED SAND, fine grained, brown, medium dense to very dense. (Alluvium) CbDOC-95-0722 Bnunlnteftec P2-3 page 1 of2 LOG OF BORING CNOdC-95-0722 nnun imc. LOG OF BORING PROJECT: CMl'Y-95-0722 BORING: VW-1 LOCATION: Dakota County See site map. 1534 Lone Oak Road Eagan Minnesota , DATE: 10/11/95 SCALE: 1" = 4' Elev. Depth ASTM Description of Mazetials - I 821 0.0 Symbol (ASTM D2488) BPF WL Tests or Notes - TOPSOII.: Silty Sand, fine grained, black to dark brown. 817 4.0 w (Topsoil) Rubber debris. 14 22 798 23.0 SP POORLY GRADED SAND, fine gtained, brown, moist. 796 - (Alluvium) END OF BORING Water not observed with 25 feet of hollow-stem auger in the ground. 0N,l7C-95-0722 Bnun Luerteo V W-1 page 1 of 1 MN Unique Well Number NA Monitoring Well Field Data Sheet Client Dakota CounN Project Number ChA7C-95-0722 Ciry/Staae EaRan. MN Well Number PZ-1 Well Locadon See site mao Date of Installation 10-10.95 Crew MR/GS Geologist RF Stick up (± 0.1') 2.3' Top of Riser Pipe 800.33' elevation (+ 0.01'w/o cap) Ground Surface Eleva[ion 798.0' ,-± 0.1') Approximate depth w warer 6efore instailatio¢ 5' Approximate depth to fust water enwuntered in drilling 4' Protective Cover: Type: None Leegth: Lock No. None Concrete Surface Seal: Yes _ No X Grout Above Seal: Neat Cement Grou[ Benroniro Seal pty" None Riser Pipe: Type Diameter Total Length Sections used Coupfiags Cap PVC 2" 1 No Yes X No Sesl Material: Type Bemmnite ch pmomt used (lb) 50 Filter Maferial: Type Silica sand Amomt used (Ib) 400 Depth to Top of Seal Depth to Bottom of Seal Depth m Top of Screen Surface 2.8' 43' Screen: Type PVC Slot Siu .010 Length 10' Diameter 2" gamarks: Temoorazv iastallatioa Compleozd by: Depth m Bottom of Screen 14.3' Depth to Bottom of Boting 15' Method of advance: HSA X Casing Tricone I.D. 4 1/4" I.D. O.D. sRauN=° INTERTEC f:\wpfilnsltmxik95\0722W722.F01 MN Unique Well Number NA Monitoring Well Field Data Sheet Client Dakota CounN Project Number CMXX-95-0722 City/Staoe Eaean. MN Well Number PZ-2 Wel! Location See site mao Date of Installaflon 10-10.95 Crew MR/GS Geologist / Stick up (+ 0.1') 2.0' Top of Riser Pipe 79833' elevation (+ 0.01'w/o cap) Ground Surface Elevarion 7963' (± 0.1') Approximare depth ro water before installation Appraximafe depth ro fust water encounrered in drilling Depth to Top of Seal 8' Surface Depth m Bottom of Seal 3' Depth m Top of Screen 5' Ptotective Cover: Type: None Length: Lock No. None Concre[e Sivface Seal: Yes No Grout Above Seal: Neat Cement Grout Benroaite Seal Other Nona Riser Pipe: Type PvC Diame[er 2" Total Length 7' SecCOns used 1 Couplings No Cap Yes X No _ Seal Material: Type Bemmnite cellets Amomt used (lb) Filter Materiel: Type Silica sand Amount used (16) 400 Screen: Type PVC Slot Size .030 Lengtlt 10' Diameter 2" Remazks: Temoorarv installadon Completed by: Depth m Botoom of Screen IS' Depth W Bottnm of Boring 15' Method of advance: HSA X Casing Tricone I.D. 4 1/4" I.D. O.D. sRauN=° INTERTEC f: \wpfilukm.cx%95\0722t0722.F01 MN Unique Well Numba NA Vapor Monitoring Well Field Data Sheet Dakota CounN Projxt Number CNLYX-95-0722 City/State EaAan. IvIIV umber VW-1 Well Location See sire man Dare of Iustallatlon 10-11-95 MR/GS Geologist RF )(+ 0.1') 2• Riser Pipe NA n (± 0.01'w/o cap) SurFace Elevation 821.1' mate depth W water nstatlaflon Drv matc depth [o er encountered ig None Top of Seai 4.8' Sottom of Sea1 7' Top of Sereea 10' Boanm of Seran ?A' Bottom of Boring 25' ,F advsnce: I.D. 4 1/a" I.D. O.D. Protecdve Cover: Type: _ Length: Lock No Concrete Surface Seal: Yes _ No X Grout Above Seal: Neat Cement Grout Senwuite Seal Benwnite erout Ofher Riur Pipe: Type PVC Diameter 2" Total Length 12' SecGOns uud 2 Couplings Cap Yes X No _ Seal Ma[erial: Type Bentnnire chios Amoun[ used (Ib) 25 Filter Material: Type Silica sand Amount used (16) 400 Screen: Type PVC Slo[ Size .010 Length 10' Diamerer 2" Remarks: 1 month instailation Campleted by: sRauN INTERTEC 's\95\0722W722.F01 Appendix B Laboratory Reports ., BRAu N,M I NTE RTEC October 27. 1995 6.auri lnteK« curporaeia, 6875 Wwhington Avenue Soud+ P.O. Box 39108 Minrreapolis. Minnesota 55439-0108 612-941-5600 Fax:942d844 Engineen and Scienfish Serving rhe 8ui1t ond Nah,rol Environmenh° Project CMBX-95-0722 Report 95-3282 Ms. Pat TerhaadNII-I Braun Intertec Corporation Re: Dakota County 1534 Lone Oak Road Bnun Intertec Corporation received your analytical request on October 16, 1995. Analytical resuits are summarized on the following laboratory report. Routine Braun Intertec Corporation QA/QC was followed. Quality control data have been reviewed. No anomalies were encountered in the analysis of this sample. We appreciate the opportunity to meet your analytical needs. ff you have any questions or need additional information, please call Barbaza Maki at 612-9424820. Sincerely, --s..%...?A .Nk?. Bazbaza J. Maki Project Manager Attactunents Chain of Custody Laboratory Results , . CGent: Dakota County Log-in: 95•7282 Project Number: CMBX-95-0722 Matrix: Air'Ihbc Lab Sample ID: 95-3282-01 C1feM 5ample ID/Description: Vent Well Labontory: Iab CootacNPhonc Sempler: % Moistum- 11II)L: RL: Bnun hartec Caryoration B. Malo/612-942-0820 Bnun martx Not AppGcable Mnhod DGec6on Limit Repoctm8 Livut nace smpka: 10/12/95 Date Recdred: I0/16/95 Date Reported: 1027195 Page: 1 Extnd F.xtnd Anal7ss Anatysia DWutlon Compoimd MeWod Date Method Date FaUor IrIDL RL Semplelteault Air AnalYSis - - NIOSH 10l17195 1 0.10 0.10 <0.10 ppm Acemne - - NIOSH 10/17195 1 0.07 0.07 <0.07 ppm Benzene • NIOSH 10/17195 1 0.05 0.05 <UAS PPm Buryl Cettosolve - - - NIOSH I0117195 1 0.04 0.04 <0.04 ppm Cellosolve Acemm - - NIOSH I0/17195 1 0.05 0.05 <0.05 ppm Ctilorobeozene - NIOSEI 10/17195 t 0.05 0.05 <0.03 ppm ? Chlomfocm - - • NIOSH I0l17195 1 0.12 0.12 <0.12 ppm Et6anol - - NIOSH 10/17195 1 0.06 0.06 <0.06 ppm Ethyl Acetaro - - NIOSH 10/17I95 1 0.05 0.05 <0.05 ppm Efiyl Benzene - NIOSH 10/17195 1 0.07 0.07 <0.07 ppm Iwbutanol - HIOSFI 10117/95 1 0.09 0.09 <0•09 PPm IsoProPant?l - NIOSH 10/17195 I 0.06 0.06 <0.06 ppm Methyl Ethyl Keeone - ' NIOSH 10l17/95 l 0.06 0.06 <0.06 ppm Met6yl Isoburyl Kerone - - NIOSH 10/17/95 1 0.06 0.06 <0.06 ppm Merhylem C6loride - - - NIOSH 10/17l95 1 0.05 0.05 <0.05 ppm Srymne Te[rechloroethylene - - NIOSH 10117195 t 1 0.03 007 0.03 07 0 <0.03 <0 07 ppm ppm TetrahydroCumn - • - NIOSH - NIOSH 10117I95 I0/17195 I 0.06 . 0.06 . <0.06 ppm Toluene Total Hydrocalbons as Gazoline - - NIOSH 10J17/95 1 1.4 1.4 <1.4 d <l ppm m Total Hydrocarbons as Mineral Spirics - - NIOSH 10/17N5 1 1.4 1.4 . pp Total Hydmculwns as Naphtha - - NIOSH I0117195 1 1 1.4 04 0 1.4 04 0 <I.4 <0.04 Qpm ppm l.l.l-Trichlomethane - - NIOSH ' NIOSH 10/17/95 10f17/95 I . 0.04 . 0.04 <0.04 ppm Trioliloroethyleae - - NIOSH 10117/95 1 0.26 0.26 <026 ppm Xylenes. Taul - (Eod of Report) Subsurface Investigation Rubbu Disposal Site 1534 Lone Oak Road Eagan, Minnesota Prepazed For Dakota County Project Number CMXX-95-0722 November 22, 1995 Braun In[ertec Corporadon ' J ? - ?J o ; 00 - 0&0 , -? DAKOTA COUNTY ENVIRONMENTAL MANAGEMENT DEPARTMENT 14955 GALAXIE AVENUE / J 3 I/ /- e) n e-. O1 Rr? March 15, 1996 Mr. Dale Wegleitner City of Eagan 3830 Pilot Knob Road Eagan, MN 55122 RE: Braun Intertec Study of the Lone Oak Road Disposal Site Dear Mr. Wegleitner: I BARRY C. SCHADE DIRECTOR (612) 891-7011 FAX(612)691-7031 APPLE VALLEY MINNESOTA 55124-8579 This letter is intended to bring you up to date on the investigation of the Lone Oak Road disposal site since my January 2 letter to you. As I mentioned in that letter, a study done by Braun Intertec Corporation indicated two immediate concerns: the high methane concentration in the vapor monitoring well and the high level of lead in the waste material itself. Methane production is due to a natural decomposition process carried out by bacteria when there is a lack of oxygen. This process requires a source of organic material that is easy to decompose. Since rubber waste does not easily decompose, it is not likely to be the source of the organic material that is producing methane. Regardless of the source, the presence of inethane gas is considered to be the most immediate concern. With an adequate supply of oxygen and an ignition source, methane gas at the level detected during the Braun sampling could result in an explosion if the methane gas were concentrated in an enclosed area. Therefore, our first concern is possible migration of the methane gas into homes and buildings where oxygen coupled with an ignition source could be present. We have taken the following steps to determine what is occurring in this area and ensure the safety of the residents: . We have checked for the presence of inethane gas in the basement of each home in the area at least once and, at the owners request, checked three homes a second time. No methane was detected on these occasions. . We had NSP do a fingerprint test on the methane gas detected in the vapor monitoring well, and NSP indicated that it was not natural gas from a leak in the gas distribution line. Pnnted on recycleC paper, 20%post-consumer `? AN EOUAL OPPOflTUNITV EMPLOYEH .. • We had probes installed at depths of about four feet and six feet next to the basement at 1534 Lone Oak Road, to test for methane near the house. We found no methane gas at these locations. We have contracted with Braun Intertec to continue the study of the site. In late February Braun personnel, accompanied by Environmental Management staff, installed additional probes in various locations on the disposal site to check for the presence and movement of inethane. The final results from these probes are not yet available, but we will contact you when we have them. However, we are continuing to find high levels of inethane gas in the area where the fill is deepest. As I indicated in my January 2 letter, we are also planning to sample surface soils from area yards and gardens in the spring. We will analyze those samples for the same metals, including lead, that were detected previously in the waste. I am enclosing a copy of the Braun Intertec Corporation report of its Fall 1995 study of the site and a summary of the report, prepared by Environmental Management staff. Since notices of claim have been filed with Dakota County regarding some of the properties in this area, please contact Jay Stassen of the Dakota County Attorney's Office at 438-4564, if you have questions on this site or the County's activities. Sincerely, Barry C. 5efiade, Director Environmental Management Enclosures o1swr/site/rebmrp3 N BRAUNINTERTEC REPORT RUBBER DISPOSAL SITE ON LONE OAK ROAD In October 1995, Dakota County contracted with Braun Intertec, an environmental consulting firm, to study the rubber disposal site on Lone Oak Road in the City of Eagan. The main objective of the Braun study was to evaluate the chemical characteristics of the waste, the ground water in the area and the gas in the waste. Terms Used in the Report: RCRA metals refer to eight specific heavy metals that are commonly found in industrial products and are tested for routinely to determine whether a waste has hazardous characteristics. TCIP analvsis refers to a laboratory method of dilution and extraction used to determine if particular chemicals are present and if they will move through the soil or waste. VOCs, Volatile Orqanic Compounds, are a class of compounds that are normally associated with industrial solvents and may be found in soil or ground water where improper handling or disposal has occurred. PAHs Polv Aromatic Hvdrocarbons, are a class of organic compounds that are normally formed during high temperature burning or heating of other organic compaunds. HRL, Health Risk_Limit, is a concentration limit set by the Minnesota Department of Health for a particular chemical that has been determined to be dangerous to heafth if ingested for a certain period of time. MCL Maximum Contaminant Level, is the federal standard set for the allowable contaminant level for public drinking water supplies. Total value refers to the entire amount of the chemical present in a sample, including sediment, compared to chemicals in solution that have been filtered or filtered and diluted, such as TCLP samples. Watertable is the upper layer of the first saturated (water bearing) sand or soil that is encountered when drilling. Dissolved Metals are metals in a water solution that cannot be removed by filtering. Often metals in solution are part of a compound or are attached to ? particles of silt or clay and will be removed when the water is filtered either naturally through sand, or with a commercial or laboratory filter. MDL, Minimum Detection Level, is the lowest concentration at which a chemical may be detected for the analytical procedure used. Chemicals may be present at a concentration that is less than the MDL. Jar Headsoace Procedure is a quick method used in the field for determining if VOCs are present in soil or waste as drilling is being done. PVC, Polv Vinvl Chloride, is a hard plastic commonly used in manufacturing pipe to be used for plumbing. VW-1 is the vapor well installed by Braun Intertec where samples of the waste were obtained and where a plastic perforated pipe was installed to sample methane and other gases that might have been present. PZ-1. PZ-2 and PZ-3 are the three temporary groundwater monitoring wells installed by Braun Intertec. PZ-3 was instalied on top of the hill and PZ-1 and PZ-2 were installed on the lower level of the property. Summary of Sampling and Analytical Results: Braun Intertec did borings to obtain ground water samples at three different locations on ihe site. They also used borings to obtain waste rubber samples at two depths, soii samples below the waste, and samples of the gas in the waste. Ground Water The water samples were taken with a fen foot pertorated PVC pipe section that was installed a few feet below the watertabie. The water samples contained various amounts of sand, silt and clay sediment. The ground water was found to be high in total metals before filtering but after filtering, most of the metals were below the MDL. The VOCs and PAHs found in the water were determined to be at levels below concern for health standards for drinking water. Rubber Waste and Soil The waste that was obtained through the boring was a mixture of soil and rubber pieces. Two samples were taken from the waste rubber for analysis: one at 10 feet and one at 20 feet. One sample was also taken of the soil below the waste, at about 25 feet. The samples of waste rubber tested high in a number of metals, especially lead, but the soil below the waste tested very low in metals. Vapor Monitoring A perforated PVC pipe installed into the waste to collect gas samples. The samples were analyzed for gases that were present, and methane was the major gas that was detected. The concentration of inethane was found to be about 16%. Braun Conclusions and Recommendations . Analysis of the waste indicated high concentrations of inetals, particularly barium and lead. . The high concentrations of total metals in the ground water are likeiy due to sediments and are not a reflection of groundwater quality. . The major environmental concern at this site is the presence of inethane in the subsurface. The levels of inethane are high and may present a significant risk to the safety of nearby residences ifi gas enters the dwelling or other confined spaces at explosive concentrations. The basements of the three residences closest to VW-1 should be monitored for methane and methane alarms should be installed. Also, vapor monitoring points should be installed next to the foundations of the houses. The potential sources of inethane should be investigated and additional studies should be performed to determine the extent of inethane and to evaluate potential corrective measures. The complete Braun Intertec Report is attached. swdletlokrebm BRAUNSM INTERTEC November 7, 1995 Ms. Pat Terhaar/MH Braun Intertec Corporation Re: Dakota County 1534 L,one Oak Road Broun IMartec CorporaNon 6875 Washingtan Avenue Saulh P.O. Box 39108 Minneopolis, Minnesoto 55439-0108 612•9415600 Fox:942,4844 Efgineers and Scienlisfs Serving Ke Built and NaNrol Fnvironmenn` Project CMXX-95-0722 Report 95-3233 Braun Intertec Corporation received your analytical request on October 11, 1995. Analytical results are summarized on the following laboratory report. Routine Braun Intertec Corporation QA/QC was followed. Qualiry control data have been reviewed. We appreciate the opportuniry to meet your analytical needs. If you have any questions or need additional information, please call Barbara Mald at 612-942-4820. Sincerely, kAd.L Bazbaza I. Maki Project Manager Attachments Chain of Custody Laboratory Results ClienC Log-in: 'Project Nwnber: Matrix: La6 Sample ID: i ! G7ient Sample ID I Dakoq Counry 95-3233 CMXX-95-0722 Solid 95-3233-0I rDescriptton Was[e Composia 10' a r , Le6oratory: Srauo Tnrerac Colporrfion Lab Confacf/Phoue: B. MakV612-442-4820 Sampler: Baun Ina`rec % MoLshae: Not Applicable MDL: Met6od Detecuon limit RL: ReporUng Limit Eztrad Extrad Analysis Anslysis Dilution ' Compound Met6od Date Method Date Faetor MDL RL Metals Arsenic, Total Harium, Total Cadmium, Total Chromium, Total ' Lead, Total Memury, ToFal - Selenium, Toral Silver, Total Microscopy Asbestas - - SW-8466010 30l20195 5 2 10 - - SW-8466010 10110195 5 1.0 5.0 - - SW-846 6010 30120I95 5 1 5 - - SW-846 6010 10/20l95 5 0.50 2.5 - - SW-846 6010 10/20l95 5 1.5 7.5 - - SW-846 7471 10/20195 1 0.01 0.01 - - SW-8466010 10l20/95 5 3.0 15 - - SW-846 7760 10! 19195 1 1.2 1.2 - - PI.M 10118195 t - - ga The mpotting limit (RL) was'sisM. A d0ution of the sample was rccesary due to ma¢iz intecfcmaces. tt No asbesros demc[ed. Date Sampled: 10f 11/95 11ate Received: 10111/95 Dau Reported: 11/07/95 Page: ( Sample Resuit u m8/k8 540 mg/kg 60 mglkg 16 mg/kg 1600 mg/kg ga ga Ba ga ga <0.01 mg/kg <IS mg/kg 1.2 mg/kg &a tt (Report condnued on nex[ page) Ctien[: Dakota Counry Log-in: 953233 Project Number: CMXX-95-0722 Matrix: Solid iah Sample ID: 95-3233-02 Client Sample IDlDescriptfoa Vent Well Rubber 20' Laboratory: Lab CaMacUPhone: Sampler. % Moisture: MDL: RL: Brnm Inceitec Co'potaaon B- MaYi/612•942-4820 Hwnn Inaxtx Not Applicable Metlrod Deradon Cimit Repoctlng f ii.e Date Sampled: 10f l t195 Date Recaved: 10111795 Date Reported: 11107/95 Page: 2 Compound Extract Extxsct Analysis Method Date Method Anal7ss Date DHution Factor MDL RL Sample Resuit lfetaLs To41 Arsenic - • SW-846 6010 1OC10/95 5 2 10 42 mg/kg ga . Barium Total • - SW-846 6010 IOI20/95 5 1.0 5.0 1600 mglkg ga , Cadmwm Total - - SW-846 6010 10120l95 5 ( 5 20 mg/kg ga , Total Chromium - - SW-846 6010 IOR0/95 5 0.50 2.5 25 mglkg ga , L,ead, Toral - • SW-846 6010 10/20/95 5 1.5 7.5 4400 mP?kB 8a tifercury Toql - - SW-846 7471 30l20/95 I D.DI OAl <0.01 mglkB . Total Selenium - • SW-846 6010 10l20N5 5 3.0 15 <15 mglkg ga , Silver,Total - • SW$467760 ID/I9/95 I 1.2 1.2 < 1.2 mg/kg Micrascopy • PLM I0118l95 1 - - _ tt Asbesros • ga The reporting limit (RL) was Iaiud. A diludon of the samPle was necessary due to matriz inreffaences. tt No asbes[os detected. (Repo¢ continucd on aext page) C6ent: Dakota Counry Laboramry: Braun intertcc Colpofavon Date Sampled: IOII l/95 Log•in: 953233 Lab CoNacf/Phom: H. Maki/612-942-4820 Date Aeceived: 10/I1l95 Project Num6er: CMXX-95-0722 , Sampler. Blaun Inte[tec Date Reported: 11/07195 ' Matrix: Solid % Moisture: Not Applicable Lab Sample ID: 953233-03 IoIDL: Method Decection Limit , RL: Reporting Limit I Client Sample IDJDescription: Ven[ Wcll 25' Page: 3 ? ExtraM Extrad Analysis Analysis Dilution ' Compotmd Method Date Method Date Fac[or NIDL RL Sample Result Volatile Organic Compounds Acemne SW-8465030 10116195 MDH466A 10l16/95 I 5.0 5.0 C5.0 mglkg Allyl Chloride SW846 5030 10116l95 MDH 466A 10116/95 t 0.1 0.1 <0.1 mglkg Benzene SW-846 5030 10/16195 MDH 466A 10/16/95 1 0.03 0.03 <0.03 mgfkg Bromobenzene SW-846 5030 I0/16/95 MDH 466A 101I6/95 1 0.1 0.1 <0.1 mglkg Bromochloromethane SW-8465030 10/16l95 MDH466A 10l16/95 1 0.1 01 <0.1 mg/kg Bromodichloromethane SW-8465030 I0116195 MDH466A 10l16/95 1 0.1 0.1 <0.1 mg/kg Bmmoform SW-846 5030 10/16l95 MDH 466A 10116/95 1 0.1 0.1 <0.1 mglkg Bromomethane SW-846 5030 10116195 MDH 466A 10I16195 I 0.1 0.1 <0.1 mg/kg n-Burylbenzene SW-846 5030 10116195 MDH 466A 10/16/95 1 0.1 0.1 <0.1 mg/kg sec-Burylbenzene SW-846 5030 10116195 MDH 466A 10116/95 1 0.1 0.1 [0.1 mglkg tcrt-Butylbenzene SW-846 5030 10116195 MDH 466A 101I6/95 t 0.1 0.1 <0.1 mglkg Car6on Tevachloride SW846 5030 I0116195 MDH 466A 10116195 1 01 01 <0.1 mglkg Chlorobenzene SW-846 5030 I0116195 MDH 466A 10116/95 t 0.1 01 <0.1 mglkg Chlorodibromomefhane SW-846 5030 I0/16195 MDH 466A 10116/95 ( 0.1 0.1 <0.1 mg/kg Chloroethane SW-8465030 I0116195 MDH46fiA 10116/95 t 0.1 0.1 <0.1 mglkg Chlorofortn $W-846 5030 10/16l95 MDH 466A 10116/95 1 0.1 0.1 <0.1 mg/kg Chlomme[hane SW-8465030 10116195 MDH466A 10l16195 1 0.5 0.5 <0.5 mg/kg 2-Chlorotolucne SW-846 5030 10/16195 MDH 466A 10/I6/95 1 0.1 0.1 <0.1 mg/kg 4-Chlomtoluene SW-846 5030 10/16195 MDH 466A 10116I95 i 0.1 0.1 <0.1 mgJkg 1,2-Dibromo-3Chloropropane SW-846 5030 10116195 hIDH 466A 10/16/95 1 1.0 1.0 C 1.0 mg/kg 1,2-Dibromcethane SW-846 5030 101I6195 MDH 466A 10/16/95 I 0.1 0.1 <0.1 mg/kg Di6romomethane SW-8465030 10/16195 MDH466A 10f16l95 1 0.5 0.5 G0.5 mg/kg 1,2-Dichlarobenzene SW-846 5030 10116/95 MDH 466A 10116/95 I 0.1 0.1 <0.1 mg/kg 1,3-Dichlarobenzene SW-846 5030 10/16195 MDH 466A 10116195 1 0.1 0.1 <0.1 mg/kg 1,4-Dichlombenzene SW-846 5030 10116195 MDH 466A 10116l95 1 0.1 0.1 <0.1 mg/kg 1,1-Dichloroctlwie SW-846 5030 10/16/95 MDH 466A 10116195 I 0.1 0.1 <01 mg/kg 1:-Dichloroefhane SW-846 5030 101I6195 MDH 466A 10116195 I 0.1 0.1 <0.1 mglkg l,l-Dichlorocthylene SW-846 5030 10l16195 MDH 466A 10l16195 1 0.1 0.1 <0.1 mglkg cis-1,2-Dichloroefhylene SW-846 5030 10116/95 MDH 466A 10116195 1 0.02 0.02 <0.02 mglkg trans-l,2-Dichlaroethylene SW-8465030 10116/95 MDH466A 10116195 1 0.02 0.02 <0.02 rog/kg Dichlorodifluommethane SW-846 5030 10116/95 MDH 466A 10116/95 1 0.1 0.1 <0.1 mglkg Dic6lomfluo`omethane SW-846 5030 10JI6145 MDH 466A 10116195 1 0.1 01 <0.1 mg/kg 7,2-Dichloropropane SW-8465030 I0116l95 MDH466A 10116/95 I 0.1 0.1 <0.1 mgfkg 1,3-Dichloropropane SW-8465030 10/16/95 MDH466A I0116/95 1 0.1 0.1 G0.1 mglkg 2,2-Dichlompmpane SW-8465030 10116195 MDH466A 10116195 1 0.1 0.1 <0.1 mg/kg I,1-Dichloro-l-pmpylcne SW-8465030 10l16l95 MDH466A 10/16/95 1 0.1 01 <D.I mglkg cis-1.3-Diclilom-l-propylene SW-8465030 I0f16l95 MDH466A- 10/16/95 1 0.1 0.1 <0.1 mg/kg trzns-1,3-1)ichloro-I-propylene SW-8465030 10I1605 MIDH466A I0116/95 1 0.1 0.1 C0.1 mg/kg EthylBenzenre SW-8465030 10116l95 MDH466A 10116195 [ 0.03 0.03 C0.03 mg/lcg EfhylEther SW-8465030 30116/95 MDH466A I0/16I95 I 0.1 0.1 <0.1 mg/kg Heuchloroburadiene SW-8465030 10116195 MDH466A 10l16/95 1 0.1 0.1 <0.1 mg/kg (Report continued an next page) Client: Dakota Counry Log•in: 95-3233 Project Number: CMXX-95-0722 Matrix: Solid Lab Sample ID: 45-3233A3 Client Sample ID/Description: Vent We1125' Labocatory: Lab ContactlPhone: Sampler: 9o Moisture: MDL: RL: Braun Inmrtec Cofporation B. Makil612-942-0820 Bmun Incemc No[ Applicable Mettwd Detecdon Umit Repotting Limit Faclnct Extnct Amlysis Amlysis Dilution Compomd Method IYate Metlad Date Fador NIDL Date Sampled: 10111/95 Date Recrived: 10111/95 Date Reported: 11107/95 Page: 4 RL Sample Result Isapropylbenzene SW-846 5030 10l16195 MDH 466A 10/16195 lwpropylwluene SW-846 5030 10/16195 MDH 466A 10116195 Methyl Ethyl Ketone SW-846 5030 10/16195 MDH 466A 10116/95 Nlethyl Isoburyl Kerono SW-846 5030 10/16195 MDH 466A 101I6195 Me[hyl Teniary Butyl Ether SW-846 5030 10l16/95 MDH 466A 10/16/95 Methylene Cliloride SW-846 5030 10/16195 MDH 466A 10116/95 Naphthalene SW-8465030 10/16/95 MDH466A 10/16195 n-Propylbenzene SW-846 5030 10116/95 MDH 466A 10116/95 Sryrene SW-8465030 10116/95 MDH466A 10/16l95 1.1,1,2-Tetrachiomethane SW-8465030 IO/16/95 MDH466A 10l16/95 1,1,2,2-Tetrachloroethane SW-8465030 10116l95 MDH466A 10/16195 Tevachloroethylene SW-8465030 I0/16l95 MDH466A 10116/95 Tetmhydrofuan SW-8465030 10116195 MDH466A 10116195 Toluene SN-846 5030 lO/I W95 MDH 466A I0116l95 1.2.3-Trichlorobenzene SW-846 5030 10/16195 MDH 466A 10116l95 1,2.4-Trichlomhenzene SW-946 5030 I01I6195 MDH 466A I0/16195 l.l.l•Trichloraefiane SW846 5030 101I6195 hIDH 466A 10/16/95 1,1,2-Trichloroethane SW-846 5030 10116195 MDK 466A 10116/95 1,1,2-Trichioroethylene SW-846 5030 10116195 MDH 466A 10116195 1'richlorofluoromethane SW-846 5030 I0116195 MDH 466A 30116195 1.2,3-Trichlompropane SW-846 5030 10/16/95 MDH 466A 101I6195 Trichlomtrifluoroethane SW-8465030 10116195 MDH466A 10l16195 1.2,4•Trimethylbenzene SW-8465030 10l16l95 MDH4b6A 10f16l95 1,3,5-Trimethylbenzene SW4465030 10116195 MDH466A 10l16/95 Vinyl Chloride SW-846 5030 I0116195 MDH 466A I0116l95 m,p-Xylene 9W-846 5030 10116/95 MDH 466A 10/16l95 o-Xylcne SW-846 5030 10116/95 MDH 466A 10/16195 Polyaromatic Hydrocarboas (PAAs) (GC/MS) pcenaphthene SW-846 3540 10112195 SW-846 8270 10/17/95 Acenaphthylene SW-8463540 10l12195 SW-8468270 10117195 pndaracerve SW-8463540 10112195 SW-8468270 10117795 Benzo(a)anth'acene SW-846 3540 10/12/95 SW-846 8270 10117l95 Benzo(6)Fluoranthene SW-846 3540 10l12l95 SW-846 8270 10117/95 Senza(k)fluoranthene SW-846 3540 10112195 SW-846 8270 10117195 Benzo(g,h,i)pcrylene SW-846 3540 10/12195 SW-8468270 10/17195 Benzo(a)pyrene SW-8463540 I0/12195 SW-8468270 10117195 Chrysene SW-846 3540 10/12195 SW$46 8270 10117195 Dibenzo(a.h)anthrzcene SW-846 3540 10/12195 SK'-846 8270 10I17/95 piberu&ofurart SW4463540 10/12/95 SW-8468270 10117l95 Fluoranthene SW-846 3540 10l12l95 SW-846 8270 10/17l95 Fluorene SW-8463540 10/17195 SW-8468270 10117195 Indeno(1,2,3-cd)pyrene SW-846 3540 10112/95 SW-846 8270 10117195 1 0.1 0.1 G0.1 mg/kg . t 0.1 0.1 <0.1 mg/kg I 0.5 0.5 <0.5 mg/kg i 0.1 0.1 <o.t mstka 1 0.1 0.1 <0.1 mg/k6 1 1.0 1.0 < 1.0 tng/kg I 0.1 0.1 <0.1 mg/kg 1 0.1 0.1 <0.1 mg/kg 1 0.1 0.1 <0.1 mg/kg 1 0.1 0.1 <0.1 mg/kg 1 0.1 0.1 <0.1 mgfkg 1 0.1 0.1 <0.1 mglkg I 0.5 0.5 <0.5 mglkg 1 0.03 0.03 <0.03 mglkg 1 0.1 0.1 <0.1 mglkg l 0.1 0.1 <O.l mglkg 1 0.1 0.1 <0.1 mg/kg 1 0.1 0.1 <0.1 mg/kg I 0.05 0.05 <0.05 mg/kg 1 0.3 0.1 <0.1 mglk8 1 0.1 0.1 <0.1 mg/kg 1 0.1 0.1 <0.1 mg/kg 1 0.1 0.1 <0.1 mg/kg 1 0.1 0.1 <0.1 mglkg t 0.1 0.1 <0.1 mglkg 1 0.03 0.03 <0.03 mg/kg 1 0.03 0.03 <0.03 mglkg 1 033 033 <0.33 mglkB 1 0.33 033 <033 mg/kB 1 0.33 0.33 <0.33 mg/k8 1 0.33 033 <033 mglkg 1 0.33 0.33 <0.33 mg/kS 1 033 0.33 <0.33 mglkB 1 0.33 0.33 <033 mglkg t 033 033 <033 mglkg 1 0.33 033 <033 mglkg 1 033 0.33 <0.33 mgf1t8 1 033 0.33 <0.33 mg/k8 I 033 033 <0.33 mg/k& 1 033 033 <0.33 mglkg 1 0.33 033 <0.33 tnglkg (Report condnued on nextpage) ? s Client Dakota Counry j'0g"°: 95,3233 Project Number: CMXX-95-0722 La6ora'or9- Braun Inamc Cotpontion 1ab Contact/py ? ti''x: Solid Me B. Mati/612A42?g20 ? : O1plu': Lab Sample ID: 95-3233-03 BrauU ?? % Moisture; ?? Not Applicabte RL: Mediod Detation Limit Cliept Sample ID/p¢sc i Repommg Limit r ption: Vrn t Well 25• Compound Extract Method Zaract Amly"s Anai7$1s Dilartion Date Method Date Factor hIDL gy 2-Methy?naphthalene NaphNalene Phenanthrene Sw'-$463540 SW-846 3540 10/12195 SR+-846 8270 10117/95 ( 0 33 10/12/95 0 Pyrene SW-846 3540 . SW-846 8270 10117/95 - 1" 0.33 30/12195 SW.gqb 8270 .33 033 SW-846 3540 10/17/95 10/12/95 SW-946 8270 10117/95 i 0.33 0.33 "`* Semi-Volauk Su?mgares 0.33 0.33 2-Fiuorobiphenyl Nitrobenzene-d5 Terphenyldl4 SH'-8463540 SW-846 3540 10/12/95 SW-8468270 10/17/95 1 SW- 8463540 30/12195 SW-$q6 8270 10/17195 1 10q2/95 SW-846 8270 Netals 10/I7/95 f 4rsemc, Toral 3arium, Tota1 :admium Total ' - SW-8466010 10/20/95 1 Z , 'h mmium, Totai - SW-gq65p10 10119195 1 1.0 - SW-Sp66010 10 xad, Totaf _ I0119195 1 1 • SW-846 6010 10119195 I [ereury Tolal 1 0.50 " ?'-846 6010 10/19/95 1 1 5 0.50 . :lenium, Topl Iver, Totai ' . ' SN'-546 7471 10120/95 1 0 01 1.5 - . ' SW-8466010 30l19/95 I 0.01 - sw-sa5 n6o tai9ros i i i .i .z Date SamNed: 10111195 Dnte ReceiveA; 10/11/95 Datc Reported: 11/07/95 Page: 5 SsmP1e Result <0.33 mg/kg <033 mg/kg C033 mg/yg <0.33 mg/kg n $o % rec 88 R ? 6 mg/kg 24 mg/kg <1 m8tk8 6.8 mg/kg < 1.5 mg/kg <o.oi ,,,glkg <3.0 mg/kg <1.2 mg/kg (Reporc condnued oa next page) •Cl+ent: Dakota County Lag'in: 95-3233 P Labontory: I,eb CoNacf/pp Bnun Intatec Corpom ?n B Date Sampled: 10111195 roject Number: CMXXA5-0722 une: . Maki/612-942-0820 Samplq: B Da4 Received: 1011 V95 Matrix: Liquid I,ab Ssmple m: 95-3233-04 % Moisture: ? ??? No[ Applicable Date Repor[ed; 11/07195 MDL: Mcfiod Derection Limit RL: Repotting Limit Ctim[ Sample ID/Descriptton: py_i Page: 6 Compomd C Extrad Aml9sis Analy?s D?utiou Method Date Method Date Factor lYIDL RL Sample Resuk Volatile Organic Compounds Acetnne Allyi Chloride SW-8465030 10/17/95 MDH465E 10/17/95 1 50 50 <50 8enzene SW-846 5030 10/17195 MDH 465E SW-846 5030 10 10117195 I 1.0 1.0 < 1.0 ugq ug/I Bromobenzene 117195 MDH 465E SN-8465030 10117/95 MDH465E 10117/95 1 0 1.0 1.0 <1.0 ug/f Bromochloromethane SW-8465030 I0/17/95 MDH465E 1 /17/95 I 10/17195 1 1.0 lA <I.0 ugfl LO 1.0 <1.0 ug/I Bmmodichloromerhane Bromofortn SW-846 5030 10/17/95 bIDH 465E 10117/95 1 03 03 Bromomethane SW-8465030 10/17l95 MDH465E 10/17/95 1 0.5 0 5 <0.3 <0 5 ug/I n-8urylbenzene SW-946 5030 SW-8465030 10/17N5 7rIDH 465E 10/17195 1 3.0 . 5.0 . <5.0 ug/! ug/1 sec-Burylbenzene SW-846 5030 10/17/95 MDHA65E 10117/93 MDH 465E 10/17/95 I 10117/95 1.0 1.0 <1.0 ug/I 1 1.0 1.0 <1.0 ug/1 ten-Burylbenzene Carbon Tetrachlorid SW-8465030 10/17195 MDH465E 10/17195 1 1 0 1 0 e Chlorobenzene SlV-846 5030 10/17/95 MDH 465E 30117195 I . 1.7 . 1 7 <1.0 <l 7 ug/1 Chlorodibromometharie SW-8465030 SW-8465030 10/17/95 MDH465E 1 10/17/95 I 1.0 . 1.0 . C1.0 ug/1 ug/1 Chlomethane SW84650.30 0/17195 MDH465E 10117/95 MDH465E 10117/95 1 2.5 2.5 <2.5 ug/I 10117195 1 1.0 1.0 <1.0 ug/1 Chlaroform Chloromethane SW-8q65030 10/I7/95 MDH465E I0/I7195 1 1 5 LS 2-Chtorotoluene SW-846 5030 SN 8 I0l17195 hIDH 465E 10/17/95 1 . 5.0 5.0 <1.5 <5 0 ug/I u A 4-Clilorotofuene - 465030 SW-846 5030 I0117195 MDA465E 10 10/17/95 I 1.0 1.0 . <1.0 g ugA 1.2-Dibromo-3-Chlo`opmpane SW-8465030 /17/95 MDH 465E 10/17195 MDH465E 10/17195 I 1.0 1.0 <1.0 ug/1 10/17/95 I (p 10 < l0 ug/I 1,2-Di6romcethane Dibromomethane SW-$46 5030 10117l95 MDH 465E 10/17/95 1 0 2 0 2 1,2-0ichlorobenzene SW-846 5030 SW846 10/17/95 MDH 465E I0/17195 1 . 5.0 . 5.0 <0.2 <5 0 ug/I u /1 1,3-DicWorobenzene 5030 SW 84 10/17/95 MDH465E I0/17/95 I 0.2 0.2 . <02 g ugfl 1,4Dich1oro6enzene - 65030 SW-8465030 10117/95 MDH465E 0 10/17N5 1 LS 1.5 <1.5 ugfl 1 /17/95 MDH465E 10117795 1 0.2 0.2 <0.2 ug/1 l,l-Dichloroethane 1?-Dichloroethane SW-8465030 SW 8 6 10/17/95 MDH465E 10/17195 1 1.0 I.0 <1 0 ug/f l.l-Dicliloroethylene - q 5030 SW-8465030 10/17195 MDH465E 10/I7/95 1 0.3 03 . <03 ugfl cis-i,2-Dichioroethylene SW-846 5030 30/17/95 MDH465E 10/17195 MDH 465E I0/17I95 I 0 1.0 1.0 <I.0 ug/I crzns-1,2-Dichloroefhylene SW-846 5030 10/I7I95 MDH 465E 1 /17/95 1 10/I7195 02 01 <01 ug/I 1 0.2 0.2 <0.2 ug/1 Dichlorodifluoromethane DichlomFluommethane SW-8455030 10/17195 MDH465E 10/I7/95 I 5.0 5 0 <5 0 1,2-Dichloropropane SW-8465030 SW-8465030 I0/17195 MDH465E 10/17/95 I 5.0 . 5.0 . <5.0 ug/1 ugft t,3-Dichloropropane SW8465030 10/17/95 MDH465E lOIUl95 MDH465E 10/I7195 ( 1.0 1.0 <1.0 ug/l 2,?-Dichloropropane SW-8465030 10/17/95 MDH465E 10117195 1 I0l17l95 I lA 1.0 <1.0 ag/l 1.0 1.0 <1.0 ug/! 1.1-Dichlolo-I-propylene cis•!,3-Dichloro-l-propyfene SW-gq( 5030 SW 10/17/95 MDH 463E 10117195 I 0.5 0,5 <0 5 u A ttans-l,3-Dichloro-l-propylene -8465030 SW$465030 10/17J95 MDH465E 10/17/95 10/17/95 1 0.5 0.5 . <0.5 g ug/1 Ethyl 8enzene EthylEther SW-846 5030 MDH465E 10/17/95 MDH 465E 10117195 1 10/17/95 ( 0.5 1 0 0.5 1 0 <115 ug/1 SW-8455030 10/17/95 MDH465E 10117/95 1 . IA . LO <1.0 <1.0 ug/I ug/1 Hezachlarobutadiene SW-8465030 1 0117/95 MDH465E 10/17/95 1 1 0 . 1.0 <1.0 ug/1 r i (Repott coawiuW on nex[ page) CGent: Dakora Counry Log-in: 953233 Roject Numben CMXX-95-0722 Matrix: Liquid Lab Sample m: 95-3233-04 r ? Client Sample ID/Description: PZ-1 Labontory: Baun Intenec Co[pofation Inb Coofact/Phoae: B. Malti/612-942-0820 Sampler: Braua Inrertec %Moisture: NocApplicable hIDL: Method Detecuon Limit ItI.: Repo[ting Limit Date Sampled: 10111/95 Date ReceivM: 10/11/95 Date Reported: 11/07195 age; 7 ExtnM Exfract Analysk Analysia Dilirtion Compomd Method Date Method Date Factor MDL RL Sample Result Isopropyibenzene SW-8465030 10/17/95 MDH465E 10l17/95 1 1.0 1.0 <1.0 ug/I Itopropylmluene SW-8465030 30/17I95 bmH465E I0137l95 _ 1- 1.0 1.0 <I.0 ug/I Methyl Ethyl Ketone SW-846 5030 10117/95 MDH 465E 30/17/95 1 5.0 5.0 <5.0 ug/I Mechyl Iwburyl Kewne SW-846 5030 10/17/95 MDH 465E 10/17/95 1 5.0 5.0 <5.0 ugll Methyl Tertiacy Buryl Ether SW-8465030 10/17/95 ivIDH 465E 10117195 1 1.0 1.0 <1.0 ug/1 Mechylene Chloride SW-846 5030 10l17/95 MDH 465E 30/17/95 I 5.0 5.0 <5.0 ug/I Naphthalene SW-846 5030 10117/95 MDH 465E 10/17195 1 1.0 1.0 <1.0 ug/l n-Propylbenzene SW-84b5030 10l17/95 MDH465E 10l17195 1 1.0 1.0 <1.0 ug/1 Styrene SW-8465030 I0/17/95 MDH465E 10/17l95 1 1.0 1.0 <1.0 ugll 1,1,1,2•Tevachloroefhane SW-846 5030 10117/95 MDH 465E 10/17/95 1 0.5 0.5 <0.5 ugll 1,1,2,2-Tevachlaroethane SW-8465030 10117l95 MDH465E 10117195 1 1.2 1.2 <12 ug/I Tecrachloroethylene SW-8465030 10/17195 MDH465E 10/17195 1 1.0 1.0 <1.0 ug/I Termhydmfucau SW-846 5030 10/I7/95 MDH 465E I0/17/95 1 5.0 5.0 <5.0 ug/l Toluene SW-846 5030 10/17I95 MDH 465E 10117/95 1 1.0 1.0 <1.0 ug/I 1=,3-Trichlorobenzene SW-Sdb 5030 10/17195 MDH 465E 10/17/95 1 1.0 1.0 < 1.0 ug/1 1;2,4-Trichlorobenzene SW5465030 I0/17195 MDH465E 10l17/95 1 1.0 1.0 <1.0 ug/1 1,1,1-'frichloroethane SW-8465030 10/17195 MDH465E 10/17/95 1 2.0 2.0 <2.0 ug/I 1,1,2-Trichloroethane SW-8465030 10/17l95 MDA465E 10/17/95 I 1.2 1.2 <1.2 ugfl 1,1,2-Trichloroethylene SW-846 5030 10l17195 MDH 465E 10/17l95 1 0.5 0.5 <0.5 ugll TrichlomFluoromeUune SW-846 5030 10/I7195 MDH 465E 10/17l95 1 1.0 1.0 <1.0 ug/1 1:2,3-TricNloropropane SW-8465030 10/17l95 MDH465E 10117195 1 1.0 1.0 <1.0 ug/I Trichlarotrifluoroethane SW-8465030 10l17/95 MDH465E 10l17195 I 5.0 5.0 <5.0 ugll " 1,2,4-TrimerAylbenzene SW-846 5030 10117195 MDH 465E 10117/95 I 1.0 1.0 <I.0 ug/t 1,3,5•Trimethylbenzene SW5465030 10/I7/95 MDH465E 10l17/95 1 1.0 1.0 <I.0 ug/1 VinylChloride SW-8465030 10l17/95 MDH465E I0117195 1 1.0 1.0 <I.0 ug/1 m,p-Xylene SW-8465030 10117/95 MDH465E 10117/95 I 1.0 1.0 <1.0 ug/I o-Xylene SW-8465030 10/17/95 MDA465E 10/17/95 1 1.0 1.0 <1.0 ug/I HPLC Analysis Acenaphthalene EPA6t0 10/25l95 EPA610 I3102195 1 Ll 1.1 <1.1 ug/l Acenaph[hene EPA 610 10/25/95 EPA 610 11102/95 1 2.0 2.0 <2.0 ugfl Anthracene EPA 610 10/25/95 fiPA 610 11/02/95 I 4.0 4.0 <4.0 ug/1 Benzo(a)anthracem EPA 610 10/25195 EPA 610 11102195 1 030 0.30 <030 ug/1 Bcnzo(b)fluoranthene EPA 610 10/25/95 EPA 610 I1/02195 1 0.14 0.14 <0.14 ug/l Benzo(k)fluacanthene EPA 610 10/25l95 EPA 610 1 l/02/95 1 0.01 0.01 <0.01 ug/1 Henza(g,h,i)perylene EPA 610 10/25/95 EPA 610 I1107J95 1 0.19 0.19 <0.19 ugll Benza(a)py`ene EPA 610 I025195 EPA 610 11/02195 1 0.10 0.10 <0.10 ug/1 Chry:ene EPA 610 10125/95 EPA 610 11/02/95 1 2.0 2.0 <2.0 ug/1 Dibenzo(a,h)anthmcrne EPA 610 1025I95 EPA 610 11/02/95 t 0.10 0.10 <0.10 ug/l Fiuoranthene EPA 610 10/25l95 EPA 610 11/02I95 I 0.30 0.30 <030 ugll Fluattne EPA 610 I0l25195 EPA 610 I l/02l95 I 0.10 0.10 <0.10 ug/1 Ldeno(1,2,3rd)pymne EPA 610 10/25l95 EPA 610 11J02/95 1 0.14 0.14 <0.14 ug/1 I-Methylnaphthalene EPA 630 10/25195 EPA 610 11/02/95 1 5.0 5.0 <5.0 ug/1 (Repott coetinued on nezt pagc) Laboratorq: Braun Inmrtec Colpocatio¢ ClieM: Counry Dakota I,ab CmtactlPhone: B. Maki/612-942-0520 yog_in; Project Number. 95-3233 CMXX-95-0722 SamplU , : iR M Bmun Inrocuc Not App4ca61e Matrix: Liquid o ure % MDL: MefLad Detecuon Limi[ Lab Sample ID: 95•3233-04 RL; gepocting L'vnit Cllenl Sample IDlDescriptlon: PZ•t Extract Extxact Anal9sis Anal7sis Ddutian tor F MDL RI' Sam p le Result Compoimd Method Date Method ac Date EPA 610 10Y25195 EPA 610 11/02l95 1 _ 5.0 3 1 5.0 13 <5.0 < l.3 ug/l ugll ?-methytnaphthalene EPA 610 10/25195 EPA 610 11l02/95 1- . 12 12 c12 ug/l Yeph?alene EPA 610 10125195 EPA 610 11l02I95 1 1 ? 40 ?'? ?0'? ug/I Phenantlireae EPA 610 I0125195 EPA 610 I1102195 . Pyrene Remarks: 'ILis sample was exuacted past the EPA rccommended holding time. iaorganic EpA 310.113 10117195 4 10 10 qy mgll Alkaliniry, Toral EpA 375.4 I0I17195 1 10 40 0 0.40 1.4 m64 Sulfa¢ EPA 3761 10118/95 I . Sulfidc, Topl Nutrient gpp 3501 l0l19I95 1 091 0.01 02 0 0.03 I11 IDSfi mg/1 Ni[mgen. Ammonia EPA 353.2 10l12195 I 0.02 . 4itrogen, Nitra[e 1letals ' gpp 200.7 - 10117195 5 50 200 10 430 1400 ugft ugll Arsenic, Total - ' EPA 200.7 10lI6195 1 10 10 10 <10 ugll Banum. To?al EPA 200J t0l16195 1 10 10 360 ug/1 Cadmium. To?1 EPA 20U .7 10/16/95 1 0 1 5 0 I500 mgEqn Chromium. Taml • - SM 2340B 10/19195 S . . Hardness. Calcium 30 30 120 uB« EPA 200.7 10116/95 1 1 0 2 0.2 1.6 uSn Lead. Total gpp 245.1 IOl20195 . 200 200 17000 ug/i Melcury. Total _ EPA 200.7 10/17195 1 50 50 <50 gll u Potassium. Total Epp 200,7 101I6195 1 20 ? 20 ug/l Selenium. Total gpp 200,7 10116/95 1 20 $ilver. Toml EPA 200.7 I0!17195 l 3? 3? 27ppp ugll $odium, Toral . MetaLs - _ EPA 200.7 10/12J95 1 i0 50 t0 <50 qq ugll ugll pxsenic, Dissolved EPA200.7 10112/95 1 10 <10 ug/l Banum,Diswlved EPA 200.7 10/12195 1 10 12 <12 ugA Cadmium, Dissolved - - EPA 20D•7 10f 12l95 1 12 30 <30 ugll Chromium, Total Dissolved EPA 200.7 10/12195 1 30 Lead, Dissolved I 2 0 0.2 0.5 ?8?? EPA 245.1 10124/95 . S0 50 <50 ug/I Mc`cury. Dissolved EPA 200•7 10A2195 1 to G 10 ugll Selenium. Dissolved _ EpA200.7 10l12195 I 10 Silver, DissolveA Date Sampled: 10/11/95 Date Received: 10111195 Date Reported: 11/07l95 Page: 8 3 i gb ? I' ? , i Ba { gb ga 'Che rcporting lunit (RL) was raised. A diluuon of ihe sample was naessary hiah concen[cauons of tlti s analY[e. gy The reporting limit (RL) was raiscd. A dilunon of the sample was nceessary due to g (RepoR continued oa next page) • • Clienh Dakota Counry Iabontory: Braun Inmrta Colpornrion Date Sampled: 10/11195 Log•in: 95-3233 Lab ContscUPhone: B. MakV612-942-4820 Date Received: 10f11/95 , Rajec[ Nwnber. CMXX-95-0722 Sampler: Bmm Inromx Date Reported: l ll07l95 Matrix: Liquid % Moisture: Not Applinble Iab Sample ID: 95-3233-05 MDL: Method Dettcuon Limi[ RL: Repotting [.imit i ? Ctient Sample ID/Description: PZ-2 Page: 9 ExtraM ExtraR Analysir Analysis DilWion Compound Method Date Method Date FaMOr MOL RL Sample Result Volatile Organic Campoimds - Acewne SW-846 5030 10/17l95 hIDH 465E 10/17l95 1 50 50 <50 ug/I Allyl CNoride SW-846 5030 I0117195 MDH 465E 10/17l95 1 1.0 1.0 <1.0 ug/l Benzene SW-846 5030 10117/95 MDH 465& 10117195 1 1.0 1.0 <1.0 ug/I ' Bmmobenzene SW-8465030 I0/17/95 MDH465E 10117l95 I IA LO <I.0 ug/1 Bmmochlommethane SW-846 5030 10117l95 bIDH 465E 10/17195 1 1.0 1.0 <I.0 ug/1 ' Bromodichloromethane SW-8465030 10/17/95 MDH465E 10/17195 I 0.3 03 1.5 ug/l? Bmmofalm SW-846 5030 10/17/95 MDH 46SE I0/17/95 1 0.5 0.5 <0.5 ug/l BromameLAane SW-846 5030 10/17195 MDH 465E 10/17195 1 5.0 5.0 <5.0 ug/1 n-Burytbcnzene SW-846 5030 10117195 MDH 465E 10/17195 1 1.0 1.0 <1.0 ug/I scc-Burylbenzene SW-8465030 I0/17/95 MDH465E 10117/95 1 LO 1.0 <1.0 ug/I tcn-Burylbenzene SW-8465030 10l17l95 MDH465E 10/17l95 I 1.0 1.0 <LO ug/l Carbon Tetachloride SW-846 5030 I0117/95 MDH 465E 10/17195 1 1.7 1.7 <1.7 ug/I Chlorobenzene SW-8465030 10117l95 MDH465E I0/17l95 1 1.0 1.0 <1.0 ug/l Clilomdibromomethane SW-8465030 I0/17195 MDH465E 10117195 1 2.5 2.5 <2.5 ugll Chioroethane SW-8465030 10117/95 MDH465E I0/17195 1 1.0 1.0 <1.0 ugll Chlomfotm SR'-846 5030 I0/17/95 MDH 465E 10/17195 l 1.5 1.5 5.3 ugll ? Chloromethane SW-8465030 10137/95 MDH465E 10/17195 1 5.0 5.0 <5.0 ug/I 2-Chlomtoluene SW-846 5030 10117l95 MDH 465E 10/17195 1 1.0 1.0 <1.0 ug/I 4-Chlorotoluene SW-8465030 I0l17195 MDH465E 10/17195 1 1.0 1.0 <1.0 ug/I 1,2-Dibmmo-3-Chlompropane SW-846 5030 10/17195 MDH 465E 101I7195 1 10 10 <10 ugll I:-Dibmmoethane SW-846 5030 10117195 MDH 465E 10/17195 1 0.2 0.2 <0.2 ug/I Dib'omometfwne SW-8465030 10/17l95 MDH465E 10117195 I 5.0 5.0 <5.0 ug/1 1,2-Dichlorobenzene SW-846 5030 10l17/95 MDH 465E 10117195 I 0.2 0.2 <0.2 ug/l 1,3-Dichlorobenzene SW-846 5030 10/17195 MDH 465E 10/17195 I 1.5 1.5 < 1.5 ug/1 1,5•Dichlombenzene SW-8465030 10117/95 MDH465E 10117195 1 0.2 0.2 <0.2 ug/l 1,1-Dichlometliane SW-8465030 I0l17195 MDH465E 10/17l95 I 1.0 1.0 <1.0 ug/! 1.2-DichlomeNanc SW-846 5030 I0117J95 MDH 465fi 10l17/95 I 03 03 <0.3 ug/I 1,1-Dichloroethyleoe SW-8465030 I0/17/95 MDH465E I0/17/95 I 1.0 1.0 <1.0 ug/t cis-1,2-Dichloroefhy(ene SW-846 5030 10/17195 MDH 465E 10/17/95 t 0.2 0.2 <0.2 ugll aans•1,2•Dichloroethyleae SW-8465030 I0117195 MDH465E 10117195 1 0.2 0.2 <0.2 ugll Dichlorodifluoromethane SW-846 5030 10/17/95 MDH 465E 10/17/95 I 5.0 SA <5.0 ug/1 Dichlorofluoromethane SW-8465030 10117195 MDH465E 10117/95 1 5.0 5.0 <S.D ug/l ' 42-DicWolopropane SW-8465030 10/17195 MDH465E 10117l95 l 1.0 1.0 <1.0 ug/l 1,3-Dichlompropane SW-8465030 10117/95 hIDH465E 10/17/95 1 1.0 1.0 <1.0 ugll 2,2-Dichlompropane SW-846 5030 10117l95 MDH 465E 10117195 1 1.0 1.0 <1.0 ug/1 l,l-Dichloro-l-propytene SW-8465030 10/17/95 hIDH465& 10l17195 1 0.5 0.5 <0.5 ug/I cis-1,3-Dichloro-1•propylene SW-8465030 10117/95 MDH465E 10/17195 1 0.5 0.5 <0.5 ugll ttans•1,3-Dichloro-1-propylene SW-8465030 10/17/93 MDH465E I0117l95 1 0.5 0.5 <0.5 ug/I Ethyl Benzene SW-846 5030 10/17/95 MDH 465E I0/17l95 1 1.0 1.0 <1.0 ugll EthYl Edier SW-846 5030 10/17/95 IvIDH 465E 10/17l95 1 1.0 1.0 <1.0 ug/1 Hexachlombutadiene SW-8465030 10117/95 MDH465E I0117l95 1 1.0 1.0 <1.0 ug/l (Report continued on nezt pagc) C6ent: Dakon Counry I.aborntory: Bmw inrcrtec Colponrian Date Sampled: 10/11/95 Log-ia: 95-3233 I.ab CantacUP6one: B. Maki/612A424820 Date Re¢eived: 101I1/95 Project Nmber: CMXX-95-0722 Sampler: 8nuo intertec Date Reported: 11/07/95 Malrix: Liquid R Moistum: NatApplicable Lab Sample ID: 95-3233-05 DDL: Method Dettctioe Limit ; i RL: Repo[ring Limit ' Climt Sample IDlDescription: PZ-2 Page: 10 Extnd Extnct Analysis Annlyas Wudon Compound Met6od Date Method Date Fador MDL RL Sample Result Isopropylbenzene SW-8465030 10/17/95 MDH465E 30/17l95 1- 1.0 1.0 <1.D ug/l Isopropylroluene SW-8465030 10/17I95 MDH465E 10l17/95 1- 1.0 1.0 U.D ugA Methyl Ethyl Ketone SW-846 5030 10/17l95 MDH 465E 10l17/95 1 5.0 5.0 <5.0 ug/1 Mc[hyl Iso6uryl Ketone SW-846 5030 10117195 MDH 465E I0117/95 1 5.0 5.0 <5.0 ug/I Methyl Temary Buryl Ether SW-846 5030 10117/95 IvOJH 465E 10/17/95 1 LO 1.0 <I.0 ug/l Methylcne Chloride SW-846 5030 10/17l95 MDH 465E 30/17/95 I 5.0 5.0 <5.0 ugll Naphthalene SW-8465030 10/17l95 MDH465E 10/17/95 I 1.0 1.0 <1.D ug/I n-Propylbenzene SW-846 5030 10/17/95 MDH 465E 10117J95 1 1.0 1.0 <1.0 ug/l Sryrene SW-846 5030 I0117/95 MDH 465E 10/17N5 1 LO 1.0 <1.0 ugA 1.1,1,2-Tetrachloroethane SW-8465030 10117/95 MDH4656 10117195 1 0.5 0.5 <0.5 ug/1 1,1,2,2-Temchloroefhane SW-M 5030 30l17l95 MDH465E 10117/95 I 1.2 1.2 <12 ugll Tetnchloroethylene SW4146 5030 10/17/95 MDH E65E 10/17l95 I 1.0 lA <1.0 ug/1 TenahydroPoran SW-846 5030 10/I7l95 MDH 465E 30/17l95 I 5.0 5.0 <5.0 ug/1 Toluene SW-8465030 10/17l95 MDH465E 30/17/95 I 1.0 1.0 <1.0 ugll 1,2,3•Trichtorobenzene SW-8465030 10117195 MDH465E 10/17l95 I lA LO <1.0 ug/I 1,2,4-Trichlarobenzene SW-8465030 10117195 MDH465E 10117/95 I 1.0 1.0 <1.0 ugll l,l,l-Trichloroethane SW-8465030 10117l95 MDH465E 10/17/95 1 2.0 2.0 <2.0 ugll 1,1,2-Trichloroedhane SP/-8465030 10/17/95 MDH465E I0l17195 I 1.2 12 <1.2 ug/l 1.1.2-Trichloroethylene SW-8465030 I0117/95 MDH465E I0117I95 I 0.5 0.5 <0.5 ug/l Tnchlorotluoromethane SW-8465030 I0117195 MDH465E 10117/95 I 1.0 1.0 <1.0 ug/1 1,2,3-Trichloropropane SW-8465030 I0/11195 MDH465E 10l17N5 I 1.0 1.0 <I.D ug/1 Trichloroorifluometliane SW-846 5030 I0/17195 MDH 465E 10117195 1 5.0 5.0 <5.0 ug/1 1,2,4-Trime[hylbenzene SW-8465030 10/17I95 MDB465E 10117/95 I 1.0 1.0 <1.0 ug/l 1,3,5-Trimethylbenzem SW-846 5030 10l17/95 MDH 465E 10/17/95 1 1.0 1.0 <1.0 ug/l Vinyl Chloride SW-846 5030 10l17/95 MDH 465E 10/17l95 I 1.0 1.0 <1.0 ugA m,p-Xylene SW-8465030 10l17/95 MIDH665E 10117/95 I 1.0 1.0 <1.0 ug/l o-Xylene SW-8465030 10/17/95 hIDH465E I0/17195 I 1.0 1.0 <1.0 ug/1 HPLC Analysis Acenaphthalrne EPA 610 10725195 EPA 610 11/02/95 1 1.1 11 <1.1 ug/1 Acenaphthene EPA 610 10125f95 EPA 610 I II02/95 1 2.0 2.0 <2.0 ug/I Anthcacene EPA 610 10125/95 EPA 610 1 U02/95 1 4.0 4.0 <4.0 ugll Benzo(a)amhxacene EPA 610 10125l95 EPA 610 11102195 1 0.30 0.30 <0.30 ug/I Benzo(b)Fluo'anthene EPA 610 10/25/95 EPA 610 11/02195 I 0.14 0.14 <0.14 ug/1 Benzo(k)fluoranthene EPA 610 10l25/95 EPA GIO 11102195 l 0.01 0.01 <0A1 ugfl Benzo(g,h,i)perylene EPA 610 10l25I95 EPA 610 11/02I95 l 0.19 0.I9 <0.19 ugA Bcnzo(a)pyrene EPA 610 10/25195 EPA 610 l l/02/95 1 0.10 0.10 <0.10 ug/I Chrysene EPA 610 I0I25I95 EPA 610 11102195 l 2.0 2.0 <2.0 ugll Dibenzo(a,1t)ant6racene EPA 610 10/25195 EPA 610 11102195 1 0.10 0.10 <0.10 ugll Fluotanthene EPA 610 IOY25195 EPA 610 I Il02195 1 0.30 030 <0.30 ug11 Fluorene EPA 610 10125I95 EPA 630 I1l07J95 l 0.10 0.10 <0.10 ug/1 Indeno(1,2,3-cd)pyrene EPA610 IOY15I95 EPA610 11102I95 1 0.14 0.14 <0.14 ug/1 1-Mefiylnaphthatene EPA 610 10/25195 EPA 610 i llOZl95 1 5.0 5.0_ <5.0 ug/I (Report continued on next page) CGen[: Dakota Counry Log•in: 953233 Project Number: CMXX-95-0722 Matrix: Liquid I,ab Sample ID: 95-3233-05 Clien[ Sample ID/Descriptiou: PZ-2 Laboratory: Lab Contactlphoae: Sampler: % Moisture: MDL: RL: Braun Intertx Cocporadon B. Maki/612-942-0820 Btaun Intectec Nat Applicabic Method Decection Limit Repomng Limit Date Sampled: 10/I1/95 Date Received: 10111/95 Date Reparted: 11/07/95 Page: 11 Extract Extract Analysis Analysis DIIution Compomd Method Date Method Dah FaMOr MIDL RL Sample ResWt 2-Methylnaphthalene EPA 610 10/25/95 EPA 610 I1/02/95 1 5.0 5.0 <5.0 ug/1 Naphthalene EPA 610 10/25195 EPA 610 I I/02N5 1- 13 1.3 < 1.3 ug/t Phenanrhmne EPA610 10/25l95 EPA6I0 I1/02195 1 12 12 <12 ug/t Pyrene EPA 630 10/25/95 EPA 630 11/02195 1 0.40 0.40 <0.40 ug/I Remarks: This sampie was zxuacted past the EPA recommended holding dme. Inorganic Alkatinity, Torel - • EPA 310.1/3 10/17/95 4 10 40 410 mg/1 ? Sulface • - EPA 375.4 I0/17195 1 !0 10 37 mg/1 ; Sulfide, Toral - - EPA 376.1 10J18/95 1 0.40 0.40 2.8 mg/I Nu[rient Nttrogen, Ammonia - - EPA 350.1 10119/95 1 0.01 0.01 0.63 mg/l Nitrogen, Nittate - • EPA 353.2 10/12/95 I 0.02 0.02 0.11 mg/I MetaLs Arsenic, Toral - - EPA 200.7 10117/95 10 50 SOD <500 ug/I Banum, Total - - EPA 200.7 10/16/95 1 10 10 2400 ug/I Cadmmm, Total • - EPA 200.7 I0/16/95 1 IO 10 <10 ug/I Chromium, Total - - EPA 2007 10/16/95 1 IO 10 340 ug/t Hardness,Caicium - - SM2340H 10/19195 SO 1.0 10 1900 mgEq/f Lcad, Total - - EPA 200.7 10A6/95 1 30 30 160 ug/f Mereury, Top! - - EPA 245.1 1020/95 I 0.2 0.2 1.6 ugll Potassium, Total - - EPA 200.7 10117195 1 200 200 21000 ug/1 Selenium, Toral . - EPA 200.7 10116195 1 50 SO <50 ug/I Silver,Top1 - - Epp200.7 10/16/95 1 20 20 <20 ug/I Sodium, Total - - EPA 200.7 10117/95 t 300 300 72000 ug/1 Metala ' Arsenic, Disso(ved - • EPA 200.7 10/12/95 1 50 50 <50 ugft Barium, Dissolved - - EPA 200.7 10/12195 1 10 IO 76 ug/I Cadmium,Dissolved - - EPA200.7 10/12/95 1 IO 10 <10 ug/1 Chromium, Total Dissolved - - EPA 200.9 10112195 I 12 12 <12 ug/I Lead, Dissolved - - EPA 200.7 10112195 1 30 30 <30 ug/I ' Mereury, Dissolved - - EPA 245.1 10124l95 1 0.2 02 <0.2 ug/1 Selenium, Dissolved - - EPA 200.7 10/12195 I 50 50 <50 uglt Silver, Diswlved • - EPA 200.7 10112/95 I 10 IO <10 ug/1 gb ga gb ga 'I'he Ieporung limi[ (RL) was raixd, p diludon of the sample was necessary due to marrix in[erfewnces. gb The reporting limi[ (RL) was raised, p dilution of fhe sample was necessary due m high concenuations of tliis analym. (Report wndnued on next page) ,,; Aakog Coun 95-33 `I Number: CM,yX 95.p7 z _u'aPle ID: q9` 3u233-pG 3amPle ID/DescriPtfoa; PZ 3 Compound ?''ganic ComPo.mda ide :ne ?medw?? ^omethane e ?ne ie oride 1eMene °fOPropane .? Lobaraeory: ota ?VP "a, Co ?? p h one: ?+Moistm.e, B. Ma ? Co?PonCOn 8nun?a???z`?20 ?L• NOt NPPlicable Me °d ? tec tlon Ligi[ ?p° ?g Li mit EktnM Method Estract q?y Date Meth? A"yIs Di7u-ffoa Date Facyr MDL RL SW-8465030 10/17/95 MDH465E ? SW-8465030 10/17/95 10/77/95 ?H SW-8465030 10/17/95 1 ' SW-8465030 MDHq65E 10 10/I)/95 1 50 50 SW$? !0/17/95 Date Sampied : Jv? 10111195 Ua[e ; P°tted: 1011 %95 11/07/95 Nb'e: ]2 SamPle ResWt 5030 10/1 DH 465E 7/93 MDH 177/95 ? 1.0 1.0 <50 u8/! 10i17/95 1.0 c I.0 u ?''846 5030 ?SE 10/17/95 1 1.0 1.0 ? 1.0 8/1 ?•8465030 10/17/93 lM H 1 I.0 ug/I ?'-8465030 IOp7/95 M ?E !0/17/95 ? 1.0 1.0 <110 u/1 10/17/95 ? 0.3 ?-8%5030 IOp7/9S DH 4eE 10/17/95 SW'g46 5030 ?I.O ug/1 1 0.3 MDH465g IO/t7/95 0.5 10/17/95 MDq465E 10/27/95 1 D.5 ?0.3 ugq S.0 5.0 <0.5 u SW-gq6505030 30 10/17/95 MDH 10/17/95 1 11.0 .0 1.0 <5.0 B/1 ?8Q SW846 5030 10/17/95 !0/77/95 465E 10/17/9 1.0 c<t1.0 .0 ? SW-g465030 MDH 465E 10/77/95 5 j 1.0 ° Sw-gq?5030 10/t7/93 ?H465E 10/17/95 1.7 1.0 10/17/95 1 1.7 <1.p ? MDH465E 10/17/95 1 1.0 1.0 <1.7 u ? SW-1465030 10/17/g5 2.5 <1.0 "8/1 SW-8465030 10/17/95 ? 1.0 2.5 <?.5 SR SW-g465030 IO/1107/95 /t7/95 MOH46 g 70/17/95 1.0 <1.0 u SW.8465030 1 u8 1.5 !0/17/9S MDH 465E 10/i?/95 10/17/95 1 5-0 1.5 3.6 i SW-gy?5030 10/17/95 ilDHq?6SE 1010/17/95 1 1.0 117/95 it 1.0 ?5? <l.p ug' SW-gq6 5030 g SW-8465030 10117195 MD11465 10 SW- 10/17/95 10 <1.0 ug/t 101 846 5030 10/17 95 ?H ?E 10 I?%95 1 <!0 SW-gq6 02 ug/i 5030 SW_g465030 10/17/95 ?H?SE 10/17/95 j S.0 S'? c0.2 u ?7 10/17/95 MDH465E 10/77/95 0.2 <5.0 u8 ?'-8465030 10117195 1 1.5 0.2 <0.2 8/1 SW'8465030 10/17/95 1 0.2 7.5 u8A S 10117195 ?H465E 0.2 <1.5 u9,7 10/17/95 '?tDFIq65E 10/17/95 G0.2 SW-gq6 5030 10/17/95 ?K? E 10/1? 9S ', 1.0 u%/1 SW-8455030 10/17/95 MAIDII UH465E IOry7/95 1.0 0.3 u// 1.0 <0.3 u8 1.0 SW-gq65030 10/1 7/95 1 00.2 .2 0.2 <1.0 u81 SW.gq6 5030 10/I7?5 M ' 0.3 cI.O SW-gq6 10117195 DH 465E 0.2 8 ,?.mH 10/17195 <0z ?g/1 5030 SW-g465030 10/17/95 b/pH46 E 10/17/95 ? S.0 8/I SW.gq65030 10/17/95 MDN46,TE 70/17/95 ? 5.0 5.5.0 SA 0 <5.0 ? 1.0 tOry7N5 MpH465E 10/U/95 1 <SA U SW-8? 5030 10/17/95 1 7.0 .0 c 1.0 8/1 SW-8463030 10117/95 ? 1.0 1.0 < 1.0 uP?1 10/17/95 MDH465E !0/17/95 1.0 ?w3o 1oin/ss ?H ?ss iomros 1 os <I.0 u? s? sw-s4cso3o m/nros acss ioini9s ' os as 10/17/95 ?H MD?SE 1 0.5 <0.5 ug/! 10/17/95 1 0.3 0.5 G0.5 u8/1 ?'-8465030 10/17/95 A465E ]0/17/95 1 1.0 1.0 <0.5 ug/i MDH465E 10/17/95 1.0 7.0 <1.0 uP?1 < 1.0 1 1.0 !.0 ugq <1.0 ug/1 r t? ? i (RePott conpnued on next pa$e) CGmt: Dakom Counry I.aborstory: Baun intettec Coryontion kif612-942-4820 B M Date Sampled: I0l11/95 Dah Received: I0111/95 Log_iw. 95-3233 I.ab CoomWPhone: Sempter: a . Braun Inrcruc Date Rep°rted: 11107l95 Project Number. CMX7C-95-0722 % Moisture: NotApplicable Matriz: Liquid ab Sample ID: 953233-06 I ASDL: Mechad Detecdon Limit , RL; Repomng Limi[ Psge: 13 Clieot Sample IDlDescriptlo¢: PZ-3 Ectnct Extnd Anelysis AuallSis DOWion Factar t D MDL RL Samp le R?sult Compaund Method Date Method a e Isopmpylbenzene SW-8465030 101l7/95 MIDH465fi I0117l95 1_ 1.0 1.0 1 0 <1.0 <t 0 ug/t ug/I Isopropyltaiuene SW-846 5030 10117/95 MDH 465E 10117195 1- 1.0 0 5 . 5 0 . <5.0 ug/l Metlhyl ENy1 Kemne SW-846 5030 I0II7195 bIDH 455E I0I17195 1 1 . 0 5 . 5 0 <5.0 ug/t Methyi Iwburyl Kewne SW-846 5030 10117195 MDH 465E I0117/95 . . Methyl Teniary Buryl E[her SW-846 5030 10l17/95 ibIDH 465E 10117195 1 1.0 5 0 1.0 5 0 <1.0 <5 0 ugll ug/1 Meehylene Chloride SW-846 5030 10l17N5 MDH 465E IN17195 1 . 1 0 . 0 1 . 0 <1 ug/t Naphthalene SW-846 5030 10l17795 MDH 465E 10117195 1 I . 1 0 . 1 0 . <1.0 ug/l n-Propylbenzene SW-8465030 10117/95 MDH465E 10117195 1 . 1 0 . 0 1 <1.0 ug/1 Srymne SA'-846 5030 10l17/95 bIDH 465E 10117195 . . 1,1.1,2-Tetrachloroethane SW-8465030 10A7/95 MDH465E 10117/95 t 0.5 1 2 0.5 1 2 <0.5 <1.2 ug/I ug/l 1,2.2-Temchloroethane 1 SW-8465030 I0/17195 MDH465E I01I7195 I . 1 0 . 1 0 <1.0 ugll , Teaaclilomcthylene SW-8465030 10/17f95 MDH465E 10lI7/95 I . 5 0 . 0 5 <5.0 ug/1 Tevahydrofutan SW-846 5030 10/17195 MDH 465E 10117195 I . 1 0 . 1 0 <1.0 ug/1 Taluene SW-8465030 10/17195 MDH465E 10111l95 1 . . 3-Trichloro6enzene 2 1 SW$46 5030 I0117/95 MDH 465E 10117195 1 1.0 1.0 1 0 <I.0 <1 0 ugll ug/i , , 1,2.4-Trichlorobenzene SW-8465030 10l17195 MDH465E 10l17195 1 1.0 0 2 . 0 2 . <2.0 ugll 1,1.1-Trichloroethane SW-846 5030 10/17l95 MDH 465E 10117I95 1 . 1 2 . 2 1 <1.2 ug/l 1,1,2-Trichloroethane SW-8465030 10/17195 MDH465E 10/17195 1 . 0 5 . 0 5 <0.5 ug/l 1.1,2-TrichloroetLylene SW-8465030 I0/17195 MDH465E I0l17l95 1 . . Trichlorofluommethane SW-8465030 10/17/95 hIDH465E 10/17/95 I 1.0 1.0 0 1 <1.0 <1 0 ug!! ugll 1,2,3-Trichlampmpane SW-8465030 10l17/95 MDH465E I0117195 1 1.0 0 5 . 0 5 . <5.0 ugll Trichloromfluoroetlune SW-846 5030 10/17/95 MDH 465E 10/17195 1 . 1 0 . 1 0 <1.0 ug/1 1,2,4-Trimethylbenzene SW-8465030 10/17/95 MDH465E 10l17/95 I . lA . 0 1 <1.0 ugll 1,3,5-Trimethylbenzene SW-8465030 10/17/95 MDH465E 10117l95 1 . VinylChloride SW-8465030 10117195 MDH465E 10/17/95 1 1.0 1.0 0 1 <1.0 <1 0 ugll ugll m,p-Xylene SW-8465030 10117195 MDH465E 10I17I95 1 l 9 1.0 1 0 . 1 0 . <1.0 ug/t o-Xylene SW-8465030 10/17f95 MDH465E 10/171 5 . . HPt,c analym Acenaphthalene EPA 610 10125195 EPA 610 11/02195 I l1 1.1 2 0 < 1.1 <2 0 ug/1 ugll Acenaphthene EPA 610 10123195 EPA 610 11102195 1 1 2.0 4 0 . 4 0 . <4.0 ug/l Anthracene EPA 610 EPA 610 1025/95 10l25195 EPA 610 EPA 610 11/02/95 11/07195 I . 0.30 . 0.30 <0.30 ug/I Benzo(a)antheacene Benzo(b)Fluorant6ene EPA 610 1Of25/95 EPA 610 11102N5 1 0.14 0.14 <0.14 ug/l Benzo(k)fluoeanrhene EPA 610 (Of25/95 EPA 610 1V02/95 1 1 0.01 19 0 0.01 19 0 0.04 <0.19 u6/1/ ug/l Benzo(g,h,i)perylene EPA 610 10125195 EPA 610 11l02/95 1 . 10 0 . 10 0 0.10 ugA -? Benzo(a)pyrene EPA 610 10/25/95 EPA 610 11l02195 1 . 2 0 . 2 0 <2.0 ugll Chrysene EPA 610 I0f25l95 EPA 610 11l02l95 11102/95 l . 10 0 . 0.10 <0.10 ugll Dibenzo(a,h)anthracene EPA 610 3025195 EPA 610 . Fluoeanthene EPA 610 1025195 EPA 610 I1102195 I 0.30 0.30 10 0 <0.30 <0 10 ug/1 ugll Ruo¢ne EPA 610 10125/95 EPA 610 I1102l95 1 0.10 . . ? O 5 50 50 S10 ugfl Methylnaphthaiene EPA610 195 I EPA610 1il02l95 1 ; f (Report continued on neze page) Cliena Dakom County Log-in: 95•3233 ProjeR Nurn6er: CMXX-95-0722 Watrix: Liquid Lab Sample ID: 95-3233-06 C(ient Sample IDlDescription: PZ3 Labontory: Hraw Intertec Cacpomtion Iab CoMactlPhoae: B. Makil612-942-4820 Samplet: Bnun Inartec % Moisture: Not Applicable IrIDL: Method Detecbon Limit RL: Reportin6 Limit Date Ssmpled: 10111/95 Date Received: 10111/95 Date Reported: I1107195 Page: 14 Extrea Ertract Ana15'sis Am1Ysis Dllotlon Compmmd Method Dah Method Datc Factor MDL RI. Sample Rcsult 2-Methylnaphthalene EPA 610 10125/95 EPA 610 11/02195 1_ 5.0 3 5.0 13 <5.0 <1 3 ugll ll u Yaphtlulene EPA 610 10/25/95 EPA 610 I1/01195 I- 1. 2 12 . < 12 g ug/1 PhenanNrcna EPA 610 10125l95 EPA 610 I1102195 1 1/02I95 I I 1 0 40 40 0 <0.40 ug/1 °ymne EPA 610 10125/95 EPA 610 . . Remarks: Tliis samPle was ezMcted past the EPA rcwmmendW holding ume. Inorganic Alkaliniry. Total - ' EPA 310.1/3 I0117/95 4 10 40 480 Sl mg/l m A Sulfate • - - EPA375.4 EPA 376 1 10117/95 I0118195 1 t 10 0.40 IO 0.40 3.0 g mgll Sulfidc, Toml - . Nu[rient - - EPA 350 1 10119l95 1 0.01 0.01 1.2 mS/i Niaogen, 7.mmonia . trare Nivogen.N Metals Tota] Arsenic EPA 20O.7 10/17195 5 . Total Barium - - EPA 200.7 I0l17/95 5 , Poul Cadmium • - EPA 200.7 10/I7I95 5 , Tatsl Chmmium - - EPA 200.7 10/17/95 5 . Hardness. Calcium - - SM 2340B I0l19/95 5 Tonl Lead - - EPA 200.7 10117/95 5 , Ytetcury, Total - • EPA 245.1 1020195 I Total Potassium - - EPA 200.7 10/17195 1 . Selenium. Total - - EPA 200.7 10117/95 5 Siiver, Toral - • EPA 200.7 10l17I95 5 iodium. Total . . EPA 200.7 IW t7195 1 Ne[als DissoLvW Arsenic - - EPA200-7 10112/95 1 , Dissolved Barium - - EPA 200.7 10/12/95 1 . DissoWed Cadmium - - EPA 700.1 10112195 1 , Total Diswlved Chromium - - EPA 200.7 I0112195 ( , Lcad.DissalvM EPA200.7 10/12195 l -Me:cury,Dissolved - - EPA245.1 10/14195 l Dissolved Setenium - • EPA200.7 10112195 1 , Silver. Diuolved - - EPA200.7 10112195 EPA353.2 [WI2I95 t 0.02 0.02 0.28 mg/1 i 1 50 200 1400 ug/I 10 50 8800 ugft 10 50 <50 ugll 10 50 1100 ug/l 1.0 5.0 850 mgEq/I 30 150 5200 ug/I 0.2 0.2 7.9 ug/I 200 200 42000 ug/l 50 200 <200 ug/1 20 100 <100 ugll 300 300 89000 ug/I 50 50 <50 ugA 10 10 270 ug/1 10 10 <10 ugll 12 12 <12 ug/1 30 30 <30 ug/l 0.2 0.2 <0.2 ugll 50 50 <50 ugll 10 10 <10 ug/1 gb ga ga ga ga gb ga ga ga ga 'Che rcporting limic (RL) was :aised. A dilution af fhe sample was necessery due m matriz inxdeeences. gb The'cporting limit (RL) was raised. A dilution of the mnple was naessuy due m high conttauations of tlhis anelyte. (Report condnued on nezt page) z CGent: Dakota Counry Lug-in; 95-3233 Project Number: CMXX-95-0722 Macric; Liquid Lab Sample ID: 95-3233-07 Client Sample IDlDescriptiou: PZ-A Compound Laboratorq: Lab Contsd/Phone: Sampler: % Moisture: kDL: RL: Baun Incerne Coipalation B. Makil612-942-4820 Baun Inrcmc Not Applicable Method Detection Limit Repoitin8 Limit Extnct Exlract Analysis AoalYs3s Dtlution Method Date Met6od Date Faetor MDL RL Date Snmpled: 101I l/95 Date Reeeived: 10711l95 Date Reported: I ll07/95 Pegc IS Sample Result Volatile Organic Compoundt SW-846 5030 10J17195 MDH 465E 10/17/95 1 50 50 ?50 u A 6 pcewnc Al1yI Chloride SW-846 5030 10117195 MDH 465E 10117l95 1 1.0 A 1.0 LO < 1.0 <1 0 ug/l ugll Benzene SW-S465030 I0117/95 MDA465E 10/17195 t 1 l 0 1 0 1 . <1.0 ugll Bromobenzene SW-8465030 10117l95 MDH465E 10717195 I . lA . 1 0 <1.0 ug/l Bromochlolomethane SW-8465030 10/17195 ivIDH465E 10l17195 . Hmmodichloromefhane SW-846 5030 10/17195 MDH 465E 10l17195 1 03 0 5 0.3 5 0 <03 <0.5 ugll ugA Bromofocm SW-8465030 10/17J95 MDH465E 10/17/95 I0I17195 1 1 . 0 5 . 5.0 <5.0 ugll Bromome[hane SW-8465030 10117195 MDH465E fi 10/17/95 1 . lA 1.0 <1.0 ugA n-Burylbenzene SW-8465030 I0/17195 MDH465 10117195 1 0 1 1.0 <I.0 ug/l sec•Burylbenzene SW-846 5030 10l17l95 MDH 465E . cert-Burylbenzene SW-8465030 10117l95 MDH465E I0l17195 1 1.0 1 7 1.0 1 7 <I•0 <1.7 uB/i ugll Car6on Te[rachlonde SW-846 5030 I0/17195 MDH 465E I0/17/95 I . 0 1 . 1 0 <1.0 ug/I Chlorobenzene SW-8465030 10l17/95 MDH465E I0l17l95 1 I . 2 5 . 2 5 <2.5 ugll Chlorodibramome[hane SW-846 5030 I0117/95 MDH 465E I0/17195 1 . lA . 0 1 <1.0 ug/1 Chlomediane SW-8465030 10117l95 MDH465E 10117195 . Chlorofortn • SW-846 5030 10117195 MDH 485E 10/17195 1 1.5 0 5 1.5 0 5 <1.5 <5.0 ug/l ugll Chloromethane SW-846 5030 10117/95 MDH 465E 10/17195 1 1 . lA . IA <1.0 ug/t 2Lhlamroluene SW-8465030 I0117195 MDH465E 10I17195 0 1 1 0 <1.0 ugll 4Chlorowluene SW-8465030 10/17J95 MDH465E 10l17l95 1 l . 30 . 30 <10 ug/1 1,2-Dibromo-3-Chloropmpane SW-8465030 10117195 MDH465E 10117195 2-Dibromoethane 1 SW-846 5030 10/17195 MDH 465E 10/17195 l 0.2 5 0 0.2 0 5 <0.2 <5.0 ugll ug , Dibromomedane SW-846 5030 10/17195 MDH 465E 10l17/95 1 . 0 2 . 2 0 <0.2 ug/1 1:-Dichloro6enzene SW-846 5030 10l17I95 MDH 465E 10117195 I 1 . 1 5 . 1 5 <1.5 ug/1 3-Dichlorobenzene 1 SW-846 5030 10/17/95 MDA 465E 10117195 1 . 2 0 . 2 0 <0.2 ug/l , 1,4-Dichiorobenzene SW-846 5030 10117195 IvIDH 465E 10117/95 . . 1-Dichlofoethane 1 SW846 5030 10/37/95 MDH 465E 10l17/95 l I 1.0 0 3 1.0 0 3 <1.0 ug/l . 1=-Dichloroethane SW-846 5030 10117195 MDH 465E I0/17195 1 . 1 0 • 1 0 <?.p ?? l-Dichloroethylene t SW846 5030 10117l95 MDH 465E 10117/95 1 . 0 2 . 2 0 ?? Z ug/1 , 2-Dicliloroeehylene cis-1 SW-8465030 I0/17/95 MDH<65b 10117195 1 • 2 0 • 0 2 <0.2 ugll , tans-1,2-Dichloroethylene SW-8465030 10l17l95 MDH465E 10l17N5 . . Dichlorodifluoromefhane SW-8465030 10l17195 MDH465E 10l17/95 1 5.0 0 5 5.0 5 0 <5.0 <5.0 ugll u8l1 DicNomFluoromethane SW-846 5030 10/17/95 MDH 465E I0/17195 1 1 . 0 1 . 1 0 <1.D ugfl 1,2-Dicliloropmpane SW-8465030 10117195 MDH465E 10117195 1 . 1 0 . 1 0 < 1.0 ugll 3-Dichlampropane 1 SW-8465030 10117/95 MDH465E I0/17195 1 . 0 1 . 1 0 <1.0 ugfl , 2,2-Dichloropropaee SW-8465030 I0/17195 MDH465E 10117195 . . 1-Dichlofo-l-propylcne 1 SW-846 5030 10l17l95 MDH 465E 10117l95 1 0.5 0 5 0.5 5 0 <0.5 <0.5 ug/I ugll , 3-Dichloro-l-propylene cis-1 SW-8465030 10/17/95 MDH465E 10/17/95 1 . 0 5 . 0 5 ? , trans-1,3-Dichloro-l-pmpylene SW-846 5030 I0/17195 MDH 465E 10l17195 I I . 1 0 • 1.0 ?? 0 u Bn Ethyl Benzene SW-846 5030 10/17195 MDH 465E 10117/95 1 . 0 1 1.0 <1.0 ug/1 Et6yl Ether SW-846 5030 10117195 MDH 465E 10717195 . Hezachlorobutadiene SW-8465030 10717195 MDH465E 10J17/95 1 1.0 1.0 <1.0 ug/1 (Report coadnued on next pagc) Client: Dakota Counry I.sbonNory:' Breun Intertec Co`porarion Date Sampled: 10l11l95 ivM: 10/11/95 D t R Log-in: 95-3233 lab CoNaedPhone: B. Maki/612-942-4820 a e ece Date Reported: 11l07/95 Project Number: CMXX-95-0722 Sampler: 8iaun Intertec Matrix: Liquid % Moisture: No[ Applicable I,ab Sample ID: 95-3233-07 MDL: Method Detcction Limit gl,; Repoxting Limit Page: 16 Client Sample ID/Description: PZ-A Extract Extract Analysis AmlYsis Dilutlan Factor t D (vIDL RL Samp le Result Compound Method Date Method a e Isopmpylbenzenc SW-8465030 10/17195 MDH465E 101I7195 1 1.0 0 1 1.0 1 0 <1.0 <1.0 ug/I ugA Isopmpyltoluene SW-846 5030 10/17195 MDH 465E 10/17195 I- 1 . 5 0 . 0 5 <5.0 ugll Methyl E[hyl Kerone SW-846 5030 I0117195 MDH 465E 10117195 1 . 5 0 . 0 5 <5.0 ug/i Medayl Isoburyl Kewne SW-846 5030 10/17195 MDH 465E 10117/95 _ . Methyl Tertiary Buryl Ether SW-846 5030 10117195 tvIDH 465E 10117195 l 1.0 5 0 1.0 SA C 1.0 <5.0 ugft ug/I Methylene Chlonde SW-846 5030 10l17195 MDH 465E 10/I7/95 1 l . LO 1 0 <1.0 ug/i Naphthalene SW-846 5030 10117195 MDH 465E 10117l95 1 1 0 . 0 1 [ 1.0 ug/l n-Propylbenzene SW-846 5030 10117/95 MDH 465E I0117/95 I . 0 1 . 1 0 <1.0 ugll SryRM SW-8465030 10/17195 NIDH465E 10l17l95 . . 2-Tecrachloroethane 1 1 1 SW-846 5030 10117195 MDH 465E 10!I7/95 I 0.5 12 0.5 1 2 <0.5 <12 ugfl ug/i , . , 2-Tetachloroethane 2 1 1 SW-8465030 10117/95 MDH465E I0117195 1 1 1 0 . 0 1 < 1.0 ug/l . , , Tevachlomethylene SW-846 5030 10/17l95 IviDH 465E 107I7195 1 . 5 0 . 0 5 <5.0 ug/1 Tecrahydrofuran SW-846 5030 10/17l95 MDH 465E 10117/95 10117l95 1 . 1.0 . 1.0 < 1.0 ug/i Toluene SW-846 5030 10l17/95 MDH 465E 3-Trichlorobenzene 12 SW-8465030 10/17/95 MDH465E 10/17/95 l 1.0 tA 1.0 0 1 <1.0 <1.0 ug/i ug/1 , 1_,4-Trichlorobenzene SW-8465030 I0117/95 MDH465E 10/17/95 1 10717l95 I 2 0 . 2.0 <2.0 ug/i 1,1,1-Trichloroerhane SW-846 5030 SW-8465030 101I7195 10117/95 MDH 465E MDH465E 10117195 I - 1.2 1.2 <1.2 ug/i 1.1,2-Trichloroethane SW-8465030 10117195 MDH465E 101I7195 l 0.5 0.5 <0.5 ug/i 1,1,2-Trichloroethylene Trichlorofluoromeehane SW-8465030 10/17195 MDH465E 10l17/95 1 1.0 1 0 1.0 1 0 <1.0 <1.0 ug/i ugll 1,2,3-Trichlompropane SW846 5030 I0117l95 MDH 465E 10117l95 1 10/17195 1 . 5.0 . 5.0 <5.0 ug/i Tnchiorotrifluomefhane SW-8465030 10117/95 MDA465E MDH 465E 10/17195 1 1.0 1.0 <1.0 ug/i 1,2,4Trimedryl6enzem SW-846 5030 SW-8465030 10117I95 10117195 MDH465E 10/17/95 1 lA LO <1.0 ug/i 1.3.5-Trimethylbenzene VinylCliloride SW-8465030 10l17195 MDH465E 10I17195 1 1 1.0 1 0 1.0 LO <1.0 <1.0 ug/i ugll p-Xylene m SW-8465030 10117I95 MDH465E 10117/95 10/17l95 l . 0 1 1.0 <1.0 ugfl , o-Xylene SW-8465030 I0117/95 MDH465E . HPLC Analysis EPA 610 lOR5195 EPA 610 11102195 1 1.1 1.1 0 < 1.1 0 <2 ugil ug11 AcenaphNalene EPA 610 10l25l95 EPA 610 11102195 1 2.0 2. . <4 0 ugll Acenaphfhene EPA 610 10/25195 EPA 610 11102J95 1 4.0 4.0 30 0 . g Anthrncene Benzo(2)anth'acene EPA 610 10125195 EPA 610 11102195 1 l ll02/95 I 030 0.14 . 014 ?014 u 8/1 Benzo(b)fluoramhene EPA 610 10/25l95 EPA 610 ? Benzo(k)fluoranthene EPA 610 EPA 610 I0I25195 1025l95 EPA 610 EPA 610 11/02l95 l 11/02I95 I OA1 0.19 0.01 0.19 0.06 <0.19 ug/i ugfl ? Henzo(g,h,i)perylene EPA 610 10/25/95 EPA 610 11102l95 1 0.10 010 0.14 <2 0 ug/l ug/i Benzo(a)pyrene EPA 610 IOf25l95 EPA 610 11I02l95 I 2.0 2.0 0 10 . 10 <0 ug/i Chrysene Di6euzo(a,h)anthracene EPA 610 l0J25195 EPA 610 11/02/95 I 0.10 . . l Fluoranthene EPA 610 10125195 EPA 610 11/02195 1 0.30 10 0 030 10 0 ? 0.30 u?' ! Bn Fluorene EPA 610 1025/95 EPA 610 11I02195 1 11102195 1 . 0.14 . 0.14 ? Indeno(1,2,3-cd)pyrene EPA 610 10115l95 EPA 610 11/02195 I 5.0 5.0 5 0 ug/l I-Methylnaphthalene EPA 610 10/25/95 EPA 610 (Report conuwed on nezc page) Client: Dakota Counry Log-in: 95-3233 Project Number: I.aboratory: Baun Lvemc Corponuon Date Sampkd: 10/11195 Lab CouqctlPhoce: B. Makil612-942-4820 Date Received: 101I1/95 CMXX-95-0722 Sampler. Bnun (ntertec Date Repor[ed: 11/07/95 Malrix: Liquid % Moivhae: Not Applicable I.ab Sample ID: 95-3233-07 MDL: Method Detection Limit RL: Reportag Limit Clieat Sample ID/Descriptim: PZ-A Aage: 17 Extract E.etrect Anal7sss AnalYsis DOWion Compound Method Date Metlwd Date FaMOr hIDL RL Sample Result 2-Methylnaphthalene EPA 610 1025/95 EPA 610 Naphthalene EPA 610 10l25/95 EPA 610 Phenanth[ene EPA 610 10/25195 EPA 610 Pyrone EPA 610 10125195 EPA 610 Remarks: This sample was extmcted past rhe EPA cecommended holding ume. ' Snorganic 11/02/95 1 5.0 5.0 <5.0 ug/l 11102/95 1- 1.3 13 < 1.3 ug/1 I1l02195 I 12 12 <12 ug/I 11l02195 1 0.40 0.40 <0.40 ug/I Alkaliniry, Total - - EPA 310.113 I0117l95 4 10 40 460 mB/I Sulfate - • EPA 375.4 10/17l95 I 10 10 52 mg/1 Sul[de, Totai - - EPA 376.1 10l18195 1 0.40 0.40 1.0 mgll Nutrient Nitrogen, Ammonia - • EPA 350.1 10/19/95 I OAl 0.01 0.99 mgll Niaogen, Nitrace - • EPA 353.2 10/12J95 1 0.02 0.02 0.29 mg/l Metals Arsenic, Total - - EPA 200.7 10117/95 5 50 200 1100 ug/I Barium, To`al - • EPA 200.7 10/17195 5 10 SO 8900 ugil Cadmium, Total - - EPA 200.7 10l17195 5 10 50 <50 ug/I Chromium, Total - - EPA 200.7 10117l95 5 10 50 1000 ugll Hardness,Calcium - - SM2340S I0/19I95 5 1.0 5.0 870 mgEqll I.aad, Total - - EPA 200J I0/17195 5 30 150 5300 ug/1 Mereury, Total - • EPA 245.1 I020195 I 0.2 0.2 8.4 ugil Porassium. Total - - EPA 200.7 10117195 I 200 200 41000 ugil Selenium, Total - - EPA 200.7 10l17/95 5 SO 200 <200 ug/l Siiver,Toni - - EPA200.7 10117195 5 20 100 <100 ugll Sodium. Tatal - • EPA 200.7 10117195 1 300 300 98000 ug/I Metals Arsenic,Dissolved - - EPA200.7 10/12/95 2 50 100 <100 ugll Barium.Diswlved - - EPA200.7 10J12l95 1 10 10 260 ugil Cadmium, DissolvW - - EPA200.7 10112/95 1 10 10 UO ugil Chromium, Total Dissoivcd - - EPA 200.7 10/12195 1 12 12 <12 ugll Lead,Dissolved - - EPA200.7 10l12195 1 30 30 <30 ug/1 Mercury, D'usolved - - EPA 245.1 10l24/95 1 0.2 0.2 <02 ugil Selenium. Diswlved - - EPA 200.7 10I12195 1 50 50 <50 ugil Silver,Dissolved - - EPA200.7 10112/95 1 10 10 <10 ugil ga The eepomng limic (RL) was raised. A diluuoe af the sampfe wu neccssary dm W matrix inaAbrences. gb The reporting limi[ (RL) was iaiud. A dilu[ian of the sample wu necessary due m high concentrzuons of this analyte. gb Sa ga ga ga gb ga ga ga ga (Report continued on nexc page) Clienk Dakom Counry 7ag-in: 95-3233 ProjeR Number. CMXX-95-0722 Matrix: Liquid Lab Sampie ID: 95-3233-08 Climt Sample ID/Description: Filtered Metals Biank Laboratory: „ • Lab CamaNPhonec Sampler: % Moishve: MDL: RL: Braun inceriec Coryorduon B. MakU612-9424820 Baun Inmrtec Not Applicable Mefhod Deaction Limit Reporting Limi[ Date Sampled: 10111195 Date Received: I0/11195 Date ReportM: I ll07l95 Page: IS Exo-ea Fxtna noalrsis Malrsis nawton Compoimd Method Da[e Method Date Factor MDL RL YO ANALYSIS PERFORMED ON 77DS SpMPI,S Sample Ravlt (Report conunued on nez[ page) . . . .. , C4ent Dakom Counry Laboratory: Hnun Wectec Coryorauon Date Sampled: 10l11l95 Log-in: 95-3233 Iab Conta¢t/Phone: B. MakV612-9424820 ihte Received: I W l ll95 Project Num6er. CMXXA5-0722 Sampler: Brdun Lnertec Date Repocted: 11107l95 Matrix: Liquid % Moishve: NatApplicable Lab Sample ID: 95-3233-09 hIDL: Method Detecuou Limit RL: Repocting Liati[ Client Sample IDlDescription: Trip Blank Page- 19 Extnct Extrsct AnalYsis AmlYsis Dilution Compound Method Dare Method Date Factor MDL RL Sample Result NO ANALYSIS PERFORMD ON TAIS SAhiPLE (Report contiaued on next page) . I " • ?1e ?p1?; 10111195 ' Breun Inretmc Cocporaaon Laboratory: Maki/612-9424820 . B Ph Date Received: I0/11195 Reported: 11/07I95 p t Cllent: Dakota Counry . una Lab ContacU Breun Intertec y e La8'iu: 95-3233 project Numher: CMXX-95-0722 sampja; % Moisture: Not APPlicable Method Decection Limit Niatrix: Liquid 95-3233-10 MDL; RL: ReWcang Limit Lab Sample ID: ft $e. 20 Client Sample IDlDe4criptton: Field Blank E,chact Extract Anslysis AaalYSis Dilution Fador NIDL N' ?ple Result M?ad pe? Method Date Compound Volatile Organic Compouuds ' S0 SW-846 5030 10117/95 h1DH 465E 10117195 1 1.0 50 1.0 <50 u8n < 1.0 ug/l <1 O °?' Acewne g?y-g46 5030 10117195 MDH ?SE 10117l95 l 1-0 p 10117195 MDH l 1.0 1.0 - 1 0 ug/1 < C6iocide Altyl , gN -846 5030 lOf Vl95 MDH 10117195 1 0 1 1.0 < 1.0 ugll Banzene Bromohenzene . SW-846 5030 10/17f95 t ytiy_g4( 5030 10117195 MDH 65E <0 3 uB? Bromochloromethane 7l95 1 0.3 0 10f17/95 MDH 465E l0/l 5 0.3 0.5 . <0.5 uHn Bromodichloromediane . SW-846 5030 S\y_gp( 5030 10117195 MDH 465E 10I17195 1 5.0 50 5 Q ?gn < ? 1 ? ugl? Bromoform SW-8465030 10I17195 MDH465E 1.0 MDH 465E 10117195 1 1•? 0 1 ?1.0 ?H« Bromome?hane g?y_gq( 5030 10/17/95 I0/17195 MDH465E 10117195 1 1. . n-Burylbenaene gW-8465030 p t ?l,p ug11 ;ec•Buryibenzene 10111195 1 1'0 g?y_gq( 5030 l0l17195 MDH 465E 10I17195 1 1.7 1•7 ?1.7 uBn 0 u6n 1 < :en-8urylbenzene ?$46 5030 1 1.0 10117/95 MDH ? E 10117195 MDH 1.0 S Z . <2.5 v8n CarbonTevac6ionde g?y_gq65030 10117195 MDH 465E 10117195 1 Z'S ' 0 1 < 1.0 u6/i Chlorobenune Chlorodibromome?ane 10117/95 SW-846 5030 10117l95 1 1.0 g?r-846 5030 10117195 MDI3 465E . 5 ugll < 1 Chloroctliane 1 1.5 $W-846 5030 10117I95 MDH 465E 110117195 0111/95 ? g'? 1 5 S.0 - . <5.0 ?Bn 0 ? <1 Chloroform gW-846 5030 10117195 MDH 465E 10I17795 1 1.0 MDH ?SE 1.0 IA . < 1.0 ugll Chloromethane 1 1.0 g?y_gq5 503D 10117195 10117195 10l17N5 MDH465E 10 10 <10 ? 2.Clilommluene 1 SWg.y65030 10117195 MDH 465E 10117195 4-Chlororolueae gRr_gq( 5030 0 Z <0.2 ?Bn 1,2-Dibromo-3-Chlompmpene MDH 465E 30117195 1 4' 5 ? c5.0 ugli h e gVV-846 5030 30117195 1011'7I95 1 5.0 10117I95 MDH 465E 0 2 0 '2 <0,2 Ugl1 %n 1,2-Dibromoct gW-846 5030 ' 1Of17/95 1 I0I17195 MDH 465E 5 I .5 1 < 1.5 ?Sn Dibmmomethane ene 1 . gqr..g46 5030 10117l95 1NDH'?SE 10117/95 2 0 02 ?0 Z ugn 1,2-Dichlorobenz ne . Sy_g465030 10117/95 1 10/17I95 MDH 465E 1.3-Dichlorobenze SW.gq( 5030 0 1 <1.0 u8? t.4-?ichiorobenune 10117195 1 1.0 SW-8465030 IOfl7l95 MDH 465E 03 IO(17/95 1 . 0.3 <03 uPil 0 u8? <1 1,1•DichloroetLane 1.0 SW-846 5030 10117195 MDH 4658 MDH465E 10l17/95 1 ' 1•0 2 0 . < 0.2 uq/I 1:-Dichlomethane l 1I95 1 02 SW.g465030 t0/l 0117195 MDH 465E iomms 02 - oz <o.z us" ene t,t-Dichloroefhy 2-Dichloroedrylene c?s-l 1 gW_gqb 5030 1 y1y_gqb 5030 10117195 MDH 465E 10/17195 <5 0 uS/I , trans-l.2-DichlofoethYlene 10/17/95 1 5.0 IOf17195 MDH ?SE 0 5 5.0 5.0 . <5 0 U?, DichiomdiFluoroenethane . 1 yryy.846 5030 SW-8465030 30117l95 MDH ? E 10/17195 10117195 1 1.0 .0 1 < ? 11.0 u8A ? °?? Dichlorofluo`omethane y?y.g465030 10117195 MDH MDH465E 10l17195 1 1.0 1 .0 1 0 ' <1.0 ug? 1,2•DicWOropropane SW-8465030 10117195 MDH 465E 10/17195 1 1'0 . 1,3-DichlornP?PmO SW-846 5030 10117195 0 5 <O 5 u? 2.2-DichloropmPane S?R846 5030 10117195 MDH 465E 10117195 1 0.5 10I17195 1 0.5 0.5 uB? <0.5 <0 5 u8? 1.1-Dichloro-l-proPYlene l 0.5 SQy$qb 5030 10117195 ?H 465E 1 MDH 465E 10117195 0.5 0 1 . < 1.0 ?8?? ene cis-l3-Dichloro-I-pmPY ne l 1 1.0 SW? 5030 SOl17195 t0l17195 MDH 465E 0 . t 0 < 1.0 u8? c vans-t,3•Dic6loro-l-propy 10117l? 1 1. S?y_gqb 5030 10117195 MDH 465E . Ethyl Senzeem y1y-846 5030 10l17195 1 1 0 ?1.0 ? Ethyl Ether . gkr_g4G 5030 10/17/95 MD1? 465E t0J17195 1 Hexachlombumdiem (gepott co¢tinued oa ncx[ page) :liend Dakota Counry '.og-in: 953233 ?roject Nwnber: CMX7C-95-0722 Natrix: Liquid ab Sample ID: 953233-10 :lient Sample ID1Dacriptiou: Ficld Blank , .. . Laboratory: Breun Intcnec Cofpocarion !ab ContadlPhone: B. MakV612-9424820 Samplv: Braun Inrcaec % Moiuure: Not Applicable hIDL: Mefhod Deucdon Limi[ RL: Repocung Limi[ Date Sampled: 1011I/95 Dah Received: 10111/95 Date Reportcd: 11/07195 page: 21 Eztract Eztract AnalYsis Analysis Dilution Compound Method Date Method Date Factor hIDL RL Sample Result :sopropylbenzene SW-8465030 10117195 MDH465E 10117l95 I 1.0 1.0 <1.0 ugll :sopmpyltaluene SW-846 5030 I0/17/95 MDH 465E 30117/95 1- 1.0 1.0 <1.0 ugA Nethyl Ethyl Kerone SW-846 5030 I0/17195 MDH 465E 10117l95 l 5.0 5.0 <5.0 ug/1 Nethyi imburyi Kerone SW-8465030 101I7195 MDH 465E 10117l95 1 5.0 5.0 <5.0 ugB Ke[hyl Tertiary Buryl Eeher SW-846 5030 I0/17195 MDH 465E 10/17/95 I LO 1.0 <1.0 ug/t Nefhylene CNoride SW-846 5030 10/17/95 MDH 465E 10l17/95 1 5.0 5.0 <5.0 ug/I 9aphthalene SW-8465030 10l17/95 MDH465E 10117195 I LO LO <1.0 ugll i-Propylbenzene SW-8465030 10/17195 MDH465E 30lI7195 1 1.0 1.0 <3.0 ug71 Sryrene SW-8465030 I0l17195 MDH465E 10117/95 1 1.0 1.0 <1.0 ugli 1,1,1,2-Tetnchloroethane SW-846 5030 I0117l95 MDH 465E 10/17/95 t 0.5 0.5 <0.5 ugA 1,1,2,2-Tetrachlaroethane SW-6465030 10117/95 MDH465E 10117195 I 1.2 1.2 <l.2 ug/l Pevachloroefhylene SW-846 5030 10117l95 MDH 465E 10117l95 1 1.0 1.0 < 1.0 ug/f I'etrahydrofuren SW846 5030 10117195 MDH 465E 10117/95 1 5,0 5.0 <5.0 ug/1 i'oluene SW-8465030 10/17195 MDH465E 10117/95 1 1.0 1.0 <1.0 ug/1 1,2,3•Trichlorobcnzene SW-846 5030 10117195 MDH 465E 10117195 1 1.0 1.0 < 1.0 ug/I 1,2,4-Trichlorobenzene SW-8465030 I0/17195 MDH465E 10117/95 I 1.0 1.0 <1.0 ug/1 1,1,1-Trichiomet6ane SW-8465030 10/17/95 MDH465E I0/17l95 1 2.0 2.0 <2.0 ugA 1,1,2-Trichloroedhane SW-8465030 10l17195 MDH465E 10/17195 1 1.2 1.2 <1•2 uB/I I,1,2-Trichloroetlrylene SW-8465030 10117195 MDH465E 10/17195 1 0.5 0.5 <0.5 ugll Trichlorofluommethane SW-8465030 10117/95 MDH465E 10/17I95 1 1.0 1.0 <1.0 ugll 1,2.3-Trichloropropane SW-8465030 10117195 MDH465E 10/17195 l 1.0 1.0 <I.0 ug/I Prichiorotrit]uoroedhane SW-8465030 10/17/95 MDH465E 10/17l95 1 5.0 5.0 <5.0 ugll 1,2,4•Tomefhylbenzene SW-8465030 10117195 MDH465E 10117195 1 1.0 1.0 <3.0 ug/1 I,3,5-Trimethylbenzene SW-8465030 10/19195 MDH465E I0111195 1 1.0 1.0 <1.0 ug/1 VinylChloride SW-8465030 10/17/95 MDH465E I0l17/95 1 1.0 1.0 <1.0 ug/1 m,p.Xylene SW-8465030 I0117/95 MDH465E 10J17195 1 1.0 1.0 <I.0 ug/I o-Xylene SW8465030 10l17195 MDH465E 10117/95 1 1.0 1.0 <1.0 ugll (Repon conwmed on nex[ page) • , ,. . ` Dete SsmPled: ? 8nun Interox Coipo1ation Date R????ved; 10111195 Dakota Counry tabontory: yob Cod%dlPhoa' B. MaW612-942-M0 Date Reported: 11I07195 Cumt. 95-3233 og m. I Sampkr. BmpIl I°?? Noc APPIiable , Project Nw?ber: CMXX-95-0722 % MoiStarr. Method Detecrion Li m¢ - Matrix: Solid 95-3233-11 ?L: Rpomng Limit gy; ; Lab Sample ID: page: 22 ? Client Sample IDlDeSCriptioa Medkod Blaak ' . AnalYsss DOutlon ? ?p1 e R?1t - Extnd Extrrct ? ? ?u Fador hIDL ' Method Date . Compo?d t p 10112195 SW'846 8270 10I16195 l uoarboa4 (P+1Hs) (GC?M ? 1 d H 033 33 0 0.33 0.33 <0.33 <0.33 ?kg mB?S r y PolyaromaUc cnaphthene p ? 35q g?y.g46 3540 10112195 ?'-8?' ?70 ?0116l95 I 0 . 0.33 0.33 <0.33 33 <0 ?g mP/k8 c AcenaPhhylem 1 Sryy_g66 3540 10/12195 ?-? ? 6195 1011 0.33 3 0.33 33 0 . <0.33 mg1r6 pnfiracene ne gW_846 3540 10112195 ???p 10116I95 1 540 10112195 0.3 . 3 ?B Benzo(a)anthrace gW-8463 033 0.33 <0.3 Denzo(b)tluoeamhene ffi70 10l16f95 l bryy-8463540 10112195 SW-846 10116?95 1 0.33 0.33 ?033 33 <0 mBnS mglkg Benzo(k)ftuocanchene SW-g463540 10112195 SW-8468270 0 101I6195 1 SW-? ? 0.33 3 0.33 033 . < 033 m8?? Benzo(B.h.i)perylene 1 y.ar?q5 3540 10112l95 10112195 SW-8468270 IOl16I95 1 0.3 D33 0.33 <0.33 mB?B Beazo(a)PYrene sene Ch g?y_g463540 SW-846 3540 10112195 ?-?' ?0 10116I95 <033 m8?8 ry Dibenzo(a,h)antNracene 8270 10116195 1 Ott2l95 S?'1-846 0.33 033 033 0.33 <0.33 mglk6 Dibenzofucan SW-846 3540 I 10116195 SW-8463540 10/12195 Sw-8??70 ta16N5 1 SVV-846 ffi7 0.33 0.33 033 <0.33 <033 ?B ?kB fluorantheae SW-846 3540 10/12195 l0/12195 SW-8468270 10116195 1 t 0.33 3 0 0.33 <0.33 n+BfkB Ftuotene [ndeno(1.2.3-ed)PY?ne y'?V-846 354U gW-846 3540 10112195 SW-846 8270 10/16195 . 33 0 <0.33 ?k8 2-MeLhylnaPh?ene 8270 10116195 i 40 10/12/95 ?"? 1 0.33 033 . 033 <033 3 mB?B ?kB Naphthalene SW-846 35 8270 t0116f95 g?y_g,W 3540 10112195 SW-846 1 SW-846 8270 10/16/95 0.33 033 <0.3 Phenanthmne SW.846 3540 10112195 Pyrene 16I95 1 Ol SW-? 8270 I 'w' _ 74 88 % rec ? ? ?*s Semi•Volatile SuaoBates y?y_gqb 3540 10112195 /16/95 SW- - : 1? % iec ?.Fluorobiphenyl g?y_gqb 3540 IOI12195 70 ?0116 95 1 SW ' ioopenune-05 ? Sy-g46 3540 10112195 Te[phenyld14 _ (End of RePort) BRAUNS"" INTERTEC Chain Of Custody - ECS Log-in Report N >S-3.?23"3 Page of Rush f! Exception Rate Site Identification Client Identification e°soi' C =mrd a=lubeorfilter ?m r wc "'a?ef a = ii e - pro ect j Manager 1J?3yi?er?eQa? K.a[4 pGkd?qL?y a .: ye o=omer Sampled By: A Bottle type and number Temperature Upon Receipt H Received on Ice °C Condition Upon Receipt p Good ? Other ? o U • E ? d .? o ? 2 Ewdence Tape Intact ? Yes ? No ? NA Project #: Task #: m 2 ?O. o y ? ? ? WI LUST Project ? Yes ? No Are samples in compl(ance with soil movement SamPle No. C ll Q ?* y re ulations ? Yes ? No NA L b o ecU on a ? 1 c ? ( a Use Only) Sample Identiflcation Time ? O ? ? ? J J ? S Anal sis Remarks Y I 3rn -3yt 3 -- 0 1 OIS tt (. 05 C /??l?U R '1' k 't -OZ T??? Llkp -Po/ ??aBr7 D/f- u ? a 05 CQl7 rhef.tl' 1s -&3 (.?c I ?5? ,?rs 3 D rv-?rc 8.? o -o - qS r 3 a 3 'z -o17 17- t) „la? 3 .? -b? q/S ?ak a?u?4f ,7• ? C& ? U ` G , 1aAf 4 o . 6 3 rloRO W - ?v al? iPr,' o0 3 at1J E Re' y? jpte 1 Tim Recelved By: Relinquished By: Date Time Received By: e inqulshetl Dete Tlme Received for Laboratory By ? Data Time Commenls: ? ,. r••• , n?. ?- ..O,11mp1un hvenue, amppmp ana riecerving, Mlnneapolls, MN 55439 Form No. Claim 1/95 ATTACHMENT3 Subsurface Investigation Rub6c Dimasal Site L" 334 Lone Oatc Road 'cagn, Wiaaesom ?reoard For D3kOL4 COUIIiy ?'oje:L NuIIlber N0VP..^I.OC: 221, iOQG 31mP. ;:^.?C^2.G --JPUC1[1JP. BRauW INTERTEC Novembet 22. 1995 blr. Jeff Luebrs Dakota Counry Enviroamemal .lsanagemeac Depaztmeat 14955 Galaue Avenue Appie Valley, MII`I 551244579 s? n,mtm co.ro.ag- ,ZA5 Nwddcnii Dd" N4ndma tlai;hes, nAimmoat SSt 2a1t at 012b83A7W F= 683A888 s'q'? md smoon s.Wj *w aw ore rawd r,w:munmr Project Yo. OM135-07Z2 Dear W. Luet7rs: Re: Subsuriace Invesrigadaa, Rubber Disposa! Site, 1534 Loae Oaic Road, Ea,•an. 1dN As auchorized by Dakota Councy, Braun Intertec Corporadon condncred a suusurf= investigadon at che referenaed siLe during October 1995. Ouz resuits aze provided in the atrac!ied reporc_ Should you have aay quesrions regarding rhe comeacs of this reaoa, Piease connct me az (6I2) 683-5 i56. $inCereiy, .. ` 17 Paaicia M. Tezaaar, CPG Supervisor, Hydrogeologic Imvestigadons Table oe Canteats L Inuoducdon .........................'................ 1 II. Scope of Wark .................•••................... 1 M. Results ............................................ 2 A. Sice Geology and Hydrogeologq . . . . . . . . . . . . . . . . . . . . . . . . . . Z ? B. Waste Characteristics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 C. Anai7mcai Results for Soil and Grouadwater . . . . . . . . . . . . . . . . . . 3 D. Vapor ivioniwring Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 IV. Conciusions and Recommeudacions . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 V. Generdl ............................................ 5 Tables 1. Anaiytica! Results for Waste Samoles Z. Anaiydcal Results for Soii Samnie ;. Aaalydcal Resuits for Groundwazer Sampies Figures - 1. Site MaD 2. Groundwater Conrour Yiap Appeadic2s A. Borin? Logs and Well Constxuction Diag?.ams B. Laborazory Reporrs I, Introductioa Braua Incercec was auhorized by Dakora Crnmcy ro condua a snbsurface iavesti,°ation ac 1S4 Lone Oak Road ia Eagaa. Minnesom- The azea m be iavestigaeed was used as a disp°sal site fnr rubber collesxd at Fort SneEling durinq World War II. Tne pucpose of this iavesagadaa was m assess subsurfice conditions and confirm the abseace of pocentiaily hazardovs wam The site is located in a residentiai aret, and sevaaI honses avedie or are adjaceat m the fll area. A seismic survey conduc:ed previously iadicmd thaz rhe waste can;es ia thickncts arom a few fers to aQQrozimately 30 feet and is weda'° by 0 co 10 feec of soii. II. Scnpe of Work The iollowing tasks were performed by Braun Intercec for tbis pmjeix. A Site-SQecifc Safesq Plan was preQazed. A hollow-stem auger boring was conducmd thr°ugii the waste az the locaaon specined as VW-1 on the artached site map. 'I'he 6oring was advaaced duvugfi rhe waste uaal narive soils were encountered az appmximately23 feeL Sampies of tiie wasce were collecred from an aopmximate dernh of 10 feec and from'-U fieet for aaatYsis of RGRA metais and asbestos. The borehote waz monimred for mechane, and the cutrings were screened for organic vapors nsing a phataionizauoa dece=r (PID). - At the teffiiaatian of che boring, a snlitfiaad soil samole was collected_ The soil wag screened for ornanic vapors usinglaz headsuace pt°cedures, and a sampie was callecxed for analysis of volarile organic compaunds (VOCs) asiag MIDH Meshod 466A. PalYmaciear aromaric hydmcarboaS (PAHs) by Method SW-846 8270 and RGRA mesals. A vaoor maaitoring wefl was iasmlled m a de,pth of 20 feet in the bormg. A consauctioa diagrem is provided in Aupendix A. Approximately 24 hoats and 48 hours aiter insrallarion. me:bane cowmmdpac m the vaQor well were measared. ?,n air sample was also collec:ed using achazcoai mne br anaiysis of VOCs. Da[cota Coumy Project No. CIXC-95-0722 Yovember ZZ, 1995 Page 2 • Tbree addirional sod borings were condncxed for rosmlIabioa of temporarp monitqring welLt. Thege temporazy wells were labefed PZ-1 thmngh PZ-3_ Locazions aze slwwa on the aaached site map. Well consttucaoa diagtams are provided in ADpendix A. • After purging tfuee well valnmes, groundwazer samptes wete coIIected 5rom eaclt of the temporary wetls and analyzed tor rhe following pazameiers: Fieid pH Total RCRA mecals PAHs by EPA 610 Total Alkaliniry Ammonia as Nimogeu Sulide VOCs by 'LAIDH 465E Dissoived RCRA metaLs Ca hatduess Maace as Nitrogea Sulfate Sodium Porassium A dunlicate sample (labeied PZ-A) from PZ-3 and a field biank were also coIIer.ed and anatyzed. All analyacal samples wece piaced ia a cooler and uanspoaed co onr laborazory following scandard chain-0f-uswdy procedures. • The wells were removed and tfie boreholes were sealed afte: sampling was comoleced. . Waste cuuings were placed in drums and are being stored temnorariIy az Braua - Inrertec. For disposai purposes, a samQle of the waste cumngs was ana(;rzed for ROtA mesals using TCL.D. As reqisested by Dakota Cuunsy, we are coordinarin; disposal with USPCI. III. ReSU1tS A. Site Geology and Hydragefllogq As indicaced by rhe boring logs (Aopeadix A), all borings zacountered 3 to 4 iee: of ronsoil. At VW-1 aad PZ-3, the tonsoil (not native) was undedaia by rubber debris to deprhs oi 23 feec aad Zl feet, cesnectively. Six to 7 fees of dayey sand was zacouncesed in PZ-2 and PZ-3 az differem horizons. The remain,? soils consisced of siity sand and pooriy g-eded saad. Dakors County pzojecc No_ C,%M-95-0722 November 22, 1995 page 3 The water table occurs at a deQth of about S feec az the locadon of PZ-3. At PZ-I and feet PZ-Z> whica are located ac the b?e ? ?? flow tabin is wnthwcs?erly,dcoa?stent beiow the surfaca, resP?vely with mpographY (Figure Z)• - B. Waste Chamctenstics was shredded aad chopped inm small co 'Ihe waste tubber obsesved in the sad borings of ciodtiag re?a? sncfi as baats or medium piec?. It agpeared to consist primanlY ??d ? coaceattado? of raincoars. Chemicai analysis of the waste for RC? me?is . arsenic, barium; cadmium and lead (Table 1). No asbescos was desecced ia rhe samples. Laboracory tepocts aze conrained in Appendiz B. TQ,p anaiysis of RGRA merdls was Performed oa a samnie of the wasre cuttings. Resdts ue inciuded in Appeadiz B. Concenn-adonS are below the limics esiablished fnr the mxiciry chardcserisric. Thereiore, the wasce is not considered ro be hazacdaus- C. AaiyUcai gesults for Soil and Groundwater The soil samPle coliecxd from beaeazh che wasse in VW-i cnntained reiatively low concenaarions of azseaic, barium aad ctrramium (TabIe 2). No odies RCRP. memis> VOCs or pp,gs weze desected• (3mundwazer aaalydcal results are summarized ia Table 3. Two VOCs, ' bmmodicfilommethaae aad cfiiomform, were decwted ia ac lesss oae wetl; however, conc:naarions were below the Minnesora Deparrment of Health, Heatth Risk Limit (HRL)- Two P.AHs, beflzo(k)fluoramheae aad benzo(a)PYre?• were dececsed in PZ-3 as relarively (ow conceatrauons. No HRI. has beea essa6lished for these comQo?mds, irut for comparison, t?eY ylaximum Contaminaas Lavels (MCLs) ?1'?hed for public dtinldn; `F'? are beiow the suoplies. The firsc ?'aon for the P_SH anaiYsis did II°t'n'°ri?, ? ??re' ?e samole had m be re-rxzacsed Put the EPA rerommeaded holding time. The quaiitg of die resul?ing data is noc 6elieved to 1s"e been signincau[LY affec'ed. aze highThe rorai RGR?. maaLs concensatians for the gnundwarer samples . 'Lhis is likeiy a resuit of sedimeat ia ?e samples since the dissolved conceaaanons are reiaziveiy low or were noL detecs?- If the weils had be? rigoronsly developed and ?ilowed tn sec lon?er. the torai mesais conceaaauons wouid likeiy have beea much lowa. Dakora Counry Project No. C.ti=-95-0722 November 22, 1995 Page 4 D. Vapor Monitaring Results No VOCs were desected ia the air samnie colleaed from the vapor monimring weiI (Appendiz B). Vezq lugh methane cancem¢ations (16% ;as hy volume) were measured ia the vapor monitoring wrll both one aad two days a8er insalIarioa _ IV. Conc3usions and Recommendations Two oi rhe borings az the sire encouncered watte rubber az 3 ro 4 feer below grouad surfaca. The tlrictmess of rhe waste az chese locauons was 18 to 19 feet. Anatysis of the waste indicated high con?entra*+ons of inerals, particsslaziy bazium and lead. Resuits of TCLP anafysis indiare thaz the wasre is noc hanrdous under rhe roxiciry c'saraczerisuc. Based on wazer IeveLs measured ia rhe cemporary monicoring we:is, ;roundwaze: az che sire is flowing sourhwcsc, consiscenc wirh ronogrenay. Concensdrions of mral mecats in che groundwarer are high_ Howeve:, sinca dissolved mesai concenaauoas are, for the most part, beIow decectioa limits, the cotal me:al wncraQarions aze IikeIy due co sediment aad noc a re3ecrioa of groundwater quality. A sou samgle wllected from immediazely below rhe waste did not indicaze elevazed levels of ineais ia rhe soils_ The major environmearal conce:n az this sice is the presenca of explosive ;as (mediane) in the suusurfaca The source aad lateral eaTent or' rhe mechaae is unkaowa We did aot obsezve any signincwt organic mazerial in the waste ivbber which wouId be [ikely to pmducs lugh concan2razions of methane. IC is uniike?y thaz the cubber iuelf woutd pmduce acnIosive ;as. Other potendal sources for the mediaae are: leaking nanuai ;as lines, abandoned sepric syscems, sewecs, or orher uaknown deposiu of degxading wazce. The porous nazure oi che shredded rnbber may pmvide a conduit or a repository for the medane. Tne amount of inemaae detected in the vapor moniroring weil is ovrs three times the lowez exnlosive limi[ (100 percenc of rhe lower =iosive [imi[ is 5 percert ;as by volume). These levels aze considered his,n' and may presea a sigaiticant risk to rhe saiery of nearby residences ii ;as enters the dweiling or other connned spaces az e:cp(osive concantradons. As we discussed wirh DakoEa County pezsonnei during iaonimring of the vanor we!1 on Ocsober li, 1995, the basements of the du-ee houses ciosest to VW-1 should be monitored fnr mechane and merhane alazms should be iasralled. In addition, vapor monicorin; poinu should be insralled ae.tt ta the fouadations oi ttre houses. , D3AOII C7ImC7 ?:oje= YO. C3,l..?.°-95-472 Yavem6a '??., La95 Pap 5 At a d3iS I We cdecammem th= the aote=l som?s of dse mrshaae 6e iaves•igmei- quld incftide: 0 . disc?s-ons wirh dse lacal ;ds c?mo?q, ?? Pa?Oi ? I'd •5jjgerVCIIM*a,d' or dte ;as; . moniaoriag oi neunY se9vess Sor emiasive ps; md i ? . imezviews widt adjacra hame owaets m ab8ia iaiocmadon oa te lacm¢oa or ald i = searic syscems, comnosc pnes or od= ae:abq disnosal sires- i 3ased oa che iaiormmoa ouraiae? adaicanai smdic4 seonid be p?iaffied m d?ae ?e ' j4?oi ttLe medlaae and m eratuaze ooceaual c2aecve ae2s=• i V. Generai a pe:ioffiiag ia secvics. Br•ma Iate.= used ?haz de? o= ase 3ad skul ordiaaziiy ju=c''sed under simu'ar esGSmsm= OY rc==ie memues oi is pml?esuoa pr.tca=g ol che same lo=liry. No o[h¢ wm==L9 is maae or imended. ?'.won'tci??+9SOTL^.?L.R!]i i !I ? s s i T i ^ G Tacles Table 1 p,nalyapt gesuits fnr Wasre Samples (m31Y-.9) _ ......_ : . ...... .:..:.._ .:.,,: .:. ?:?;- •.??°-:- ,,.,.,.....:. _........ _...,.:;. .:?::;.,,.M...::-:,. . ?.,......,..... _,:?...:?.:. ?.::. : feetr , ,.;... ,..:.. 2 5 a2 Arsenic, Toral . 540 1600 garium. Torai Cadmium. Tural :8 •'S CSsomium. Toral 16 ? 1600 4400 Lead, Toral ,y(ercury, Toral ND ND Szienium, Torat ND iNfD 2 I ND SIIve:. Totai ' ND ND .Asbestos i?ID = Noc Demcxd i 1 ? i , t i f:lwonlesle=c\951072''1072Z.T Table 2 elnaiyrical Results ior SoiI Samnle (25') ,___._._?.._....?,..,;,:,•?.:•::::•::....,. .... .: . ;. .:::::.:._. _::<:.w.,.,. ._? VOCs Noae Demc,ed P AHs voae De.ected Arsenic. Total 6.4 Barium, Toral 24 Cadmium, Total iqD Chromium, Total 6.8 Lzad. Toca! LNp Mercury, Total VD Szienium. To[al ND SIlver, Total ND ? W = Noc Derttmd i:iwo'n;eslc=1951072210TL2T Tahle 5 ` - p,naiydcal Resuits for Ccroundwater Saumles (µg/L unless odierwisse indic=ei) -- ? 1? .1D (ND) ° Bmmodichlomma??' `ro 53 3.6 (ND) 60 C81oroi?orm ND " 0.04(U-06) N A BmmQc?fluur.mtheae W ND ,ro 0.10 (0.114) YA Beuzo(a)PY=0nd - ?.gMliniry, Toc+l m5R- 450 410 S80 (s60) NA MVL 49 3.7 51 (52) MA Sulfax 9 1 IS 3 (1.0) NA Sulfide. Toml mgiL . ia m3f- 0.0"a 0.63 1? (4.99) YA Niaogea. ,ammoc 1? 0 0.23 (0.29) 10.000 Yaogea. Nia3m m4n- 1.1 . 330 .`ID 1400 (.100) NA Arseaic, Toral 1400 2400 8800 (8900) 2000 Barium. TomL ? vp L?ID (ND) ? C"dmium. Toral 360 340 L100 (1000) -0.000 CSromium. Toml Hardaess. Catc.um m&E?iL 1500 1900 850(370) NA 1^<D 160 5200 (5300) NA Lead. Socal 1 6 S.b 7.9 (8.3) NA ,ylerasy, Tomt . 000 17 21.000 42.000 (41.000) NA Pom«^•^- Toml . ND vp ND (ND) 30 Solenium. Toai ? .?7 DTD (ND) -0 Siiver. Tatal 000 ?7 11.000 89.000(98.000) NA Sodium. Tatal . p,rsenic, Dissolved YD ND `ro NA 59 76 ?70 (250) =000 Hazium. Dissolved - ?p •tp ND W - S c,dmi?m. n;?tvea ? ,D rm ,rn :o.aoo C3mmmm, Dissolved ' ? .ro Yp ;•Ip NA usolved Lesd. D 5 0 YD DiD iYD NA ?iccsy, Dissolved . ? Yp ND *ID 30 Seknium. Diuoived SIlver. Diswlved ? _ ` Yp `ID W 30 = Ya Aopl'rabs NA vp = Ya Daeaea • :IIU. _ IdDx amm a" L= Dwtin¢ rmom rcma smw a?umtca X. vpG ? bims L'.waidu? 9A0 _'tJ.'1- ??? • LONE OAK HOAD _ - - - ' ? ? - . ?. , -- p.o.w. ? ? ? = I ' I . \ ' I . 1 I P I : ` APPROXIMAiE LOCAiION OJ l VAPOR MONITORING ? L 1 j ( ' I GROUNOWATER I I , rCOW DIREC'.10N 1 78 i.35 . 1 PZ-3 0 ? 1 ? N,' ? . I? . 796.10 1 \ >o i I P2-Z ) 9 ? ` S9 I 25' 4 50' ?? SCAL•: 1'. 90' ) `SO -10 ?r S10 1 ' . 795.77 - - ?RaPERTf UNE ? PZ-i 46 ? ?Sy PIEOMETER CRCUNDWAIER CONTOUR G? NAT10N (FT.) 795.77 GRCUNDWAiER 'E.._NA110N (F-1.) ? ???lf f?? GftCUNDWA ic.4 CONTCUR MAP 3/ ?? DAKCT.i CCUNTY 1534 t.ONE OAK ROAO I N I C!'t TLC _.>G.:N. NINNESaTA HT I eensa+ Is+EE ORANTI 31: JAG I i1-73-45 APP'!) 3Y? n%A i : ;i -1?-35 IV .OB v0. ;:AXX-?5-7722 OWG. NO. UXS077-2 I nGURE N0. ScuP - 40' 1 - ; t i R_O.W. -- -- ? -- -- I . -- 1- ?- LONE OAK Rit t. - - -R.O.W. - - T ? - - -` - - - ? - ? :- ? APPROXIMAic LOC.1T10N OF VENT WELL 7 ? ?. ?. _- PZ-T? ` ? - ? ? ? ? - - aReFERr, ur,e ? - n . PtEZOUE.-ER , i ? ?o• c eo' _cat.?. : = sa• ?..`..-..-..-. ? _..-..- - i __?-- ? / ?..-..-..- -.._.._.. ? T..__..-. -?..?.. . ? ? J wr oA1c A DeAwil BY: JAG 95 ' SITE MAP ??? ar?r'u pr: PMT 11_13_95__ DAKOIA COUNTY 1539 IAt7E OAK ROAD c`? , doB n0 CMXX-fl5-0722 - EqL'API, MINIIESOTA -- ?WG NO MX50722 SIIEET OF ? sf.eLE - I"= 1 i I ..-..? -? i i I ?.._ i ..-...I_. ? BeAUN- INTERTEC Appendix a Appendix A Borins Lags and Well Construci?on Dia?`rams LOG OF BORING PROJEGT: =-95-0712 - BORING: P7r1 LOG"IION: Dakota County See ate map. 1534 Looe Oak Raad Eagan, ?Tmesota DATE_ 10/20/95 SG1LE: 1" = 4' Eev. Depth ASTM Desaipdoa of Mmale - 798.0 0.0 Symbal (AS.4I DZ488) BpF Te? ? Yamy TOPSOIL: Organic Qay, blaclc, moisc (1'oPso+1) SP POORLY GRADn SAND with SII.T, 5ne SM : 'gaiaed, brown, watcrbeaciag, Ioose. 10 (Alluvium) au.l z aAiNu> nae g.uaea, crowmm gmy, watecbeating. (AlIuvium) 22 : POORLY GiZADID SAND, fine to medium :,aiaed, brou+n. water6eacin8, medium dense to very loase. (tllluvium) 2 Sec sczeea from 5 ro 15 feet ? ? i ? ? t ?'A7L:-')-)r= 3nun finertee ?Z4 oage I oi 1 LOG OF BORING BORING: PZ-? PROJEGT: G14.Y.Y 95-07ZZ LOC.?TION: . See site map- Dakota Cnuaty ! ]534 Lone Oak Road F?aan, D?Lnne4ota DATE: 10/10/95 SC?.LE: 1" = 4' ?iev. Depth AS'Iti I L Descripdon of Materiais (AST+?4 D2488) B ? PF I WL 'Ptsa or Nores Symb 0.0 oi - ? TOPSOII.: Orgaaic Clay, black, moisG I cropsoin L L 1 I 40 I SC . . a.AYEY SA`ID, fine gtained, Yellowish 4 i_ bmwn, wuerbearing, loose. { L I !I i ? i - (Alluvium) I i ? ? ? I SP r : POORLY G?ZADID SAND, fiae to medinm I ,aiaed. bmwu, wateroeariag. I ? (AlIuvium) r ? L ?%813 I 15.0 i i E:NID OF BORING + I I Screea sec from 5 t0 15 feet I ? - ? I i ? I ? I i r - , ( i ? 7 I , a, . fL-: ?sgO 3taun finenec LOG OF BORING PROJECP: GI1Y.Y-95-07L' Dakota Camty 1534 Lone Oak Road Eageu, Nume4ora EIev. Depth ASTM 8220 0.0 Symbol ? TOPSOII.: aion zn? . Desaipdon of :14acerials (I'aPsoil) BORING: LOCMOjd: See site maQ. SCALE: 1" _ : Tess or Notes 9 CL.-1YEY SAND, Ciae g'aed, gtey, moisx, medium dense. (Alluvium) . ? .•. ? I SP ;. POORLY GZ :DEJ SAND. :iae gRaiaed. - brown, medium dzase co very dense. . i (Alluvium) 13 i i 3nun ime¢s nz.3 cage . )[ = I PFOJECL: Cdxx-95-07'?S Dakota CountT 1534 Lane Oak Road Eagan, ,l4imesora ?1ev ? DeP?h I AS'M I ? .: ? _wacemeazing. END OF BORiNCi Sc:eea set 4om Z3. S co 33.8 feet LOG OF BORING LOCATION: See ste map. SCALE: 1" = q' BPF I?`/LI Tesrs or Notes 18 ? ? 62 7 ?Z ; aage 3mun Icuentt i .' i i 1 I ! r i i i ? ? LOG OF BORTNG Y-95-0TL' BORING: ?T?T_i LOCATION: a Cauoty See site map_ one Oalc Road ,,lTinnesoca DATE• lO/I]/9$ SCAI.Ec j" = 42 I?f ?escipdonofl?faterials - 1 bol (AS'M D2488) BPF ?VL Tesm or Notes ?.-. dark hxnwa tY Sand, fine vaiited, black m ? (ToP?? ?-: F?d I I + Rubuer debns. - i 14 ZZ I SP J POORLY GiZADFa7 SA ND, hne gtained, ? 6rown, moist I ?.'.'..: I 795 25.0 I ? s : I (Alluvium) ' END OF BORING i Water not observed with S feet of hoflow-;cem ? i auger in che grouad, ? I ! ? i i ! T.i:CC-?c_;i" 3nun in[enec VW_. ?age i or I MN IIniaue Fleff Numba NA 1lonitoring Well kield Data Sheet Genc Oakora Conncv ' Projecc Yumba C4IICC-95-0722 Ciry/Shaz Eaeav. MN 'eavumba pZ.1 Well C.ocatioa Sx rire mav Dare oFlusmllari o¢ 1040-95 ;ew VlR/GS Gwio4ist RF ick uo (- 0.1') ?•3. ?o oi 2iser xoe 80033' evauo¢ ;_ 0.01'wlo cap) mund Suriace IIevarian 798.0' . u,:") ornoxamare deo[h m water ::ore ss 'cuaaoa 5' ovraximue deoth w sc .vares =ncAUatered i• _aa m ToD aI Sea! •n :c 3auam oi Seat M ioo oi Sceen Surtace 2.31 a.3' eadh m Socem oi Screen 1a.3' ec[h co 3oaom oi Horiag 15' _Enoa oi aavanm: SA :t I.D. s !/a' swg I.D . :cane O.D. Promcuv¢ Cover ? Type: None LragcL* Lock Yo. Vone Concrem Suriatt SeaL• Yes _ No X Gmuc Above Seal: Yeu Cemrnc Grouc $enranire Seal Other None Riser P!pe: Type FVC Diameter Z" Tamt Leagtfi %' SeGians vsed 1 Cauplings No Can Ya X No Sca! Yta¢rial: Type Beomnim c5ivs Amamc asec (lb) 50 E7ter ?vtaaerial: Type Siliea sand Amaunt nsed (]b) 400 Saeea: Type PvC Slot S've .010 Leagrh SO' Diamatw Z' &emazlcs• Temvorarv msdladon Compkrcd 6y: sRa 1 NTE RTEC kQI tJoiaue Well Number NA . . Monitoring Well FieId Data Sheet ient Dakota Councv Project Numher C= 95-0'T= C'itylStatz Eaean. NIN sll ,yumea pZ.Z Wei1 Lacadao See sire man Dam of 7asm11a6on 10.I0-95 ew MR/GS Geoia3?t RF ckw(± 01•) 201 0 02 Riser Pice 798.33' :_ 0.01'w/0 cao) vadon (- ound Suriace Mevanon 796.3' 0.1') oroximare deorh ro warcr icstailauon 5' 'nre oroximate dep[h ra x warer encouarered ariiliag S' orh m Top gi Seal Surface orh m Bovnm of Sea! 3' odi m Too of Sceen " orh a Boaom of Sazm IS' orh m Bounm of Saring 15' rhad ui advanee.: A :{ I.D. I tia^ i,n" I.D. cone O.D. Proacuve Caver: ? Type: None Len3dx: Lack No. Vone Cancres Suriace Sesi: Yes _ Yo GmatA6ova SeaL• Neac Cemeac Gmuc Benmcim Seat Othar Nane Ruer P'ipe' Type PVC Diamerer 2' Tool LoagGt T Secdoat used 1 Couoliags No Cm Yes X No satiIuateria: Type Benmeure oellea Amouat used (!b) F?lter Starerial: Type Silica saad Amaua[ used (ib) 400 Saeen: Type P`/C SIot Sixe .010 Leagrh l0• Diamerer ?" - - Remarks: Tamoorsv asrailaaon Comnlered by: BRAU N" INTERTEC U. _:..",vsor=' 0 ?'=-', 1 - MIIN IImque . . Well Numbei YA . Vapor iMonitoring Weil Fieid Data Sheet ; pbj?C Kumbc C'CG95?77L City/5= Eaean 'tiIId "l0O7 pare af tnsmiladon 10.i1-95 W_I WeII LxsCmn See si¢ mao L Geologisc RF ?e NA It'w/a eaQ) aeyadou 821.1' nw m warrs 3 . a D- evth m >uuroted None proreecve Cavc - Typc ? LeagN: _ (.odc Yo• - Canccere Siaiaee Sesi: Yes - No .f Grauc .1Yove Sn(: Nnc C:meac Gmuc Beammte Se:t! Bmmm¢ 2auc Other Riser Proe: Type Diamexr Tod Lenr,th Sernvvs used Cawun;s Ga PVC ?- i? 2 Ya X Va Seat Hsrecial: Type 3emmmm alvea Amomt nsed (lh) 25 F1mr Mauriai: Type S?ica sand Amovat 'Jaed (Db) 100 Ii Seai 4 .31 m of Seal % uf Scua 10' Saeen: Type YVC Slot Sim .010 [=gry t0' Diamemr 2" gema'ss: 1 aonrh rosnilaunu I i ? i i I 1 t ; ? ?T ? ? ? . T . i t s ? am oi Sceen ?0' am or 30ring Z' LD. 4 i/d" ? I.D. O.D. COmpYeed hy: B.aauN9 INTERTEC =or=.: m Appendix B Laboratory Reports B RAI! N'" INTERTEC October 27, 1995 l&. Pat Terhaar/MIi Braun Incerrec Corporarion Re: Dakora Councy 154 Lone Oak Road BnKm bdwt? cqmmtj? 6e75 was,cmjm a?m smdh P.O. Baac 29108 MhUMOPOU4 ,wrm= 5sA39,010e 612•9a]s600 rme9azesaa CxV? mid Sdmmm Sa.ing du duitr mid Nonrrd fnvuonmene Projax OIBX-95-0722 Report 95-3282 Bnua Intertec Corporatioa received your analy[icai mquac on Ocsober 16, 1995. Analyacal resujts yn enmmarizwi pII tlle fo110wIIIg 1ao0i3tory IepOrt. Routine Braua Inte:tec Comoration QA/QC was followed. Qualiry conanl daca have beea reviewed. No anomalies were encountered in the aaalysis oi this sampie. We apnreciaze the oppornuriry ro mee: your analydcal needs. If you have any ques[ioas or acd addirionalinTormadoa, please call Barbara ?bfala at 612-942-4820. Sincaze:y, Sazbaza I. Mald Projecz Manager Attachments Chain of Custady Labordtory Results -3_ Dalon Coucry .?; 9532ffi _a Ymober. C.`MX-95-0722 tS: Air Tuba vmple ID: 953282-01 .ic Sample ID/DaciPtioa% Vmc Wdl Labontor7: La6 Conta.xfPhanc Sampdee: % 14oisnac IMDLI RI.: Bnun IarcRC Cocponcon B. MAio1611--942-ffi0 Bra'm t¢¢ns Noc Applncahla methOd DCRiS06 f.GY1C RqwmnB r ;m.. mcesmplea: iawss AateBerri+ed: 101I6195 ?ate Bepocted: 10lZ1195 P!%SC t p=ad Ertrra Aw17sis Ami7m DiLud°° CamPUwd Mestrod Date Meshod Date Facsor iYIDL RT. Sample Rcdt kr-qlyw _ NIOSH 10/17l93 1 0.10 0_30 <0.30 ppm :one . NIp$fi lNl7/95 l 0.07 0.07 <0.07 pQm t`Q - NIOSH 10117195 1 0.03 0.05 <0.05 ppm t+.xlosolve ' ? _ NIOSH I0117I95 1 0.04 0.04 <0.04 ppm isoive l.ceax ' _ Mpgl 10117195 I 0.05 0.05 <3.95 ppm macz'ne . NIOSH I0117f95 1 0.05 0.05 <0.O5 ppm `Mmaa - MOSFI I0117195 1 0.12 0_:2 <0.12 Qpm ."01 ? . PlIOSH 10117/95 I 0.06 0.06 <0.06 Qpm 't iC°ctm - - NIOSH !0117195 1 0.05 0.03 <0.05 ppm „-`m:e° ,aosx iorvrss i 0.07 o.m <n.m pl= MOSEi 10117193 I 0.09 0.09 <0.09 ppm HIOSH 1071i/9S 1 0.06 OA6 <0.06 Qpm „vi _thYl ?? - ' ilIOSH 10111l95 t 0.06 0.06 <9.06 ppm -Yi :Somuy1 Kamne ' - TIIpSH 10117195 I 0A6 0.06 <9.06 ppm nv _: echlardc - - Mp51i 10117l95 l 0.05 0.0.5 c9.45 ppm +7IOSA 10117195 I 0.03 0.03 <9.03 ppm - • :llOSfi 10l17195 1 0.07 0.07 <0.07 ppm =vamtiuaa ? . N[p$f3 10/17193 1 0.06 4.06 <0.06 ppM ?as u Gasoiine - v 3Y VIOSH ' 10l17/93 1 L3 1.4 <1.4 G 1 4 ppm m .l YYC[OCI[OOIIS ]S NIOCrdI SQIIIC • ? MQSH to/17193 1 1.4 1.1 . PP L xvdrocurbons yS Nepyzba - - MOSFi • NIOSH 017195 I0117195 1 I 1.4 0.06 Ls 0.04 <3.4 <0.04 ppm ppm :. -xnlometbw Y[OSH I01I?!93 I 0.06 0.04 <0.04 ppm - - NIOSEI 30117193 I 0?6 0.26 <0.26 ppm Tomt (Fnd of RepocU i 7 . S 't 1 ,. , ' ? ' ' "I ? t' l_/L •, , ' I --- - - -? -_ -- ?- --- ----..--------- --- - ? H?ii, i e tly; Dale Tlme Recelved By: RellnqulsbeJ 9y: Dala T4ne ReceWed By: Rclinquislied By: Oale Tlma Received for lzborolory By: , oi? Datles Time•a3 CommeNS: lioum lulcilec Cniporallon, luc 6875 Washlnplon Avenue, Shlppinn and flecelvlnn, Mlnneapolis, MN 65439 Form No. Clalm 1/85 B RA!! N° INTERTEC Navember 7, 1995 Ms. Pac TerhaarlMIi graun Incertec CorQorarion Re: Dakota CoUMy 1534 Lone Oaic Road B'vun Inlerlee Carpermion 6275 washingron Avenue Sowh P.O. Box 19108 MinnaapoGs, Minnmaa SSd394108 61244S600 Fmc9d2-48dd E+gineers wd Sdannm Serviig :he BuiG and NMnud &n+ronmanb' Project C.b1xY-95-0i?? Report 95-3233 graun In[ezsec CorQoradon received your analydcal reaurst oa Ocmoer 11, 1995. Ana(yrical resui[s ara samm?^'ed on che following taborawry repoa. Rouriae Braun Inter= Comorarion QrVQC was rollowed. Quaiicy con[rol dara have bcea reviewed. We xppreciace the oopommiry co meet your analyrical nee°ds. If you have any auesrions or ne? addirional iniormacion, ple:+se call Bazbam Maki az 612-9424320. Sincerely, aarbara r. Maki Projec: Manager ; ? ; Attyc'sneau Chain of C:utody Laboratory Resulcs aimc Dakon Comry uboracom• Brum Lasnx corPonuou Luq-in: 95 -J'273 Iab CaorrcdPhanc B. Yfaiol612-942-4820 ProjectNuta6er: C.1=-95-07Z2 Sampier. BrnmSnam¢e W¢u: Salid ,S Jioiaiac NotApptioble Lzb Sample ID: 95-1233-01 MDL• Memod De¢mua Limit . BL: ReQorring Limit Qenc Sam41e ID/Desaption: Wass C.omPasis LO' . Ex¢art Faaaa Amlyais Aml7sis DOutlo¢ Ccmpomd Meshud Due Mahod Date Faeu bIDL RL Mmis Da[e Sampled: (0/I ll95 Date Reedsed: 101I1195 DateRepoted: 11/07/95 Page: 1 Sample Resuit ? ? Sa 92 Sa Atsenic,Tami - - SW4466010 10lZO/95 5 2 10 ZS mglkq 9armm. Tont - • SW-M 6010 1020I95 5 1.0 5.0 540 mg/kg r,dm..m.Tonl - - SW-8465010 10lI0I95 S 1 5 60 mg/kg Cuomium. Toal - - SW-8466010 102W95 S 030 23 16 mglkg tl^d Tod - - SW-9466010 10l10195 5 13 7.5 1600 mg/kg Neccsry,Tad - - SW-3467471 1M_0/95 I 0.01 0.01 <0_01 mglkg Selevum. Tanl • - SW4l4G 6010 10l10l95 5 3.0 IS <15 mg/kg Siiver,Tonl • - SW-84677G0 10719195 1 3: 1.2 12 mg/kg ltiaauooy ?sbesms • - PL*.t 10/38195 I • - - ga The m?orang limu (RL) was ?uM. A daueoe oi `he sium.ple was necemey duc m cou¢sx ia¢:re:eaces. ¢ Vo asocsms dexcttd. ga K (Aeoort conumted on nezi page) Cueat Daka¢ Counry Ga4-ia: 95-5233 ?rajecc;fumher. 0WCfA5-0722 Nnvnc Solid ah Smple ID: 95-3233-02 Climt Sample ID/Descippon: Vmt Weil Rubbec ZO' labantoi7: BcuminemcCacporsdoa Lab Canraulphonm S. MaYi/612-442-i82p samWm- ° Bnun [oxcxc ?6 "Vfaisnac No[Appli=ble 'N'IDL• Med6od Decdun Lim¢ RS" PCPOzfmB r ;m:. Extraa Emnct Ana11m ,1mlYSit Di1Woo CamPomd il4ahod Date Heshod Date Factor lIDL RL D'+k S2mPled: 10/11/95 DateRecei+ad: l0/lI/95 Dat° Reported- 11107195 Pa4c 2 `rtetats ' Atsema. Totai 3ariwa ?oai 547-846 $010 102ql95 S 2 IO 32 mgft z . C_acmuat i oa! - - SW446 6010 102Dl95 5 I.0 3.0 1600 mg/kq 9 ' p . . :::m mwm. Toral ' ' ' SW$46 6010 - 10l20195 5 1 3 ?p ?? p 'omi . SW-8a660t0 (0l20/95 5 0.50 :.S S m)kg 3a SVV-846 6010 1020l95 S IS 7.5 440p mg/yq p . SG:TiN, TOd - - SW-8a6 7471 1p/20195 1 0.01 0.01 <p.Qj mgft •;vet raw - sw-aa66oio iazoros s 3.0 is <is mgAcg J 92 . - • sw446 nbo iaivros i 1.2 iz <i , mgiks ticr¢sm49 O9n05 PL*.t SO/18/95 I ' ' ' - ? 'he :evoctmq timu (RL) was nued. A d8umn of Ne vmQle was axessary due m matru inxriereeeg, Vo asbams de¢c;,ed. (ltepo[[ conmitted an nexz nage! ]ient: Dal:an Caunry ,ag-in: 95-iZ33 tojed Yumber: C.`A=-95-07L' Lacia Salid ab Sampie ID: 95-3233-03 'Gmt Sampk ID/Dacxiptfoa Vmc WeR 25' 1 •MnW7: Bnun Iotarns Caryondaa Lap ('..nr+...m... .... .B. S1aW612-942-1820 Sampier: Brarm r"m^^^ ^6 Jtoisn¢c No[ Applin6ie MDL• Nedad De¢coon t3mic RL: ReQOoma6 Liuit DateSampled: 101IU95 Uue Recd+ed: IQllll9S Da[e Reported: Ill07I95 Pnv-- 3 F.ZGRC! $2ti'dCL ACalTffi Amif56 MIm06 Cumpoimd blehod Date Hathod Date Faaor bIDL RL Sample Rci 'olatlle Or^anic Comuaunds - cexne SW4465030 10116I95 ;.mH4bbA 10lI6/95 L SA 5.0 <5.0 mgllcg Ityl CSIorMe SW466 5030 10/I6l95 SIDH 466A 10/16195 1 0.1 0.1 <0.1 mglkq enme sw-ans saso 10116/95 ,rma 466A 1011&95 1 a.M 0.03 <0.03 mVU iomabeme¢e SW4465030 I0116195 AIDH4b6A I0116I95 t 0.1 0.1 <0.I mglkg umochlommethane SW446 5030 10116195 JfUH 466A 10116195 I 0.1 0.1 <0.1 mg(Yg amadichioromet6aoe SW40 5030 10116195 MDH466A 10116195 1 0.1 0.: <0.1 mvJYg vmoiorm SP!-846 5030 I01I6l95 SIDH 466A 10116195 1 0.1 0.1 <0.1 mqlkg umomerhwe SW4465030 10lI6/95 yIDH<6bA t0/I6l95 I 0.1 0.1 <9.1 mg/1g Burylbecacne SW-3465030 10116195 bIDHa6fiei 10116/95 t Q.! 0.1 <0.1 mykg c-aarrln«une sw-946 3030 ion6195 rMxas6a 10/16m5 t 0.1 0.1 <o_i mgxg rz-auLrrocnzcnc sw446 s030 ian6195 .rmxa66n 10n6r95 i 0.1 0.1 <a.i mgft uoan Te¢ac'iloride SW-346 5030 10/16I95 NDH 466A 10116195 I 0.1 0.1 <0.1 mg/kq ilom6enzene SW.446:030 10/16195 !ADH466e\ 10116/95 L 0.1 0.1 <0.1 mg(kg ilomdihmmomemane SP/-S46 :030 20/16f95 MDH 466A 10116l95 I 01 0.: <0.1 mg/kg iloroethane SW-846 1030 I0f16195 'vIDH 466A 10/Ifil95 1 01 0.1 <0.1 myYg ilomform SW-846;030 10/16J95 NIDA46fiA I01I6195 1 0_1 0.1 <0.1 mg/kq ilommedhaoc SW-846 5030 I0/16195 ?MA 466A 101I6I95 1 0.5 0.5 <OS mglkg .^.ilommWene SW4465030 10l15l95 XD8466A 10/16195 t 0.1 0.1 <0.1 me,lkg Mlommluene SW-3465030 t0/16l95 MDH<66A 10/16l95 I 0.1 0.1 <0.1 mglYg :-Dibmma-3-CSlomoropane SW4a65030 10116/95 bIDH4b6A I0/16195 L LO 1.0 <I.0 mglkg :-Di6mmaedianc S'N-846 5030 10116I95 3tDA 466e1 10116195 I 4.1 6.1 <0.1 mq/kg bromamechane SPl-346 5030 1011605 MDH 466A 10/16195 I OS 0., <OS mqlkg =-Dicalomoemene SW-846 5030 10116l95 MDH 466A f0116195 L 0.1 0.1 <0.1 mqlkq ,?Oicalombcnzeae SWSC65030 10116195 ?IDFIi6fiA I0116f95 I 0.1 0.1 <0.1 mq/kg :-Dichlorooenzene SW-8a65030 10/16195 .ISDHaG6A 101I6195 I 0.1 0.! <0.1 mg(kg t-Dicttlamemane SW-846 5030 w16/95 MDH 666A I0116195 1 0.1 0.2 <01 mg/kg '.•Oicalomedome SR'4465030 10/16195 11DHa6fiA I01I6/95 1 0.1 0.1 <D.I mqlkg l-Diculamerhylene SW-346 5030 lO/16195 YSDH3b6A 10116v'95 1 0.1 0.1 G0_3 mg/Yg 4=-Dichlortlemylene SW-346m0 ID/16/95 xDH<fi6A 10116l95 1 0.02 0.02 <O.OZ mykg ns-i?-Diciiloeoetltyirne SW446?030 10116195 MDH666A 101I6195 1 0.02 0.02 <0.02 mglkg chlarodifluammedhane SW-846 5030 10/16195 `ADH4GfiA 10/16l95 1 0.1 0.1 <0.1 mykq ctLLamduommeNane SN44fi:030 10116195 ?.IDH466A 10/I6J95 ! 0.1 0.1 <0.1 mg(kg :-Diehlompmpane SW-S455a30 10116195 NDH466A 10116/95 L 0.1 0.1 <0.1 mglkg i-Oichiompmpmc S4J-8465030 101I6l95 YIDA466A 10/16195 1 9.1 0.1 [0.: mqlkg '.-0ichtomoropane SPi-3<65030 10116195 MIDH466r1 10116195 t 0.1 0.1 <0_1 mg/kg :-Oicnlom-l-pfopylene SW-8465030 10116195 MIDEiafi6A 10116195 t 0.1 O.i <O.A mglkg -f.3-Dichlom-l-prooyleoe SW-3465030 IO/l6l95 NDfi46fiA I0116195 ! 0.1 0.1 <0.1 mglkg n:-i,3-Dicnlaro-1-pmpylcnc SW-3465030 1NI6l95 9IDA466A I0116195 1 0.1 0.1 <9.1 mglkg ry1 Benzcae SN-R46 5030 10/16195 MDH 466A 10116195 1 103 0_03 <0.03 mg/Yg ryl Eder SW-846 5030 10116195 NDH 466A 10116195 1 0.1 0.. <0.1 mglkg zacalambuodieae SW-9465030 10116195 MIDHa66A 10116195 1 0.1 0.1 C0.1 mgrkg F f ? F i (Rcporccondoned on neztpage) Climc Dakna Couary Log-in: 95-3273 ?roject iYimher. CvL'LY-95r0TL Na¢ix: Soiid (ab Samole ID: 95-733-03 Q'imt SnmPle ID/Desciptloa Vmt WeR ZS Ubonmrr. _ Lah CowalPhooc SamPler. % Mo bIDL• RS.: Biam In¢ctee Cacpocarion B. Maldl612-942-48Z0 Bcmufn¢cxe YacApplinbk bfeihod De¢ecan Limic Repofm8 I.bmit EMW= a.m?? AnLrm .+mlilysis nmmon Gmpowd Mahod Due J4eWod Dae Fwnr bIDL RI. soomoyibcvena SW446500 INSb195 hIDHa66A I0116i95 isopmpyimiueae SW4146 5030 I01I6195 HIDH 466A 10/I6195 Natlvl E'?hvt Semne SW446 50.30 10/16195 MDH 466A t0J16/95 `4emyl Leaaur/l Kemne SW446 5030 INI6l95 MDH 466A 10I1695 ?rfcnvi -a-jacy gury1 Fjyer SN446 5030 INl6l95 N1DH 466A 10l16193 N=vieae t:Storide SP!446 5030 1011fii95 MDH 466A 1N16/95 Yaon:tuic.: SW446 3030 10/16l95 hIDH dGbA 101I6195 ;.2-ooybemeae SW4465030 10116M MDH466A 10/I6195 SW-8465030 10/16/95 bIDH466A 10116l95 . ? ie?zciilofoed?ane SW-8465030 IO/1CJ95 MDH466A I0l16193 ?_-Teawhlome?ane SW4465030 1011605 FIDHaG6A 10116195 ?e¢?eeiumcyytene SW446 5030 10/16l95 MDH 466A 10/16l95 -?yCmiuim SW4465030 101I6195 N1DHi66A 10/16J95 'aiucste SW446 50.30 I011N95 MDH 466A I0116195 _'.. Tric.lam6enzce SW-M 5030 LO/I6195 MDH 456A 10116195 _ -'nc-.lombenzeae SR'443 =030 10116195 MDH 466A 1N1N95 ..:._-1'ric.lomemane SW41465030 1011605 YIDH166A 10/16195 . ='nc5ioroeCUae SW-846:030 10/16195 MDH 466A 10116195 ...: 'ric:tamediytrne SW-8465030 10II6i95 MDK4SGA 1Q11N95 ':calomdunmmethane SR'446 =030 I0l16i95 J1DFi 466A 10116195 ,^ticalnmpmpane SW4465030 I011605 biDA466h 10/16l95 ":-cmm¢¢lmmethane SW4465030 10/I693 NDH;66A 10116195 ,.:-7rimethylbemme SW4465030 10116i95 NDHJ66A 10116195 ..L.=-^.nmezhvibwuae Sw-M 5030 I0Ii6'95 MDH 466A 10116195 %invlChlande SW446:030 1011605 NDH<66A I0116195 :+.::Sylene SN-8465030 10116r95 MDHaG6A t0/1fil95 ?.'+yie:ro SW446 5030 10/I6i95 MDH 466A 10116195 "naromatic Hydrowruoas (PAHt) (GG'hLS) .,,x=vhtGcnc SW4463540 101i195 SW4468Z70 10117/93 :_:.avnmv?eoe SW446 3540 I0112l95 SW446 8270 10/I1/95 .n,M1nceee - SN4463540 1011195 SW-3468270 10/17193 ::.xom?amhcdcene SW-8463540 10/1195 SW4468270 10117/95 :enzotblftuormtlteae SW4463340 10111195 SW4468270 10117195 :c:aolklfluurandtene SW4463540 I0/1Z195 SW-&468270 10111195 c,mfg.S.Aperyiene SR'4463540 10l12195 SW4468270 10117193 _nzolalpylsne SW446 3540 1011:195 SW4S468170 10117193 rysem 59V-846 3540 1011195 SW446 8270 I0/17195 :i6enm(a.h)auU7nceae SW$46 3540 LO/I7l95 SW466 8270 10/17195 rbc=,,,= sw4as 354a iaivvs sw-sas 827a iaiTros 9u0ranfhene SW446 3540 INl'195 SW446 SZ70 10/17195 ?uoi,cw sw-sas asao 10117J95 sw-aas ano 1011:19s ieem(1.2.7?d)PYrtne SW-W 3340 10117195 SW4468270 10l17195 Date Sampied: 1N11/93 D'+te Beeelnd: !01I1195 Date Repocted: ll107195 Paga 4 l. 0.1 0.1 <0.1 mg/kq l • 0.1 0.1 <0.1 mg/1cg i os os <o.s mgieg I 0_1 0.1 <0.1 mg/kg 1 0.1 0.1 <0.1 mg/kg 1 LO 1.0 <1.0 mq/1g ( 0.1 0.1 <9.1 mg/kg I 0.1 0.1 <0.1 mgfkg t 0.1 0.1 <0.1 mvkg 1 0.1 0.1 <0.1 mg/kg L 0.1 0.1 C0.1 mgJkg I 0.1 0.1 <0.1 mglkg 1 OS OS <0.5 mg/kq 1 0.03 0.03 <0.03 mgifcg 1 0.1 0.1 <0.1 mg/kq 1 0.1 0.1 <0.1 mykg t 0.1 0.1 <0.1 mVloj I 0.1 0.1 <0.1 mg/kq 1 0.95 0.05 <0.05 mqikg I 0.1 0.1 <0.1 mg/Icq l 0.1 4.1 <0.1 mg/kq 1 0.1 0.1 <0.1 mg/kg 1 0.1 0.1 <0.1 mg/kfj i 0.1 0.1 <n.i myxq 1 0.1 0.1 <0.1 mgtkg 1 0.03 0.03 <0.03 mgikg 1 0.03 0.03 <9.03 mg/kg 1 0.33 0.33 <0.33 mqlkq I 0.33 0.13 <0.33 mg/fcg 1 0.33 0.33 <0.33 mykq 1 0 a3 0.33 <0.33 mgekg 1 0.33 D..i3 <0.33 mg1Yg 1 0.33 0.33 <0.33 mg/1cg I 0.33 033 <0.33 mqikg t 0.33 0.33 <0.33 mgrkq 1 0J3 0.33 <9.33 mglkg 1 O..i3 0.33 <0.33 mykq I O..i3 0.13 <0.33 myYq 1 0.33 0.33 <0.33 mglkg t 0.13 0.33 <0.33 mglkg I 0.33 0.33 <0.33 mv4g (Rmort com-rd oa nezc page) ' Dakoa Caunry , -im 95-3233 ? Ntm6er: C?OLYAS-072Z Bram fmRe Crnpucdau Z-1820 Date SMUPLed- ? $? ? Da[eB iai iros SamQle ID: 95-3273-03 T' HOtlamr= NotApQliayl¢ D-u° RP"ted- IL07195 AIDL• MerAod Demepo¢ Lak RI'° 1tq OCCn4 r .:• u sm? IDm?;Ptl,n: vmt ww zs Compoimd 3tetLad Dace Sl h et od Due FaCar SIDL HL SIRMpfe Re+ott hylnaphdalene tw°„` SW-445 3540 10/12l93 SW-W gZ7p 10/t7/93 I °t?""` sw-aaa aseo iatv9s sw-aae azm ian/ns t: a o? <o?-? mgft ' sw-aae ssaa ' 10112(95 swaw szm ia17iss i n ? °-? <o..,; ? SK -8d6 3540 10/12J95 SW-W gZ7p IN17195 1 _ 033 In <D.T mVkq . 033 <O.:u' m4lkY mi.VOlauie Surtogaxs ? m6iphevyl °?°a? SW-8463540 IO/12195 SW-846 nyldl4 SW?A6iSC0 1W12l95 SWa46? 1WI7/95 1 ' T? : iec sw-aae ;seo 10/ 17J95 sw-aas az7o 10/17iys i _ - so %?x 98 .? : Tomi . Tomi SW-8466010 10/10195 1 2 m.'faul ? ' sw-846 6010 10/I9195 ( [ 2 I D 6 mvk4 wn. Tomi - SW-8466010 10/i9/95 t O . '? mvkg oa • I aq/ 4 SK`-8466010 IW1995 I ?S ?'? 6.8 ?kq . Tao1 <13 my7cg i. Tomi - ' SW-946 7471 10lI0/95 1 0A1 0 01 'om! ' ' SW-34660f0 1WI9/95 1 3_0 . 0 <0.01 ag/Icq - SN-846 7760 10119195 1 1.2 ?. <3.0 yg?k4 <12 yq/gq i i { i i i f (Repua coa=ed on neu oage) .0e-in: uakoca counry -njecz Ytmber: 95-3737 C,yp?,y_95-OT? :airsx: Labanden' I?6 Canta ip Bm?c hm= -•o S?+mple ID: 5 UqUid 3273-0a e ? ?Wa: ? S B. N.sl d/ 61?.gy???n Br2UII hXU . SluistIDt 3IDL• I = `YOLaPPi+abk 1mc SamWe ID/Da?py?o; PZ-1 R` q bterhad L'm"¢ ? ° Limc °2hs20PIed: ta11ro5 !0/I!/95 ? I3/07/95 phS'c 6 .,a ' Campouod Fmft"res E,=_ MetLad Dm ? Aaa1? D?Dt' o F? NAL 7u, 'w?Q O?Eanie Campo? 3am* R=att ?:mne iyi CSlor?de SW-846 5030 :nzm 10/171vs nma 40E taniss i ' SW-W ' =benz=, ?'-smo iaivss Mnr?a6se ? imi7?s ?mochlofomedune ?-846 SQ30 1010/17/95 /17f95 ?? ?E IO/17?95 ? 1.0 I,0 I p 0°? ?'-846 5030 IO/17/93 ?q ?? 10/I7/95 I f.0 1.0 <I.0 , ,maaicaloromemane ?H'?45E f0/17193 1 lA 1'0 <I.p ? :maronn SW-34650.30 10/I7N5 1.0 C1.0 w :?+omeau?e SW-84650.30 !0/17/95 ?H?? IN17/95 ? u?yl6en:ene SW-946S030 fWI?/93 ?x? lN17/95 0'3 ?? <0.7 ? 'durylbenzene ?-8a6 5?0 10/I7195 ?? ? IN17N5 1 0-5 OS -846 30.;0 I S.? S.0 465E lN G0.3 ? 10/17/95 1N17/95 I 1.0 1.0 <5.0 ug/I ,on duryl6eveoe ^ ?H17/95 1 L <IA uy[ ecae'?londe ?'-8465030 1WS7N5 O I.0 <I p sw-aaesa3o iav?s ?Aia1zms ? i ?roaiummome?hane ?'-8465030 10/I7/93 ?H? I0/17/95 I LO LO <I.0 uy7 '??aune SR+'8465030 1N17195 ?11 4M 10/17195 1 1.7 1.7 <1.7 SR'-8a65030 t0/17/95 ?H? t0/I7/95 l is ?•0 <I.0 ?i mromn uqr? H465E IN(i195 I !.0 m'newne SW-8465030 10/17195 ?5 cl_p yl ?roroluene SRC8d65030 10/17195 ?H? !.0 10117/95 ! l:romlmne SW-946j030 10/17/95 ?9 46M 10/17/93 1 1.5 (S <IS 'Om MDH cro m-eromPmpane SW_8a6 5030 LO/17/95 JDH 4? !0/I ? 1 t ? ip 0 1 ?? .0 <<.;.0 '0 u4R ? nomersftan, SW-846.030 f0/I7N3 YIDH4?7g 10/I7195 <10 tcq/I .vorooy.??,- ??o iaii?s i px ? 1at7ros i s o 5= <o ??t stv c -?soio ioii ?s xDqa ia?ros ? °s ? j ?o ? ? alome 17/9s ?3/t ilaroe 1 0-2 <IS ?? ?lene ?'-346 SQ30 !0/17/95 JiDHa65E IO/17/95 I 1.0 00 <OS ?1 ? 10/17195 ;6{pg,?E 1 <ZO ? -Dic.?lomethylene -8465030 IO/I7/95 10/I7I95 1 ?:? 0.3 <0.3 ? 3W-346:030 !0/17/95 y1p$ ?E 10/17/95 I 0 ? 0.2 <9D °g/1 fifluamme?e '? t0/l7/g5 f 0; 0.2 ' luommethanc ?'-3465030 10/17/9-1 ?1 o'omonane ?'-846 5030 10/17I93 y?mg ? 10lI7195 ? 5.0 5-0 ?pY ?? "MMff o'oomPsue SW-8a6 5030 10/I7193 lIDA ? 10l17/9S 1 SA ?'-3465030 10/17/95 ? IN17/95 j 1.0 lA <7 p ?l M'1-Propyfene ' ND$d6,55 I0/17/95 1 1.0 I'0 <IA 1? . 1.0 10/17/95 -0cQlo`v_pPmi=me ?-030 1W17/95 SlD8'Q7p 1W17/95 1 0-5 0-5 <03 u? iai7?s ?H,? ?anr?s 1 os os ?? Usn -5030 ?'xa? sosa ion;?s i - madiene 465E tmry7/95 ? [A LO <IO ?j ?'-8C65030 !0/I7/95 !A LO <I.0 'vf MDH 465g 10/17195 1 1.0 1.0 <i_0 vyl (lteaort mnnm?ed on nexc p'qU i ? ? Y : r 1 f { 3 ? i i ! { : i pairon CouncY 95-i2ri c Nw?? ?-95-0722 am4k ID= 95-3237-04 : SamPk ID/D's°zFnoc ?Z'1 ComPuuad mpylbenmm ,npylmluwe ayl E3ty1 Kemnc hYl isoouryl Xemne 'hyl Te:dary BucYI Ether thylce C'slocide cndmiella rropyiyeazeae 'Rm l.l'-Te.raeldom F'^" : :.^_-T?y?omahane :mciilomedryle°e srmnydmiiuan oluaw ..3-Tric^domhenzgnl ?.s-iriezlombe •"s ..1.1-Tdcloroeduu? n Tncalometbaee ....? :rie?tomedrylene ?ricdWmduarom??° ,: .?-TncalumomPane i nc.No comiluo[oetheM :?.LTntne&YibenzpO -rimeshY ibenu= w¢yl C!71ande a,;-;[Ytene o-Xyicnc gpLC .1nalYm ,??oy?halme .accuaBhthene .aamracem denzn(a1a°??° , 3enzulblfluorauthe+u aapylk)fluoiandiem 3aao(B.h.i)PnYleae ' 3enm(a1PYm1e C?yseae 7 itaao( a.h)mdttdceae riuoramhem ;suoie7m ?(l; .3cdiPYmnc j-HtthYlmoudai^au acmn Snx= CO`ppjpOE MWb12A42-t820 B . 9aua In¢?e SamN? Not App??1O °6 Mn? . Mnycd Daecnou limic ?t^ RProg Limix RI.: ZZMAa g3=ad Yfethod ?t° ? Ytdhad D°t° Facor bIDL ?' ? ? 10I17795 gp/$a65030 10117193 JDHafiSE I0I11195 ?Mx 4656 SW-W 5030 10I17195 10/17195 yq/$46 5630 10f17195 MDH ? 10l11195 ?? yy,r.gqb 5030 1N17195 SW-W Spgp 10117195 MIDx ? me aesE . 10l17195 iai7ros , sw-sas 5030 imvms SWA4b 5030 10l17195 y1D8 ? IDEJ 465E ? 10I17l95 10117195 , gy/$46 5630 10l17195 10111195 ,1dDH "SE 1d17195 yW$a6 5030 Sy.946 5030 10117195 l'DII 46SE ?x assE 10/17195 ?ai?r?s sw.sas soso ion7r9s gp/A46 5030 iavros ?,rox Asss ?IDH ? iat?ros 1at7195 ?? gpg0 10l17195 NOA 465E l0l17195 LOfI7195 SW-946 5030 Sp/4a6 :030 10l11195 Y1DH ?E 10117195 IOllil95 SW?846 5030 (Nl7l95 Sryy$a6 5030 10111195 `dDH 465B yfDH 465E 10/11195 10117195 yry/_ga6 5030 10117195 10117195 yIDH 465B 10111N5 Sryy446 5030 SW$a6c030 LOllif95 .'?x ?E >tDH'f6? 10/11N5 10117195 ? -030 L0119195 ? 10117195 MDH 46% l0l17195 5 p/?ga6 5030 g y?$q( :030 I0IIi195 y1DH ?14SE `?x 4? lO11T19 t0It7/95 gqr.Sa6 5030 10117195 sw,g46 S030 10f11195 NOx 465E `tDH 465E 10117195 10117195 SW4" 5030 10717195 lOft9/95 MDH 465E 10117195 yryy.ga6:030 EpA 610 :OR=m LOf'3/95 r.?A 610 =?A 610 EPA 610 10R5J95 FR+? 610 EpA 610 1Of35195 B4 610 Epp fi10 I00195 EpA 610 ppA 610 F3A 610 IOI13I95 I01,795 EpP' 610 FpA 610 ppp 610 lOfL5195 r'P4 610 gpp 610 ? EPA 610 E?4 610 iQ??? A 610 gpA 610 10fLS195 10(]5195 c"PA 610 e?A 610 FpA 610 EPA 610 1011=195 FPA 610 !k 610 "D VA 610 lOf7Sl95 e - M? SIMV"& 101tI195 Dale Recu.e& iaiu9s Date It*Ort`d6 lLU7195 Pa%C 7 5.Mpie Aedt 0 1 <I.0 ? 1 t_p . 0 <3-0 ugn 1- 1.0 5 n? c5.0 1 5 p 0 5 <3.0 WA 1 . <1_0 41 1 1.0 5 Q <5.0 ?L 1 5'? 1 0 <1.0 uei 1.0 . ? l p 0 1 <1 0 u&" 1 . °S <OS nHft 1 °S 1 <12 u4?i ? o i <1.0 uN" t t.o . 5 0 <s.o uv1 1 5.0 . 10 41.0 uBil 1 40 0 1 < :_p uyl 1 t.0 . <1.0 a?l t ?-4 ?p <_.D u&t I ?? 1 2 <1_ u411 1 . OS <O.S uvi I 0.5 <1.0 uv1 5 Q <5.0 u31, 1 SA n4?1 1.0 < 1 ? ? i ? 1.0 uvJt < L <1.0 u4il 1 1.0 ? Q <1.0 uP/i ? 0 I <1.0 ?i 1 10 . 11/02195 t1102195 11IwS ll/OZJ95 11/02195 11102195 (1f02195 1107193 t1f4Q195 11/p2795 ll/4?!95 11101195 11102195 lllO7J95 11 <1.1 ?1 1 1.1 0 2 <ZO aBfl 1 ?.0 . 4 0 <S.0 u4ri ? a ° . o a <n.sa oe+? l 0?0 0 14 40.14 n4« 1 0.14 . I 0.01 0.01 <0•01 19 <0 uwl W 1 019 0.19 . 10 <0 ?1 1 0.10 OSO . <20 aPJl i 2.0 Q p <0.10 uYJ, 1 0.10 ' 1 0.70 0.30 10 <0 uBJI t Q lp 0.10 . 14 10 ?i t 14 0 ? 1 . 0 <5 uBli 1 5.0 0 . ?g?port conawed oa nexe P24o) s Iaboramr}: B"uu fnceaxc Corponco¢ Dakom CaumY Uh ComaclPbonm 1. Na1d612-942-420 954233 c SsmPl Bfa?clnxRc I,mmber. C,f.'IX'95 ' 4, Yfaistmc NocAppGnble Liquid ?y. yfe?od De¢eaon lim¢ ple ID: 95-3733-04 xy. (iepotdng Limic implnIDlDacriptlon: PZ•I - d Ana17a? Extract Ddutlon A?I7? Extr2 ryktyod Data Sintrad Dnte Faanr YIDL RL Campound EPA 610 IOl71195 EPA 610 ilf0'Lf95 l, 5.0 13 5.0 3 1 inacsttuiene ?'3A 610 10f25193 F3A 610 11101193 1 - 12 . 12 tene IM= c'PA 610 1025195 EPA 610 13l02l93 1 11103195 1 0.40 0.40 EPA610 IOlZ5l95 EPA610 was uaaemd guc the EPA t meommeodd haidin6 um e temaris This samP +c _ E+A JiO.IA 10117195 4 IO ? Y. ioOi FpA375A 10117195 1 10 10 . _ QA 76.1 10118195 l 0•40 0•40 Iacl 9 EP.4 730.1 10119195 1 0.01 0.01 x. .?mmowa . _ EPA i531 IO/IJ95 I 0.02 0.02 :. Vi¢ue - FPA:00.'1 10117195 5 50 200 'ural ?p:00.7 10/36195 I 10 10 . 'ud `q:pp,7 I0116195 1 IO 10 z. ro? ' _ ?.a:oo,7 iaicros i io io ?m. 'uai ?q ?qpg 10/19195 5 1.0 5.0 .2. :?C33I[t Uq.pp.7 10116195 I 30 30 '=i ? pA=aS_i L020195 1 0? OZ T EP.4200.7 10/17/95 1 200 300 Taol an. ?q:pp.7 10/16195 1 :0 50 ca. Tool EYA 200.7 INl6l95 1 ?D Z? 'aml - ' EPA?OQ.'1 IN17195 1 300 300 i.:'ont ?,q?p01 LO/i2195 1 50 =0 j - ...°A.00.7 10112l95 1 [0 LO ssolved . - - EPA aoo.7 tawvs i to io ym. Dissoi.ea . E''A-00.7 10117J95 I IZ 12 :w:i. ?oal Disso(ved . - - .PA3011.7 1W19J95 1 30 30 Diuolvcd E°A 245.1 10l14l95 I 0.2 0.2 ry.'.?.issoWed Eep?p0,7 I0112195 t 50 SO im. ?issolved ' _ ppZpp.1 10112195 l 10 l0 Dissatved Te m?o[anB Iimu (RL) was miscd. A dilunoa ai tl7e aama?e was nmesmcY due w mamx intesiexeac s. aoalY¢. ': he :e?oma4 limu (RL) '? ?- .'? dilunon or ihc ssmple was necessaxY due whi6b C0?OII6?0? ot rhis DaasaceMed: Iaiuvs Daze Aeceired: 10/IL95 7)ate Repocmd: ILOTNS P]$C 9 Sampie Rcsnlt <5.0 ag!! <1.3 oglt <!Z ugft <0.40 ugll 450 mgll 49 mgll 1.4 mgll 0.03 mgll Ll m8ll 130 uBII 1400 ugft <10 ugll 7!0 ugft 1500 mgfrqll 120 LLgll Lfi ugfl 1i000 u4R <50 uglt <20 ugfl 27000 ug/l <:0 ug/1 59 u811 <10 uSll <iz Ugii <;0 ugfl 0.3 uq/l <50 ugll <10 ug/l gb ga gb (RcPon conmucd on am P26c) i 'rsc: Dakon Caumy . . 95-5233 ject Numher: C.`.AX-95-07?2 L'+quid ampia ID: 95-3733-05 . Samp(a IDlDesaipuoa: PZ-Z iaboramcy: LS.. Iay [',,...,.cLm,,,= Sampiec: 4. ltoishac 6IDL- RL: Booa lnou¢e Corpondan B. Malo/611-9e2-s820 Brm ioaecae Na[ Appliohle MedaC Deacdon I.ink RepordnB Liwk pate Snmpicd: 10/11195 o-ue Recei.ea: t0111/95 pate Repor[ed: L1107193 Page: 9 Ez=ct Esmad anal7js AnaflsLt Dftdo° Compound " yiedwd Due Mnhod Date Faaor JDL BL Sampk Reml[ roiatlle OrTacdc Campowds sw-aas 5030 10/17195 MUH assE 10f 17r95 i sn su <so nn kcMMW SW4465030 10117I95 NWH 46SE 10/17195 1 1.0 1.0 <1.0 ag/I wYl chiorkda sw-aas smo 10/17195 MDs asse ianM i 1.0 i_o <i_o uvi levte= sw4as smo iavrvs MDH essE i0117195 i 1.0 1.0 <i.o oan immob„neez: immochbo,omn.h,,,e sw-sassmo 10117195 r.msasse iavros i 1.0 i.o <i.o uvn / Iromxficbia?mdmm y'tK8461030 10/17195 bIDH465E 30117193 7 95 t i 03 os 03 os 1S <as ugAJ ugrt lmm,fb,,,, n sw-sas;oso $W-8465030 lanrss I0137195 NmHasss MIDH465E 10n 1 10117195 I 5.0 SA <5.0 ag/I ?mtoo,,,,. wn sw-sae smo 10/17195 MDH aese tmnrvs i i.o c.o <i.o ugri Ia„ryibcm=-x sw-846 5030 10117193 r.mx asss 10117195 i 1.0 1.0 <i.o asn vaatrymeftzene eR-auryixettene sw-saa 5030 iavms INCx aess ia17195 i 1.0 7 i.o 1 7 <i.o 1 <i uvi uyi :?o remic-liforide sw-aas 5030 ianros MDH asss i0117195 i 1. 0 1 . 1 0 . <i o uvi .110,obeom,: - sw-aas 5030 sw-sas smo 10117r95 ia17195 MDH asss eMa assa 10117195 10/17195 i i . z.s . a _ <zs UVi -flo,od;tmmomethaw SW-846 SOiO 10/17I95 MDH 46SE 10117195 1 IA 1.0 <1.0 uvl Mloro..i.m. SW446 5M0 10/17/95 NII7Fi 465E IOl17l95 t IS IS 51 u8l1 ? :Slamiocm SW-846 5030 10/17/95 SIDA 465E iW17195 1 5.0 5.0 <5.0 ug/1 Mlowmemme SW-8465030 10/11/95 yIDH465E I0/17N5 1 lA 1.0 <1.0 vglt :LSlommluer.e . SW4146 5030 10117195 MDH 445E 10I17193 l lA 1.0 <1.0 uqll ?„C .?ommiucu: omo-3Llilaroompane [; Ji6 SW445 5030 I0117J95 MDH d(SE t0/17195 I LO LO <10 ugll - r ;-Di6mmaeaaae SW-8465030 10/I7195 IMIDA465E 10117195 95 I 1 03 0 5 03 0 3 <02 0 <1 ugll ugll Jibmmomedune SW446 5030 SW-846 5030 10/17195 10117195 J1DH 465E bIDH 465E 10117/ 1N17N5 I . 02 . 01 . <0? ug/t l'-Diohiofooeaune r SW4465030 10117195 MDH4GSE 10l17195 l tS IS <I.5 ugli ; Dickdomoentenc SN446 5030 10l17l95 SIDH 465E 10117195 1 OZ 01 <02 uq/I 1_;-Oichlamaetizcne !-0iciiloroc3ume l SW446SIXi0 10/19195 SIDHd65E 10/17N3 I IA 03 LO Oa <1.0 <0 3 ugll ugll . ??Oicylarccdnp? SW-8465030 10117195 MDA465n 10117195 1 IA lA . <1 D ugll 1,1-Jic4lomamylene SW446.U30 SW-84(i 5030 IU117I95 [0/17/95 hmH465E !rIDH 465E 10117193 10lI7f95 1 1 03 02 . <01 ¢gll u-l _-aic5loroetlrylene SW445j030 IO/17195 MDH465fi 10117195 l 03 01 <01 ug/1 tans-1.2•Dic^.lomcmyfeoe DichlomditluoMmedtane SW-846 5030 I0/17193 MDH 465E I0117I95 ( 5.0 SA 5.0 5 0 <S.0 <S D ugtl ugR picaloroduoromemanc SW446 5030 10/17195 16IDH 465E 10/17195 1 L lA . LO . <1 0 - ugll 1: -airbiomoropaae SW-9465030 10/17N5 7195 JiDH465E NIDH465E 10/17195 10/17195 1 lA 1.0 . <1.0 ug/I , SW4465030 SW-8465030 1011 101I7195 SIDH465E 10117195 1 lA LO <LO ugll _0ichlorupmpane 2 l-Dichlo'a-l'ProVYlre l SR'446 50ri0 10/17195 YIDH 465E I0/17195 1 OS S OS 03 <OS <OS ug11 uyl . 3-Oicalom-[-ompyiene cu-i SW-9165030 10117195 MIDHJ65E 10/I7195 1 O OS OS <OS ug/I . aa¢s-1,3-Dicaiom-l-propylene SW-9C65030 10717195 SIDHa65E :0/17l95 1 I lA 0 1 <I 0 ug!! Ethyi gemen: SW4465030 10/17195 hmH<65E 10117195 0 1 . 0 1 . <1 0 ugll cthyl Ether SW-SC6 -`U30 10117195 bmA 46.5E 10l17l95 1 . . . Hezachlomouadiene SW446 5030 10117195 LMIDA 445E 101177/95 1 lA 1.0 <3.0 ugll i ? i ; t 1 t i 1 (Repatt mnamied o¢ nm pagc) Csmt: DaYoia Counry L++4-tn: 95-3233 ?rajeciNumber: C.N7L1'-95-0'12? Ytairc uyuia !?n Sample ID: 95-3733-05 Guienc Sample ID/Daaipttou: PL-Z Coaupowd fsoompylhea+-a• isoorvvylmlume YlectYt EthYl;SeWtw Ne:Ryl Isobvryi Keaoae Ncnyi "emary Buryl Etder 4temywne Cilonde Vaanmalrnc a•2vvy16eamne )NtL:IC . ' : .-TetACh(oc0ethnn? .: Tevachlocoedune C:S3CRI0[OESfIYIE[?C -«remiuraa 'omene ._.J•irichlo?nbepzenc .. -.richtome?Gane .. = :ncYtomefhaae "-.2-:ricalamchyfene ?;.clhloroduofomemaoe ?..._•Tricaiampmpane "'nc?iorocncluo've?ane =?nmerIIylbecaene ._._ -nmeraYl6en¢rne iinvi C.Uoridt . -'-Xvlene -.:yrcne Trsc .wwrm +c=mnhrhakne :cenaonmena r.mrapne :c:.mtajanwracene :=untb)fluorzuNcne :e.va(k)tluosaatheae .ce¢o1g,s.Dperyleae caaiaioyreae .:C/SC.^.C i ceomla.hlamh.•,c.m, ?::oranmeae ?ua[tac .:acnat I,-.3?:d)pyrcnc -.(emYlnaohCtalene L+6onmr7: Hcmn Imccmc Co'ponuoo Oate Sampled; 10l1I195 La6 CaumcUftone: S. Nald/612-9s248ZO Date Reeened: [OfIIl95 Sampier. Hwi¢ L?mc Date Rewtid: Ill07195 % Jlnisp¢c Nat Appli26le JIDL- Mahod Deaction limic M Repormg I,im[ ' PagC 10 F.ztrrct E=la Amy= Amllss Difauon Metlmd Dnts Jlethad Date Faanr ADL SL Sampie gesot[ . SW-846 5Q30 10l17195 MDH 46SE l0117N5 L- LO 1.0 <i.p uq/! SV7445 5030 I0117l95 MIDH 465E 10117195 L- LO 1.0 <LD nq1l sw-aae;asa ianms nmxasss iavPvs L 5.0 5.0 <s.o avi swaw smo tai7195 MDg asss iavM i 5.0 5.0 <s.a uyi SW446 5030 10117195 SIDH 465E 10/17AI5 t 1.0 lA <1_0 agll SW-84G 5030 10117195 NMH 465E 101I7N3 i 5.0 5.0 <5.0 uglf 571-M 5030 10/17195 MDH465E 10/17l95 1 IA (A <1.0 ngil sw-sas saw 10/17195 MDe assa 10117M i 1.0 1.0 <i,o uvi SW-8465030 10117195 J1DH465E 10l17195 l 1.0 1.0 <1.0 uyl swBau $mo 10/1;195 MDx assa 10/17ros i os os <o.s a#i sw-s.w 5030 10/17195 NmR assa ia17195 1 t: 1.2 <IZ oVi sw-sas 5030 iavrvs nmx asss ia17ros i 1.0 E.0 <i.n twi swaas 5030 10117195 Mroa assE iwnros ! 5.0 5.0 <s.o uvn SF'446 5030 30/I7N5 MDH 46SE 10l17195 L lA 1_0 <1.0 ugfl SW-&46 5030 10f17195 bIDH465E I01I7I95 I !A 1.0 <1.0 ug!! N1-4765030 10/17l95 ?vIDH465E 1011995 1 LO 1.0 <1.0 vyl S5V-8465030 (4/I7N5 AMX4SSE 10/17/95 ( ZO 2.0 <2.,0 uy7 SW-8465030 10117195 MDH465E 10117195 1 tZ G1 <1.2 ¢g11 SN-846 5030 10l17195 hII3H 465E 10/11195 1 OS OS <0S uqll SW-846 3030 017/95 NDH 465E 10/17195 1 1.0 1.0 <1.0 ug11 SW-8465030 [0/I7195 bIDAS55E 101I7195 I !A 1.0 <1.0 ugf! SW4465030 10/17195 MDH455E 10/17195 1 - SA 5.0 <5.0 ug/t 5W-8465030 101I7195 NIDHa61F I01I7195 I tA 1.0 <I.0 ugll SW-846:030 10117195 !ADHJfiSE 10l17/95 I f.0 LA <lA ugrt SW-946 5030 IW17195 l.IDH465E 10/17195 ! IA 1.0 <1.0 uvJl S'V$46:030 10/I7195 NDH455E 10/17/95 L 1.0 lA <1.0 ugll sw-aab 5030 canros ame assa 101 17rss 1 1.0 1.0 <i.a ugri E°A 6I0 1025195 EPA 6I0 I1102195 I 1.1 LS <1.1 ug/1 E°A 610 10l25195 EPA 610 1I102195 I ZO 20 <2.0 ug! EPA 610 1025l95 F3A 610 tl/02J95 1 4.0 4.0 <4.0 ugl EPA610 f0/25l95 °3A610 11107195 1 0.j0 0.30 <0.30 uqlt r'3A 610 t0l25195 EPA 610 illO7J95 L 0.14 0.14 <0.14 uqll fPA 610 10/25195 EPA 610 1L01195 1 0.01 0.01 <0.01- uy1 FPA 630 10/2995 EPA 610 11lOZl95 1 0.19 0.19 <0.19 uVl c?A 610 102:l95 EPA 610 11l02l95 1 0.10 0.10 <9.10 uqlI I-3A 610 I02195 EPA 6I0 11/07195 1 Z.0 :.p <ZO agtt FPA 610 IOlLSI95 EPA 610 131OZl95 I 0.10 0.10 <0.10 uyl EPA 6I0 [025145 EPA 610 11107J95 f 030 0.30 <030 uy1 e?A 630 10fl-5195 EPA 610 11102195 L 0.10 0.10 <0.10 ug11 FPA 610 102/95 EPA 610 1U01195 1 0.14 0.14 <0.14 ugll c"PA610 1025195 EPA610 1L02f95 1 5.0 5_0 <5A ugy7 i (Repua romm...A an nex[ page) Dalcoc comry . Li6orawn: , sr,un 1nR.?c cofponaon I?are sampied lawvs mc La6CmnNPhooa B.NaId/612-9424ffi0 DateRemted: 10/iL95 Q.?; 2.43 95-i - SamPier: Brmn Wetrcc Date Reported: 11l07N5 3ject Yimmher. G'A7LY-95472? % bfoiawc Na[ Appticzbk ims_ Liquid '41DI'c b[em°d Dar?on i'.+?'r b Sampin ID: 953233-05 RI.: Reparcin8r;m,* :eat Sample ID/Descriptioa: PZ-2 Es=a Excaa Am17a+ AnWYffi Ddum°° ComPuwd Method Date bf'thad Date IRrcmr bIDL RL Smt de Re olt EPA 610 1025195 EPA 610 11102195 L 5.0 5.0 <5.0 ? 4tedrylnaohWalene EPA 610 tOf25/95 EPA 610 11102/95 1- 1-3 1.3 <1.5 vh?m EpA 610 lOfL5/95 EPA 610 IllOL95 I 12 12 <32 n8n ?? EPA 610 302995 EPA 610 IL07J95 1 0.40 0-40 <0•40 n811 Rm Remarks: This samPk was e.c¢acsd Pas[ du EPA cxommmAed hotding cana. °rpnic ? - EPA 310.1/3 10/17195 b IO 40 410 mgfl Sb {y'niry. ra°i - EPA 3-75.4 I0117195 I IO 10 j-7 m4/1 dfacc , . EPA 376.1 IOI18195 f 0.40 0.40 ? 3 m4/I dHde. Taral urient . g.q's50.1 10119/95 1 0.01 OAt 0.63 mgit iwgea Ammoma _ gp 353,2 ' 10iI2195 1 0.02 0.02 0.11 mg(t iav4ea. Niua¢ ? - EPA 200J I0(17I95 10 :D :00 <500 ug?l rse c. Toml EPA200.7 10/16193 1 10 t0 ? u4J1 UU= ro°? EPA _00.7 I0l16195 l IO l0 <10 uyl ? mmmm - EPA 100.1 10116195 t 10 10 740 n3+1 Smmmm. t'otal - SM _340B 10119195 l0 1.0 10 1900 mqEq/! ?? Calculm ' EPA?00.7 10l16l95 I 30 30 160 uqrl =d. Tod - EPA 245.1 IO/ZO/95 1 01 0? 1.6 ¢g4 ?e:css Tod n E.°A200.7 10/17195 1 200 ?00 21000 ugtl im."Cod )rus - - EPA 300.7 10/I6195 1 50 30 <'M u6<< ;lmntm. Tonl - • - EPA 200•7 10116/95 I 20 20 <-U °vI Iver. Toul EPA 200.7 10It7195 1 300 300 72000 ugtl wium, Total letais _ EPA 290.7 10/12/95 L 50 :0 <:0 ug/t n°°??•D?O??? EPA200.1 10112f95 1 10 10 16 uqtl anum, ?issofved ? II,p 20p,7 10/12l95 1 10 10 < 10 uyl adm?um. ?issoived ? . Fpw 200.7 10112J95 l 12 12 <12 ayt y??n?. ?p?lDiswlved gpA?pp.1 " 10117195 I 30 i0 <=0 uyl caC, ?iuolvea EPA?45.1 IORCf93 1 0.2 0.2 <03 uyl 1e?cury. Dissolvcd ' gpp 200,7 10112195 1 50 50 <50 ?i demum. Dissol?ed gpp 20p_7 10117J95 1 10 10 <10 - aq11 ilver, Dissolved " ga g6 1r i 1 i. ;a The rooomng liavc (RL) vras rused. A diluaon of rhe sample waz necrssazY duc m mamx inmdassscrs. ;v The rsportm8 limss (RL) was rmsed. A dduuon oi Ihe sample was necusazY due m 41311 mneen¢anons at rha anaiY¢. (gepnR cpuOoned o¢ nex[ pa4e) D akaa Counry ?ber, C.LYX 95.4712 4auid 95_,y3-06 aiDa°vtlay. pZ_3 I?b ?tofi; m a- ?O g - ? ya?. p? • M ti c ? ?o 8 a oo 1612-9q ? 8L: 'YIxOPPGo6k ° [,iam R"ru . as CoMMund ? ? d D a ? Arahslt ? =omaovpdq ^d ? ?tion F?or ?Mt ItL SW'846 5030 5030 10/17/93 1 0/17195 ?A 10i17/95 - 5030 !t7/95 'NDH?g 10/17/93 ! ISD SO Dah Date ??.__?0 10111/9S DateRepo? 10/17,95 /95 Nge 12 SamPle ge? le 5030 10/17/95 ?H?E I,/q,s t A 1011719S 11 H I? IQ <.0 U 0 <1 ? t 'uca?sa3o iat;iss y?H idn/gs t i.o ?-9<65030 1 4 . 1,0 1.0 c1.0 ?yi 4n <:A SE 0/t7/9 SF'-8a65030 (0/!7 S NDHq65E lOry7/95 j SN 195 K !0/17/9S 0.3 LO u <I.0 '4?1 4?1 10/17/95 1 '?'-8465030 7010/17/95 /I%95 ?H ' ? 10/17193 t s ? 1.0 1?17lq5 ?'A465030 ? S ? <0.5 ? SR <S 0 1 !0/i7195 SW-8a65030 I0ry7/95 xDFIq65E 1.0 ?-d%s03p j ?H ? ` ?s u . j 0 1.0 <I.D o4R 4/1 <I o p?17i9s W ! 1 tA a17 10/17/9 M-9465030 1 I ' . 0 ' ? 0/17195 , ? j I?1 ?'-a465030 10/17/95 2-5 V! ? ? <I, ? 4R ci t 5030 (p/17J9 1.0 S ?x ?'-aaesoao 1anros ',6? ia17i9s ?H i .0 ? osn ?u 1.0 <: o ?I . Ine SlY'g46 a??r9s ? t 1-5 5030 I0117195 &Mq %SE 10/17/95 t S.0 i.S "'tDHq6yE 10/17/95 SW-U65030 10? 7.6 S I 17/95 .0 unxac? ianros 10 1 I.o <s.n ?i' !0/17195 ?- aa6 5030 <r $ ia??ms .a ?sn i iu i•a ?SO30 3'0;70/t7/95 ?FI'?SE 10 < 1-0 u '-10/17/9 8465p3p <I0 '?MH46 10/17195 SE !0/I795 1 SA'-8465030 10/17/95 ?y?? f0/ 1 S'Z 0.2 '?-d<65030 17195 °? <OZ iai7ros ?q? t 0-2 5.0 10/17/93 ? p? 465E 1a17/95 ? <S.0 o?S7 VI' <0 1 ?? S Wa? 5030 10/17/95 ? q ?E t-S IOii7/95 0-2 !0/i7/q5 ?? '?o ?H? Q .2 <IS 4?1 °3q SE 10/I7/95 ?'-3<6:030 J1DH 46gE !0/17/95 t I.0 1.0 '?''? 5030 I?17/9J ,yID? 101I7/93 0 3/f <1 ? f0/17/9S ?? I 0.3 f0/17/95 ?? 465E lOp7/95 1 01 1.0 ?? S?? .0 a0.3 `? <i ? 10117195 1 0.2 0.2 -8-846 5030 10/17/95 '?1DH465E f0/17/95 0.2 . d6 Sp 3p ?x 0 . <0.2 ?4/1 <OZ , 1?17 ?'8<65030 ?5 ?NDA t?17Ig5 46SE t 5.0 5.0 10/1 ?-aaeso3u ?s ?H s.o 1an?s u? <s ? t t 5.0 an?s &fDH ioinros ? i.a i.o '?u'-a,ssoso °? iai7/ss t.a .o <s.a vvt vr < zain9 i 1.0 ?'-s??o3o ta17ms arnx i.o t.0 SN'g46 3030 3'?IDq q IO/17/95 i.n ? <t.a . D ?i <I 1 6SE 10/17/95 ?x 10/17/95 ?-8465030 !0/!7/95 y?? ?E 10/17/95 1 OS 0.5 '?''?65030 . <D 10/I7/95 ,?.?H `? ?M !0/17/95 I 0.3 0'5 SW'3463030 E 10/i7/g5 1 1.0 0.5 .S „s °?1 <0<0 °q/i 10/17/93 MDH 1 1.0 i ? alug .5 <I.0 U4?1 lpi77/95 1 1.0 <T.0 w u4/t !.0 ct.o avi (RaoaR ?nmmed on neR p29e7 Hco?ice?us CuRo?a Date SamPied: 1011 V95 Daka?a Coucu7' ? ramdQ man B. Maldlfil2-9aZ-4= 10111/95 ed: Itl07N5 DateReP? 95-3233 ?? Hsmnla2xvc ' N,umbec: GVCLC-95-0722 Sd4aismec eablc NaAQpI Li4wd bIDL; Mdwd Drsectma° Lmc mple ID: 933333-06 RL. geQotdag t,^"k Paqg 13 snmpie ID/D'saiption: PZ'; ' , . E:saa Fsaaet ? D1mm Avaom Drte Faaar MDL RL sg.P ? Result Compoimd d mabo ? swaas smo iamros r,ma essE 10117195 i. 1.0 ? o 1.0 ? o <i.o nn ,y??'?° s?v? smo iai7rvs .rwH acss . 1ai7ms 1 • 10117195 1 . 5.0 . SA <s o oe ! t rylmWene Syygqb 5030 10117195 MDB 465E tan?s t 5.0 5.0 <S.0 cg/t i ! E`nYl Kemne y?ar.sas 5030 ianros rm?[ assE i??? 5 MID84CSE IOIIT793 1 LO 1.0 <1.0 ag/l ? I TatduY 9utY1 c'hPz yryy$46:030 gqg Mp Sy 1011719 10117195 btDH 40E 10117195 1 5.0 SA 0 1 <5.0 <1 0 v811 ug/l jme Cbtonde „ SVV-W 5030 10117195 hmH 465E 10l17193 L L 1.0 lA . 1.0 . <3.0 nFJ1 s 't Wenc $9y4q$1030 10l17f95 b1DH4fiSE 10111195 i 1 0 1.0 <i.o ? - . ,yinermadO SW?a65030 10/17/95 bII7H465E iai71vs . T , F S4/-Sa6 5030 lQl11N5 ?H ?E 101 L 0-5 <DS c t_ ug/l uglt ; ?•Teaacidomethane SW-8465030 !0lt7l95 M???E 0l1193 I 1 0 t lA <I.0 n8ll 3-Temc:ilomed?wa S9V-S46 5030 10111195 b?H 465E I0117195 1 . <3.0 uBd alocvethylene SW446:030 10I17195 NDHS65E 1 IA IO <1.0 uqlt droiunn ry gqr_g46 j030 l0l17195 MIDki 465E 10f17/93 . MZ SW-8463030 10117195 ??? iari;ros i L 1.0 LA 1.0 lA <i.o <1.0 ugA agJi •Tnc?lomoenzeae S774ab 5030 10117195 NMH 465E 10117193 ZO ZO ? <?0 ugll .'Crichlomoeazeae S9V-846 5030 10l17195 NDH 465fi (O/1II95 1 1 1= 1' •Tnchlomedunc gpr-846:03p LOI17/95 MIDH465E LOlIiN3 OS 0a <OS ?? ? •Ttxhlometl?ane Syy?q6jp30 l0/1i195 mIDH4bSE I0117195 i •Sricniomethyteae 1U117l95 " 1 IA LO <I.0 u8/l . lo'ociucmmeduae SW446 5030 SW? 5030 Id17195 hIDH 465E 10117195 `?IDH 465E i0117195 i 1.0 1.0 SA <i.o <5.0 o?ri ? , -Tric.hiomomoaue SW4465030 10117N5 1?IDH4656 LOJI7N5 t 1 5.0 < .0 1 u g/I dorom8uocaewana SW-846 5030 10117195 MDH 465E 10I17195 `_p l p < 1 .0 611 u -TnmdhYlbenzeae SAr-8a6 5030 10/17195 MDH 465E iNI7195 L . 1 1 0 1•0 SR'-846 3030 t0/17N5 hIDH 465E iNl?NS . ? 1 0 ? i C?londe SW44G5030 10117/95 ?H ?E I 0 1 1.0 <1.0 ugll Xylene yy,t?4$ j030 10111195 MDH 465E W17N5 I . _ ' ? •C Ax? EPA 610 101Z3l95 EPA 630 1L07195 1 Ll t.l <20 u81( '. 'iPh°? - EPA 610 !0/15l95 EPA 610 IllOL95 1 iLU7J95 1 S o i ? <i.0 uq/l s ' 'nP°?? EPA 610 l02`!93 FPA 610 02/95 1 11/ 0:0 0?0 ?0.30 u8l? ' Iracene w(al??nc EPA 610 LOfL5195 EPA 610 10l25I95 EPA 630 tllOL95 1 0.14 0.14 <9.14 ug/l . EPA fi10 : ?6j????? (1/07195 1 0.01 0.01 0.04 vgft? ??)flu0mmIi0UM FPAfilO 10l2-9195 °3Afi10 10/Z5193 EPA 610 11107195 l 0.19 0.39 <0.19 10 0 ugil ugll ? m(6A'IPa/ic= EPA 610 F3A610 IOlZ`J95 EPA 610 tll07195 1 0.10 20 0.10 Zp . <20 u8ll =(a)p?= EPA 610 l0f23l95 E°A 6ID Ll/OI195 1 1llD1195 l 0.10 0.10 <0.10 uHft : : yuae EPA fi30 L02'!95 EPA 610 EaZC{1.?I)?I?dCp10 13I02795 1 0.30 0.30 ??..]Q ?? { EPA 610 102:195 E°A 610 IilOZl95 1 0.10 0.10 <0.10 ugll ` o??? EPA 610 10(15I95 EPA 610 I1102195 l 0.14 0.14 <O j4 ?1 a? 3.?A1py? enai l= EPA 610 l0lL195 EPA 610 02`195 EPA 610 Illa'J95 1 5.0 5.0 <5.q ug/I ? . A ?Y???e? EPA 610 1 : (RcPoa wndnocd a¢ aeu pa4e) Dakaa Couery Li6oncorT. Bnm Iarcr¢c Coryacadou Da[e Samp[ed: 1011I195 95-'233 Lab CanactlPhacc 9? Na1d1612A42-4ffi0 Date Reeeised: I0111/95 qim6er: C.WCL-95-07'I2 SamPler: Btvm[a¢t¢e DatnHepoKed: I1107195 L*d S Moiuec Na Applia6le iple ID: 93v233-06 MIDL McA°d Demm°° r'T° BL: RqmmnS Lbk imple ID/D'scxipdov: PZ-3 Paga 14 Ez=a Exmes Am11sat .1nal7sst lh7caim Cnmpomd afetEad Darc Mdhod Daa Facor AML RL Sampk Resdc naondwem EPA 630 10I25195 EPA 610 1 l/01193 t_ 3.0 5.0 <3.0 ug11 _rz E4A610 10lLSI95 FPA610 11101195 !- ts U <1.3 ug/t --e EPA 610 10/25/95 EPA 610 11102795 l U. 12 < 12 ugll VA610 1025195 EPA610 lllOL95 1 0.40 0.40 <0.40 ugfl emnra-s: Thit sample wu cctraexd paa =he E.°A cerammmdrd holdiug dme. e , -„caL ' - FPA 310.1l3 I0117f95 S t0 40 490 mg/l gb . ` - . pA75.4 10f19795 I LO IO 51 mg/l Loy EPA T6.i I0l1B193 I 0.40 0.40 3.0 mgll ,.?a?? - • EP.4750.1 10119195 t 0.01 0.41 IZ mglt . Vi¢a¢ EPA.i53.2 10111193 l 0.02 0.02 0.'_8 mgll ^„Mi . ' ' FPA200.7 10/17195 3 50 w0 1400 91 -,;? - - EPA200.7 10117N5 5 10 50 38W uglt qa EPA20OJ I01I7195 5 IO 30 <50 uqll ga n. -omi FPA_(10.7 10117195 5 l0 50 1100 ugll ;a _?Qum SM iaOB IOlI9195 5 l.0 5_0 850 mFnrl gb EPA'_OO.i 10/17/95 5 30 150 5200 ug/I ga ',? - - pA2a5.1 l020195 I 03 01 1.9 uglt ,. -ocu - • Era 200a 10117195 t mo mo azoao „8n Ern_oo.1 ianros s so 200 <zaa asn p ,a, - • EFs=oo.7 10/17ro5 s m ioo <iao ugri aa 70mi FPA200.7 10117195 1 700 300 39000 ugrl Dissolved - - F+'A=l70.7 IO/IZl95 l N :0 <°0 ugll Dissolved - • EPA110.7 iW17195 l 10 IO 270 ug/i s. Dissolved - • EPA_(10.7 10/17J95 I LO 10 <10 ugll m.'.aalDissolved - - FPA=00.7 I0/1ZI95 l IZ 12 <12 ugft uo?ved EPA,00.7 I0/17195 1 30 30 <:0 ugll p??ved - - EPA 245.1 1024195 1 01 01 <0.2 ny/1 ., ,asspiyed - • EPA:A0.7 10112W 1 :0 50 <50 uqll isalved - - EPA:A0.7 10/17l95 L 10 (0 <10 ugl! ' "4e rcpo'tinq limu (RL) was nued A dHuenn ot Ne ampic was mcessary due m ma¢u iacii.-caca. ',he mpotvag timrz (RL) was rasse4 A Nluaoa or the simple wss nxcwy due m high =smaooas ai fhis aaalY¢. (Report comnued on ixxc page) ; s ? : : i I ' Hrn+n lnec¢c Corpaamo ?? Da[e SampIed: 10l1ll95 11ate Re?"?' 1a11/93 Cauory llen[: pakoa Lab Cout+NPha? 8. J?isld16i2-9422-?87d Data gepotud: 1IfOT/95 o??; 95-3233 cvjeaNummber: C1LYX-95-0TL ??? %Moi4m? Htam In¢t¢e NaAPP? laUiu: U9uid bID4 MethodDmm=06LhWt ab Sam41e ID: 95-5233-07 gy; 8epoctin8 Lmit page 15 7teoc Sample ID/De+aiptiom PZ-.4 . ' . Fs?aa ? ? ? g? SmL SL R°Oft x? Compu?md vaaoie o.zm-ic c^mn0-3e' sw$as smo ianros aDx asss iam19s t so lA m L 0 <so <lA osn ?Pl1 ?cemm y?t.gq65p3p 1Nt7/95 .`.mHa65E IOI17/95 1 tN17195 L lA . LO <1.0 uyl ).IIYI qilonde SW-SC6 5030 1N17195 SflJH 465E 10717795 l 1.0 1.0 <1.D u64 8eaccx $Vl446 5030 10/17195 ?H 46SE ymx asss 10117195 t i.o 1.0 <i.o ugf, sromon°,tt°lt swaw sma 10117195 BmmocWomcoedhme IDl17l95 bIDB 46SE tW17/95 L 03 0.3 <03 u8ll B????o???? SpV-846 5030 SpV-8465030 10I17195 ?H? 0 50 <30 uqll ?ro? 8 sw.s-w 5030 ianns a?x assE 10/11/93 1 10117195 I l.0 1.0 <i.o ?? Hmmomemane gp,r? 5030 !Ol11195 MDH 4656 MDB4558 lUl17195 l 1.0 L.0 <1.0 agrl n•durytbeaune Spt..gq65030 10117195 xc•durylbemene SW-8465030 10117195 MDHa65E tN17f95 I IA t 7 !A 1'1 <IA <17 nq?l uvi re:c•dutYlbenzene yW446 5030 t0117195 MDH 465E 10117195 ? l0l17195 L • 1.0 LO < 1.0 uyt Camon Temchlaride yy/? S030 10119195 P.II7H't65E 1 5 -5 <u ?l Ctlomuenaene bIDH s65E y'tV-846 5030 10/17N5 10717195 1N17f95 1 - lA 1.0 <1.0 nyl C1lomdiummomslhane y?yr? 5030 10117/95 NDH ? Cilome+hane SW-8465030 10JI7195 MD8465E 10l17f9S t ?S Is <1s <s,0 uyt C4lamiorm ' ytiy.g6b 5030 1N1il95 MDH 465E ?a1?f95 ? 1N17/95 1 i ? ? p <1.0 wyl CSto?amedwu y?r.gq65D30 t0717195 ?1DHaG5E 1 ?17?5 ? t'? 1.0 <1.0 uyl :LSlommluene Spr_gq6 S030 t0f17195 MDH s!? 1N11195 I l0 10 <70 uql? s.,.^,yWmroluene yryy?5030 t0f37N5 ?1DH46SE t.:0i6ramaJLtilompropane L OS 01 <92 ugll e d Sp??A6 5030 L0/17N5 MH ? MDH 465E IO117l95 IOlI7l93 I 5.0 5'? <5.0 02 u3?l u ri un l.7'Oibmmoe e b y?y? j030 10117193 95 MDH46SE 10117195 1 0.2 s [ <1S 3 (t u an Di6romomet : Oicolombenzeae i Syy4655030 10/17/ gqr-w 5p30 10117195 MDH 46SE 10117195 1 1.5 0 1 0? <D2 g uSrl . 1:•Die.hloevbescae Syy.gq(5030 10117195 MDfi465E 1W17 95 1 ?.:.piailamoeeame 10l17195 bIDH465S L0/17f95 1 1'? 03 <I.0 <93 u4fl ugel l.!-w?o?? SW?465030 $WA4G5030 1N17N5 1?Ha65E 10l17N5 1 1 03 1.0 <1.0 ugll 1: -Oiculome?hane ??j030 1OJ17195 MDH465E 10117195 10I1795 L Q? 0.2 <01 tiVL OichloNnhYleae Sp/.gqb 5030 10117I95 MDH 465& 10117195 1 . pu QS <fl .2 uyl css-i :-DicblomemYime sW-W 5030 10/17195 MDH 465E ?-;-1'D[c.ulacoetuYiene 5.0 <5.0 uglL Spl446 5030 10l17795 MDx ? I0/1'1? 1 5.0 5.0 <S.D uF/1 DichWmdifluamm°?a? SNN8465U30 10111195 MDH'?65E _ 10117195 1.0 1.0 <1.0 ugll Dichlotoduoromednue gW.gq( 5030 10117195 'MIDH465E IW17N5 1 I.0 1.0 <3.0 ug11 l.='Dictilor°4?P? gqr_g465030 10117195 2?H465E 10/17195 < <•a ?'? <1.0 uqlt 1.3-?7ichtomompanc SW-gCb 5030 10117195 bIDH 465E ,_;-pichlomPMPAMe LOlI7195 MDH'?SE IOf1?/95 1 0s as OS <OS <OS ugll ?l !-piUilom-l-pmPYicae l $W4465ff30 yyy_gq65p30 10117195 MDH<b5E 1W77l95 ? OS OS 0.5 <OS u6tf . cu-1.3-Dichlom-l-pmpylrne SW4y65430 10117195 MDH465E I0117195 l ? 1 0 1.0 <1.0 ugll ,,aa,_I..Dictrtom-i-P,ny?Yienc Spr4q(5IX30 I0/17195 -VEDH465E l0/17195 ? . 1 0 lA <7.0 u1? EthYl a?== SW-846 5030 10/17195 NDA 465E 10/17195 . chyl EthrS t0/17195 ?H 465E 10117195 1 1.0 1.0 uPJl <1.0 yti{cgq(i 5030 ; ..?L?a?hu??? i ? e 5 (p.MR madmied on nGCt na3e) C:tmc Dakom Cm+mY Log-in: 95-3233 ?rajea Yumber. CN[7CL-95-07L' Yta[rix: Liquid Gb Sampk ID: 95-jM3-07 C'"ueo[ Sampk IDlDcsciQCOn: PZ•A Compoimd !sopmoyibe?aeae sopmoYimlueae xen,ri ?lavt xemne 11edry1 fsoburyl Kemm xemyi Tenicy Buryl EWer Ylemylene CSlonde 4aphta?lene n-amoyixozene Sryrcae t.l.l.: Teaacdlomethane t.l.: =-Teaachtome+hane Tetcac.'ilomediYlene i etT311yd[OIUI3II UILLCt1G 1 :.3?-ichlorobenzeoe 1.2. =--InWlombemene I ' -?nCl11o[oe?hane .. =-Trichtome?hane , _.._ 'richlomeCryleae "nc :lomfluoromethaue 1.:.: -ric5lompmmane 'iWommduomabane ;-; r`meNylheniene i ._.?.o..nvlhemene v;mii Cyioride m.7•Xyiute o-:{yiene iiPS.C .1ml7sis .Scenaund?sicne .ac :?aomhrne knwacme 3CNA(S)3IIthI3CElIC 3eozotb)fluocandiew 3enmtklfluormfhene '. 3e:vai g,h,t)perylem 3enZalalpy[CIIe :::rysesfe '.ioenza(a.h)arrnmc.__s ,uoiaamene .1uo`ene :naeuol1.2.3<d1PYiene i.Mem/inapnchalene I?bontnry: Bnou In¢trcc Catporauau Dute Sampled: 10111l95 Lab CaooNP6ooc B. Mald16C-462-t8:0 Da[e Receired: t0113195 Sampler; 11 • Brbm Indstec Dace Reporxed: t U07195 % Moitnaa Nac Appiiabk !4mL: Ncdzod Deocmn r ;••,:• RL: Repomn6 Lok Pagc 16 Eaaaa Eana dmym Amhs+ D&'°°° ytethod Dam Mnhod Dun Faaar MIDL RL Sample Radt SW446 5030 10/17195 l4IDH 465E 10117/95 1 LO 1.0 <1.0 uq/I sw-aas soso iarnvs Mma 4sss 1011719s i- 1.0 1.0 <i.o an sw-4as5030 10117195 wme+sse tomrss i s.o 5.0 <s.o ugn SNN-g46 5030 IOll7l93 SII7H 16SE 10l17195 l 5.0 5.0 <5.0 uqll sw.aaesaso iai;ns .rmx465E 10117195 i t_o 1.0 <i.o Uyt sw.aassmo ivi;ms NnK4sss iai-Irvs i 5.0 5.0 cs.o ugrt sw-aas 5030 ion;/vs eDe AM 10117195 i 1.0 1.0 <i.o uvn sw-aassmo rornros Mma+asa ianms i 1.0 i_o <i.a uyi sw-s.wsmo 10117195 amxasss 10117195 i 1.0 1.0 <i.a wvt SW446 5030 10117195 bIDH 465E 10It7193 t OS 0.5 <OS uqlt SW4465030 101t7l95 bIDH465E lel17195 L 1.2 13 <1Z ug/1 SW4465030 LW17195 MIDH465E 10117195 I lA 1.0 <1.0 uqll SW46 5030 10/17195 9IDH 465E lO/17195 1 5.0 3.0 <5.0 ugrl sw4" 5030 iai;rvs Mmx+6sE 10117ro5 < <.o 1.0 <t.o uvi SVV4465030 1011T195 NDHA65E 101I7195 1 lA LO <1.0 uyl SW4iA65030 I0117195 }mH4bSE I01I:145 I LO 1.0 <1.0 uyl SN-846 5030 10/17195 %IDH 46.5E 10/17195 I 10 2.0 <2.0 uyl sw-sae 5030 iat7195 .rroE14Ue i0117195 i 1.2 1- <1.2 ugit SW-846 30:30 10117195 MDH 465E 10117195 l 03 OS <0.5 uyl $VV44b 5030 10/17195 i.DH 465E L0/17/95 L 1.0 lA <1.0 ugll SW44fi 5030 I0117195 NDH +65E I0117195 I t-a LO <1.0 ugrl SP/406 5030 IDI17/95 NDH aGSE I0117193 I 5•0 5.0 <3.0 uyl S9V4465a30 10/17J95 MIDK465E 10f11195 1 tA 40 <1.0 uyl sw-aas soso 10117195 AlDH 465E i0117195 i 1.0 1.0 <i.o ugii sw446 5030 tor17195 ,rmxessa ta17195 i i_o 1.0 <i.o uyi SPl4465030 10/19795 NWH465E l0117195 1 IA 1.0 <2.0 uqll Sp/4465030 I011i195 'viDHd63E 10117195 L LA 1.0 <1.0 ayI EPA 610 102I95 EPA 610 Ill07J95 L 1.1 1.1 < 1.1 aglt EPA 610 102/95 E°A 610 11lOJJ95 I 2.6 2.0 <?.0 ugli F3A 610 IOlL5195 E.°A 610 11102195 [ 4.0 4,0 <4.0 uyl EPA 610 101i195 E_°A 616 11102l95 [ 0.30 0.70 <9.30 ugll EPA 620 1011:195 °DA 610 11107195 1 0.14 0.14 <0.14 uq/l EpA 610 1025I95 f39 610 11107J95 I 0.01 0.01 0.06 ugll f EPA 610 10f25195 &°A fii0 iLQZf95 1 0.19 0.19 <0.19 ugri ? EPA 610 l012195 EP.4 fii0 I1lOll95 L 0.10 0.10 O.i a uyi &°A 610 LOl15/95 FPA 610 IU01193 l ZO ? 0 ? <?0 ug+l EnA 610 10/Z'!95 FPA 610 11/02195 L 0.10 0.10 <0.30 ug11 EPA 610 10(1:195 FPA 610 L]/OZ195 l 0.30 030 0-12 ugf I! EPA 610 1DfL5195 EPA 610 !1lOL95 1 0.10 _ 0.10 <0.10 ugil °A 610 E IO/Zl95 EPA 6t0 I1102195 t 0.14 0.14 <0.14 ugtl . EPA 610 I02'135 E?A 610 I1102195 I 5.0 5-0 <5•0 ugtl i i i (Rcpoct conanued oa neu Pa3n [ahoramrT Brnm inrecxe Co`ponuoa Date Sampled: 10111195 f1;.,,r• Dakoc Caunry Lib CaWaNPLuuc B. M20612•942-&820 Date Betei+ed 101II195 jpq-im 95-3233 '? Bmm i?ise Data ReP"rced: I1107195 Praject Number: C.`??'95-07Z ?? Not Applio6la ?taanc I.:Wid bID L• ?(efCod De¢rsou r;m» ?b SamPle ID: 95-3273-07 L RL: RqomnS Limic P+CC I7 ClIeac Snmple IDR)va'+4nuo: PZ'A Cumpomd E=-.ta NIedhnd Eann Aml7= Date Slethod Anz7s+ Dmn DilatiO6 Faaor SIDL %L S.. * Res ult 2 'Methy WphtNalene EPA 630 30/l5/93 EPA 610 IIIO'7J95 lLPL95 ! I- 5.0 13 5.0 13 <5.0 < 13 ug/l aB!! Naphihalme EPA 610 EPA 610 L025I95 EPA 610 10125195 EPA 610 11/OL95 t 12 12 <12 agll Phe=mmrwc EPA 610 10lL'!95 EPA 610 11/OL95 1 0.40 0_40 <O.JO ngll pyRne Remaria: This amPk was exrtac2d Puc the EPA tecammmdt4 holdm6 MIRe• . IDOrcinic - EPA 310.1/3 10117195 d 10 40 360 mg/L Sb ,Vkalicury. Toal FpA 75A LO/I7195 L IO l0 32 m411 SuiCarc " _ F3A3' 36.1 10118793 L 0.40 0.40 l_0 mglt Suifde. Tocal V'niew . EPA 750.1 10119/95 L 0.01 OAL 0.99 mg/! Ni¢ogm. Ammonia ' . EPA 3333 1W17l95 1 0.02 0.02 O.S mqll Yi¢o4en, Ni¢Me metau - EPA SIXI.T 10/17195 5 50 270 1100 ugll ,?,a paemc, Tad - FPA200.7 tNl7l95 5 IO 50 8900 ug/l ? $anum. Toml - - gA?00.1 1N11l95 S l0 30 <:0 ug/t .a ?.,?,o? Cadm - FPA?00-7 10117195 5 10 50 1000 ugll ga C.tmmmm. Taol - • SM Z.i' a08 10119195 5 1_0 5.0 370 mBEo ll Sb Hudness. Calcmm - EPA:00.7 10117195 5 30 L50 5300 ugft Sa Lnd. Tool - EPA i45.1 1020/95 I 01 01 8.3 ng/l Ylacury, Tooi gpA?qp.7 10117195 1 200 200 41000 ugfl Porassium. Tod E-A _f10.7 10117195 5 SO 200 <:00 uqfl 3% Sdemum. To°! ? EPA :00.7 19117195 3 ID l00 <100 ug/I Sa Silva. Tud - EPA?00.7 LNI7195 I 300 300 98000 uga Sadium. Toml - uetnLS EPA2(10.1 101I2/95 2 50 100 <100 ugd Sa Arsemc. Dissolved ppp?pp.7 10112195 1 10 t0 26tl ugll Banum• 7'%5°Wed gpA,^,pp-7 10l12l95 1 10 10 <10 ugll Gumma. Dissoived EpA;,p0.1 10112195 t 12 12 <12 ugil Cuvrmum. Total Dissolved ' - EPA 2oo.7 - 10111195 1 ;0 30 <iD ugll I.cad. Dissolved II'A 245.1 1024J95 1 0.3 0.= <0? ?( Macury.Dissalved fipAZ00.T 10117195 1 50 50 <50 uyl ?$denium. Dissolved ppA200.7 10111195 I IO IO <10_ uyl Silaer. Dissolved ? i ? i .a The iepo?ting :imu (ItL) 'a'az catsca- A dilumn of rhe a?ie was ieem[Y due m rmaic imaiaencs• P The cepotdng limu (RL) was nused. .i dilunan ai Ihe ample was neresn,y due m high contzm=110113 ui tlhis amlyrc- (Renon convmud on mu Pa4e) L Dalron Caunry n: 95-32?3 ¢ Yumher. CWLYAS-0iZ x Liquid 'amole ID: 95->>3-08 .iample ID/Des¢iptlon: Filteted mmLs Bladc Labora[or7= Braun fnrcaee Comonco¢ La6 C01112ctlP6ooc S. Naiq/612-94..-i87D samPl?- " Braua tamenec "L &IaXm? Not.AppGabte MIDL: Methad Dexr,o¢ Limic Ria Rcpotmg Limu PaarG ExUIAet Amt)ss Aoai7str DQtdm Compowd Nuhod Da[e Mahad Due ffaenr MIDL BL 4A1.YSLS PERFORIYIED ON 1ffiS SAMpSS,E DUe SamNed: l0/t U95 om Recei-ed: fOttll95 D't° RPm%ld: lI!!T;/95 NBc 18 SamP(e Ravlt (Reoort mnomncd oa nut page) i 't i e i f S F ? ? 1 E { 4 ? r ? f 1 ? i ? ? ( cyenu 1)akoa Caumy I„?g-im Pzoject Yum6er. 954233 C?eIXX'95-07Z M2trd Li4uid L2b Sample ID: 95-32330 Clieat SomPle ID/DesaiPuu°: TciP Blaclc Compound La6oratorT Br,a I¢ecsc C?Rorauon Lab Cu=C/Phuac' B. bfa0512-942,SL0 Sunpler; Bram Ia¢= % mIout? Noc Appliable MIDL- Mctliod Oemaoa Limk RL: RqmrdnB L'°uc Extmct ?? M n?d Dau Futor YIDL Met4od NO ANALYSiS PERFOR^NW ON THIS SAh1P7.E n,m s=nled.- 10111l95 pategeriired: 10111195 pate RepoRed: l i/07195 paea 19 gy SamPle Rmilt (gePuR candwed on nex[ Pqe) DaYUr+ Caunry ?o7ecc Yumber: 95-1-293 G`AX.'C'95-0722 i.uix: L'Wuid .u jample ID: 95-3273-10 .imc Sampin ID/Desc+Puow Feld Hiadc Lybora(Qry; BnotII I02IQL COtpoIa00O La6 CametlPhanc 8: Ma1d612•9424820 SamPU+'= Bnm¢luemamc s. IMtoimac NotAPPil=bIo bIDL• Mediod De2cdoa i ^^;• RI.: RP°1dn8 Limic nu,s=aled: iailms Dace Recen'ed: l0l11195 Date gepo`ted: lll07195 P2[p: 20 -- FHtia E yfethad urad Date A°alyas mnhod Aml7sst DiBmoa Dm Faeur rIDL RI. SamPk Ran Compowd 'loiavie Oc'qauie ComPounds ?? q?0 10111195 :?IDH 4658 IOI17I95 t 30 5o LO <50 <1 Q °g/i v81l :.e:one Spy-846 5p30 1 0117I95 HDH 463E IW17t95 1 t_0 1 0 1 0 - <I.0 agll ?::v? C_loride ?ry?r.gyg SQ30 1N17795 bIDH aGSE 10I17N5 L . 0 1 . 1 0 <LO ug/! ie.._ene ae z yryy? 5030 10l17N5 MDH 465E E iW17N5 10l19195 l 1 . lA . 1.0 <1.0 ugd :- ??mooca gpr?Sp30 10117195 ??ID8465 immac::loromedaae O 10/17195 MDH465E 10117195 1 0.3 0•3 ? 3romodiuommedunc SW-846303 S1t/.gd6 9030 I0II7195 MDH 46SE 10f11N5 t 0-5 OS 0 5 s 0 <5 uqfl 3m??? SW-346 5030 I0/11195 StDH465E 10117l95 I 5.0 1 0 . LO . <1.0 ugtl 3mmomemane SW4465030 10117195 MDH465E I0117195 I . lA 0 1 U.0 ugtl i-3uryitesene SVV-846 5030 10/17195 MDA 465E 10/17193 I . :x-aucrlbwzene SW-8465030 10l17195 YIDFI465E I0I17I95 1 LA 1.0 7 <1.0 <I i uqil ll u :ea-Butvi6eazeae _ _ _ y i? ytiV-S4G 5030 I0117195 MDH iSSE 10117195 L l1 0 1 1. . < 1 .0 g uq/i ?? ? ? ?? _aeoa _l r SVV-8d6 5030 10117/95 yIDH 465E t0117/95 1 . ' ? ? C? ? ? •:Slomaeyem SW-846 5030 1N11N5 ?dDH 46Sfi INL7/95 L - LD 0 1 <1.0 ugll h .^iloma:ommumesan? SW-S465030 10117195 NDHd65E 10117:95 1 . Z:Ilom?ane SP/4846 5030 10711795 MDH -165E IO/ITNS 1 1.5 1-5 5 0 <I3 <5 0 u3+1 uqlt ..."domiorm sw-sassmo iai;rss a+nxssss iavms i 5.0 0 1 . 1 0 . <i.o ?i V,to?m-ateac ' SW-846 3030 t0117fl5 MDH 465E 10/17195 l . 0 ( . lA <LA nqil `.darvcolume 't. ^ Sy,.9465030 I0/17195 ldDH<GSE 10117195 L . 10 10 <:0 ugil .:yomloimnc :-. SW4" j430 10117795 MDH465E t0117195 I 2•Dibcomo-3-CSIomProF= ' . SW-846 3030 10117l95 Y1DFI 43E 1U117195 1 &- 5 0 0.2 5 0 , <5.0 ugrl ,:-Dib'omoeduae « SN4q6 5030 IN37I95 MDH 465E 10f17N3 l . 02 - 0 2 <0 ? ?? ,a. D??mo?d SryV.g46 5030 10117I95 ?1D8 a65E IN17/95 I 1 1 . tS < l.i wyi ? ?:?omo?? ' S9V-8465030 iai;ros aIDHS65E 10117195 l - 0 2 0? ? <0- "ga -z;jc=lomocnzcne SW-8465030 10117195 NDH465E I0117193 1 . '..-Jie^.lombenzena sw-aasimo iomrss MDH 46ss 10117195 < <.o `.a < 1.0 <o ? u8l1 ?? ?..•;,?w.n? SWA46 %030 10117l95 bIDH 165E 10/17195 1 0.7 1 0 0.3 0 1 . ?1.0 uyl ,:.Jiclqmethzae :7ecclamdIIylene i S1V-846=030 10/liNS StDA?65E H465E 10117195 I0/17195 l 1 . 0.1 . 0.2 <01 ugfi . :s.;,:D ic.hloroemylene SW4465030 SW-8463030 10117f95 10l17195 ND 9tDH4bSE t0f17J95 L D' 03 <0= ugfl ,=-;.,-DiWomcdhYtme : ' . , Dicalomdifluommethane SW-8465030 I0/17195 hIDA't65E 345E DH (0117193 10117195 l 1 5.0 5.0 5.0 5.0 <5.0 <S.0 uv/l ugll Dic:tamfluommahaae SPI-846 %D30 SW-8465030 lO/17193 t0117195 ? M a1DFIybSE 10117195 I 1 .0 1.0 C:.O < 1 0 ugll u8l1 030 SV.`-846 10/17195 1?ID1?465E 10117195 l LO 1.0 LO . <1 0 ugll J-,^,(ezlampmpane c yryy.g46.030 IW17195 `LDH465E 101I7195 l 1.0 . '-_o?o?p?P,,,. 10/17195 `?H465E 10/17195 1 0.5 0-5 <OS aBfi l.:•Jic^.lom-t-propylem SW-8465030 SW4" ??0 10117195 'dDHa65E 101t7N5 I OS OS <03 ugil cs-l.? Dic6lom-i-P?PYime SW44b 5030 10/17195 MIDH 465E 10117195 ! 0.5 - 0.5 1 0 <? 0 ?l •.,w-,.?-Diciilom-l-piaPYlme SVV-846 5630 I011T195 MDH 465E I0/17195 I 1.0 . 0 1 <1 0 ug/l E:hyt 3enzenc SP/4465030 10l17195 MDH 465E 10117195 L 1.0 . . Rhyl ztff SVY$665030 10111195 MClid65E 10117195 I lA 1.0 <I.0 uqil Ycx=alerobumdm: (gzpon coaMued on nest pvSe) ranonwrr- smm twaoa r.omur,ooa 1 nate samalea: 10111195 Dticon couccr tan ca?r?? B. ?+,?eiz-9az?szo n.? x«?.ea: iaii?s ; 93-i233 s,,,? amn r? nue a?wreea: ivmros ? aber: C.`?17Ct-95-072? yo? ,6 No[ P.ppliable ' ?^9u? yID?; Me?ad Decxdo¢ Limic e ID: 95-?3-10 RL. Reportiag T:.mjrt f ? ftgC 21 ple IDlDaa'ipt[ov: Ficid Slaalc ? Cumpound EXWaa Me[hud FstraG Date Ami1ffi Me[Eod Anaipss Due DWUfoa Faoar NIDG RL ?qaw Ple Regult SCV446 5030 10/17195 MIDA 465E 10I17195 1 IA O I.0 IA U.0 <2 6 ugtt ugfl ILZrnO ? Spl-846 5030 IO/17l95 JdDH 445E 10/17/95 I- L 0 5 S 0 . <5 0 ayl '? ?? ?D? SN-8465030 1WI7195 :4IDB465E DH 465E L0/17195 I0117195 I 1 . 5.0 . SA . <SA agrl mryt Kemne S4l446 5430 10117/95 M Buryi Ether us SW-W 5030 1W17l95 bIDH 465E 10/19N5 7/95 1 I 1_0 0 5 1.0 SA <1.0 <5.0 n8lf ugll ry CNaride SW4846 5030 10117/95 MDH 465E 1011 10/17195 i . 1 0 1.0 <i-a uan ? sw.aas so3o 6 5030 sw44 10/17/95 10117rn5 Nmx asss MDH asss 10117m5 i . i_o 1.0 <i.o %n . sw-aas 5030 Vnros MI)K assa tai;ros i i.o i.o <i.a uan hane achlotor SFI4846 5030 LO/17195 MDH 465E 10117195 I l OS 2 1 0.5 t3 <OS <1? ugA ugll . ? mc'ilomexzne SW-946 5030 0 10l17I95 IO/17195 hIDH 465E MIDHa65E 10117195 10l17195 ! . 1.0 1.0 <1.0 uqlt )ewYIenc SW4a6:03 SW446 5030 10137195 NWH 465E 10/17195 t 3.0 5.0 <3.0 uvl inma yryY$46 5030 10/17195 2.mB S(SE 10117195 1 1.0 1.0 <1.U uq(1 110m6mzene SW4465030 I0117195 bff7H465E 1N17195 1011i195 l 1 lA IA LO 1.0 <I.0 <1.0 ugtt ugrl ilamuuizene SW-84650.30 $W$46 5030 10117195 10117195 YIDHa65E !tiIDFI 465E LO/17N5 1 7-4 ZO <i 0 ?i 110?edulne yyV$6$jp30 10117195 YfDA465E 10117195 1 1-2 1-2 OS <OS ugyl yo??e gp/..gab 5030 10117195 MDK 465E 10111195 1 OS 110madryiene $W4665030 10117195 *MH<65E 10/17193 t lA 1.0 LO <I.0 <1 0 ugft ugft ?Wromcxbane ane SW-846 5030 10117195 MDH 465E 10117195 I 1.0 0 5 SA . <5.0 ugll yomQmp - M1+n SW4465030 10117195 MDH465E 1011i195 l . 0 I ,u e iuamed . SLK846 5030 10117195 MDH 465E 10/17195 t 1•0 ' 0 1 < 1 0 uyl as icthYfbeny SW.Sa6 5030 IO/1'/195 MDH 465E tat;ros l 1.0 . . ?yiye?ne SW-84G5030 f0/17195 bIDH40E I01l7195 1 LO lA 1 0 <1.0 <i o ug/1 usn mde sw-sae smo iamrvs Nrox assE iaiTrss i i_o Lo . 1 0 . c 1.0 ugil ? sw-aas 5030 iarnvs MDH asss 10117195 i . ($GOOR COadm1M o¢ OG[[ PSYiG) > 9 i ? f ? S. [ I ? D'JIG .S'd1IIPk& • ?n??, gde¢ fn¢rme Cacpomco¢ Wifi/fi12-9a2-t820 ? B ?wRecared; LO/I1/93 ? Ill07N5 G Dalroa CoucttY iab Co . maalPh"° InCs ? m Bre ?R? 93-;233 ? :a Vumber: CNL'CC'95 ?p?: liabla App Nac % HoisOSc ydwd Dco:== t'„„E ic Sotid 3am1ie ID: 95-i733•11 YIDL: RL: Repomq Limit pagc 2Z u SamPle IDlDesa'i4dQw Mbod $lank . F-VU-d E straa AuROM y° g?n SIDL 8L ? a Rnult Methad Dam ? ComWund (?AHs) (GCIMSI vocomatlc S9drocarbans 35 SW-846 40 0/1Zf95 LOIlN9S I. 1 ? 0lt6195 OS3 033 033 0.33 G033 <033 m3l? m4?k8 k on? sw-aas 3540 ian2ros s -84b 3= 1 svr?as srm taurss 1 o.?"3 0?3 o 49.33 <a.?-3 m?J B ? ,Jo?)«= u-nc r swaw 3540 846 3340 W taivs 10l17J95 iai?ss i SW-S46 8Z10 95 1 oss 0?'3 ? 0.?? <a?-? ?+rs : . -miaia¢tluaceue $ - $W-8467340 1W11195 l0l167 SW?46S270 <0 ? mg/1aS sotblduardameae 0 10117195 6l95 1 SWa46 g?p [0l1 0-'3 033 0?3 . <0?'3 ?+1 m81 .aiklfluorandIene y?VV-84633a SW4q635d0 10112195 10II6l95 t SW446 ZM N95 t ??? IOIl ? 0.?3 Oa3 •3 <0?"3 <0.33 mglk5 mgle6 aal4.i.:1P?Yi? y?y.g4635?10 0 10l1T/95 tN12l95 - 1a16193 1 SWA46 8270 0.33 33 0 0.. 0.33 <0.53 aBok4 :?ota)W.ccne ytiV-84G 334 iaivss L0116l95 1 svr4as azro . sw-aes 3540 6195 l t0J1 ?-? ? Oa"3 O.S? 3 <033 <9.73 m817c8 mVk8 zoiuna - : Sty-846 3540 846 33a0 W I0/12195 IWIS195 1 ?1ld95 1 ? 5 1 033 033 0.? U?3 <0?7 m8/?4 :< . .:nnmcae y . yryl-8467540 l0l32195 $aG 82T0 IN1619 10116195 L 0.33 Oai ? <0-33 GOJ'3 m81k8 oWJk6 ? ..:^ne d] SW-8463540 110,12,95 0112195 SW?46S170 1011N95 1 0.33 i O.3 _r.at1.:.3< PY SW-8463540 33 0 <033 auyY4 :.IeaYunaPn"WI= SW-846 3540 10/17195 10/16195 1 SW-846 ffi 195 1 0.33 033 . O..i3 <033 ?k4 acntGalene SW-846 3540 t0117J95 1W16 SW-846 l95 1 sw-aas srm lOllfi 0.33 0.33 <9a3 m811?6 ?::?m?M sw-aas ;sao iaixros ^,,ne 74 ,i cec ...g?'JalaoleSuccoB=a° gp!-8C655a0 10I17J95 5 SW-84G827Q tN16l95 1 57l446 8270 10116l95 ? gg 10T Scec ;.?uorooiaueaY+ n==?•is SN-846 3540 10/1249 sw$as 3540 iaizms sw-aw ano 10I1G193 1 ' -:P6ar/1-014 E (Fnd of Repan) 111fI\l/111 vI1u1/1 V! I.USLOLl)/ - C(.?? ?a?, . ,_ul Exceplion flale Site I(leMification 1/? 1-?j J?? Ao,)e 0, !c Ka[4 Client Idenlificatlon 1/? I Qy k D'Pc? lcawll?? a=?°" `°so0d e?ui°a°f fillaf a=w?,ldr a=iiyuia i=,i„aUa o= owur ProjeclManac?er Sampled By: ? BoUle lype and numUer Temperalure Upon Recelpl ]A Recelved on Ice °C Candilion Upon Recelpt q Good ? Olher m o U • O X ? m ? Evidence Tapa Intacl Q Yes ? No q NA Project !l: C'mB -qs O7121? Task k: m ? . r i 'r- r N G -o ? ? o WI LUST Project q Yes ? No Are samples In compllance wlih soil movement Sampla No. C ll ll a v ? w °1 V c d ? " re ulalions Yes No NA - l b U O o ac on 9 Q ? = ? ( u sn nly) Sampla Idenlificatlon pale Time o Z -' Anelysis/flemarks R 4 - ? ' ? . 3m ry5 _3,l?i-UI ol.S t C.. S t 10 ??u '.i /c?o0 .? ? ? ? 11 _ _oz f lti / ? -?40' ,: ve?s q,ty- a _ ? < qs s os -?(S!7 41, QCQA rn?f,? 1 J u, is ID;?S g 3 _ 4, s xs 0 ' ' -?? P2- l ? ? - 3 - - W•d9c 8:t o l? ? ..?? i?, .? .-- - ? P6 P2'3 IQI, ILI' '? •I 1 ? 3 z . . -09 PZ- 4 „rks : s k j ? - - -a? E.Is l", L h- _ ? - _ _ V -UL n? T'?nlSk,x? ul? I ? o ! ? ? /foAO +1 - )rJ ? fiut, ? py ? Dple? L=[LCLl 3TI ? Recelved 6y; RullnqulshnJ By: pala 74ne qecalvad 9y; , e Inqulshecl pale 1 I Tlme RecelYed 1or labwelory B• ? ? < ? Date Time Commenls: ? ? ?•- ?? - iG // li" /S ?'.3 uraun iniwmc coipo(allon, Inc. 6875 Wnshln(pon Avenue, ShG)plnp anJ Recelvlng, Mlnneapolls, MN 55438 Form No. Clalm 1(85