1950 Jade Lane - 2010-04-29 Analytical Results NELAC Standards19 Co
aceAnalytical
waaw pacelabscwn
April 29, 2010
Mr. Dean Nething
Dean's Tank, Inc.
PO Box 22515
Robbinsdale, MN 55422
RE: Project: DRO -soil
Pace Project No.: 10126869
Dear Mr._Nething:
Enclosed are the analytical results for sample(s) received by the laboratory on April 20, 2010. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Cory C Lund
cory.Iund @pacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent off Pace Analytical Services, Inc.
1 1
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
Page 1 of 7
aceAnalytical ®
www.pacelab &corn
Project: DRO -soil
Pace Project No.: 10126869
Minnesota Certification IDs
1700 Elm Street SE, Suite 200 Minneapolis, MN
Alaska Certification #: UST-078
Washington Certification #: C754
Tennessee Certification #: 02818
Pennsylvania Certification #: 68 -00563
Oregon Certification #: MN200001
North Dakota Certification #: R -036
North Carolina Certification #: 530
New York Certification #: 11647
New Jersey Certification #: MN -002
Montana Certification Al: MT CERT0092
Minnesota Certification #: 027 - 053 -137
CERTIFICATIONS
55414 Michigan DEQ Certification #: 9909
Maine Certification #: 2007029
Louisiana Certification #: LA080009
Louisiana Certification #: 03086
Kansas Certification #: E -10167
Iowa Certification #: 368
Illinois Certification #: 200011
Florida/NELAP Certification #: E87605
Califomia Certification #: 01155CA
Arizona Certification #: AZ -0014
Wisconsin Certification #: 999407970
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent ♦ off Pace . Analytical Services, Inc.
.
,gtrIelac'.
PaceAnalytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
Page 2 of 7
aceAnalytical
.pacelabs.cam
Project: DRO -soil
Pace Project No.: 10126869
Sample: 1950 JADE LN #1 Lab ID: 10126869001 Collected: 04/20/10 14:30 Received: 04/20/10 15:15 Matrix: Solid
Results reported on a "dry- weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIDRO GCS
Diesel Range Organics
n- Triacontane (S)
Dry Weight
Percent Moisture
Sample: 1950 JADE LN #2 Lab ID: 10126869002 Collected: 04 /20/10 14:30 Received: 04/20/10 15:15 Matrix: Solid
Results reported on a "dry- weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quat
WIDRO GCS
Diesel Range Organics
n- Triacontane (S)
Dry Weight
Percent Moisture
Date: 04/29/2010 05:11 PM
Analytical Method: WI MOD DRO Preparation Method: WI MOD DRO
ND mg /kg
86 %
Analytical Method: % Moisture
9.0 %
Analytical Method: WI MOD DRO Preparation Method: WI MOD DRO
ND mg/kg
80 %
Analytical Method: % Moisture
ANALYTICAL RESULTS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
5.2 1 04/22/10 05:19 04/26/10 14:02
50-150 1 04/22/10 05:19 04/26/10 14:02
0.10 1 04/23/10 00:00
5.1 1 04/22/10 05:19 04/26/10 13:55
50-150 1 04/22/10 05:19 04/26/10 13:55
10.2 % 0.10 1 04/23/10 00:00
Pace Analytical Services, inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
REPORT OF LABORATORY ANALYSIS Page 3 of 7
aeeAnalytieal
www.pacelabs.com
Project: DRO -soil
Pace Project No.: 10126869
QUALITY CONTROL DATA
QC Batch: OEXT!12764 Analysis Method: WI MOD DRO
QC Batch Method: WI MOD DRO Analysis Description: WIDRO GCS
Associated Lab Samples: 10126869001, 10126869002
METHOD BLANK: 778264 Matrix: Solid
Associated Lab Samples: 10126869001, 10126869002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Diesel Range Organics
n- Triacontane (S)
Diesel Range Organics
n- Triacontane (S)
Date: 04/29/2010 05:11 PM
mg/kg ND 5.0 04/26/10 13:06
°10 83 50- 150 04/26/10 13:06
mg /kg 80 65.3 64.8 82 81 70 -120 1 20
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
LABORATORY CONTROL SAMPLE & LCSD: 778265 778266
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
ok 83 82 50 -150
REPORT OF LABORATORY ANALYSIS Page 4 of 7
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
(Math
Project: DRO -soil
Pace Project No.: 10126869
QC Batch: MPRP /20132 Analysis Method: % Moisture
QC Batch Method: % Moisture Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 10126869001, 10126869002
SAMPLE DUPLICATE: 778864
Percent Moisture
Percent Moisture
Date: 04/29/2010 05:11 PM
QUALITY CONTROL DATA
10127148002 Dup
Parameter Units Result Result RPD Qualifiers
SAMPLE DUPLICATE: 778865
° !0 17.8 18.0 1
10127040003 Dup
Parameter Units Result Result RPD Qualifiers
13.9
15.4 10
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
REPORT OF LABORATORY ANALYSIS Page 5 of 7
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
aceAnalytical
wwwpacelabs.com
Project: DRO -soil
Pace Project No.: 10126869
DEFINITIONS
WORKORDER QUALIFIERS
QUALIFIERS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2- Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
WO: 10126869
Et) The samples were received outside of required temperature range. Analysis was completed upon client approval.
Date: 04/29/2010 05:11 PM
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
REPORT OF LABORATORY ANALYSIS Page 6 of 7
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
L
aceAnalytical
wwwpacelabs.can
Project: DRO -soil
Pace Project No.: 10126869
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
10126869001 1950 JADE LN #1 WI MOD DRO OEXT/12764 WI MOD DRO GCSV /6658
10126869002 1950 JADE LN #2 WI MOD DRO OEXT/12764 WI MOD DRO GCSV /6658
10126869001 1950 JADE LN #1 % Moisture MPRP /20132
10126869002 1950 JADE LN #2 % Moisture MPRP/20132
Date: 04/29/2010 05:11 PM
REPORT OF LABORATORY ANALYSIS Page 7 of 7
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..