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1950 Jade Lane - 2010-04-29 Analytical Results NELAC Standards19 Co aceAnalytical waaw pacelabscwn April 29, 2010 Mr. Dean Nething Dean's Tank, Inc. PO Box 22515 Robbinsdale, MN 55422 RE: Project: DRO -soil Pace Project No.: 10126869 Dear Mr._Nething: Enclosed are the analytical results for sample(s) received by the laboratory on April 20, 2010. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Cory C Lund cory.Iund @pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent off Pace Analytical Services, Inc. 1 1 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607 -1700 Page 1 of 7 aceAnalytical ® www.pacelab &corn Project: DRO -soil Pace Project No.: 10126869 Minnesota Certification IDs 1700 Elm Street SE, Suite 200 Minneapolis, MN Alaska Certification #: UST-078 Washington Certification #: C754 Tennessee Certification #: 02818 Pennsylvania Certification #: 68 -00563 Oregon Certification #: MN200001 North Dakota Certification #: R -036 North Carolina Certification #: 530 New York Certification #: 11647 New Jersey Certification #: MN -002 Montana Certification Al: MT CERT0092 Minnesota Certification #: 027 - 053 -137 CERTIFICATIONS 55414 Michigan DEQ Certification #: 9909 Maine Certification #: 2007029 Louisiana Certification #: LA080009 Louisiana Certification #: 03086 Kansas Certification #: E -10167 Iowa Certification #: 368 Illinois Certification #: 200011 Florida/NELAP Certification #: E87605 Califomia Certification #: 01155CA Arizona Certification #: AZ -0014 Wisconsin Certification #: 999407970 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent ♦ off Pace . Analytical Services, Inc. . ,gtrIelac'. PaceAnalytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607 -1700 Page 2 of 7 aceAnalytical .pacelabs.cam Project: DRO -soil Pace Project No.: 10126869 Sample: 1950 JADE LN #1 Lab ID: 10126869001 Collected: 04/20/10 14:30 Received: 04/20/10 15:15 Matrix: Solid Results reported on a "dry- weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual WIDRO GCS Diesel Range Organics n- Triacontane (S) Dry Weight Percent Moisture Sample: 1950 JADE LN #2 Lab ID: 10126869002 Collected: 04 /20/10 14:30 Received: 04/20/10 15:15 Matrix: Solid Results reported on a "dry- weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quat WIDRO GCS Diesel Range Organics n- Triacontane (S) Dry Weight Percent Moisture Date: 04/29/2010 05:11 PM Analytical Method: WI MOD DRO Preparation Method: WI MOD DRO ND mg /kg 86 % Analytical Method: % Moisture 9.0 % Analytical Method: WI MOD DRO Preparation Method: WI MOD DRO ND mg/kg 80 % Analytical Method: % Moisture ANALYTICAL RESULTS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 5.2 1 04/22/10 05:19 04/26/10 14:02 50-150 1 04/22/10 05:19 04/26/10 14:02 0.10 1 04/23/10 00:00 5.1 1 04/22/10 05:19 04/26/10 13:55 50-150 1 04/22/10 05:19 04/26/10 13:55 10.2 % 0.10 1 04/23/10 00:00 Pace Analytical Services, inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607 -1700 REPORT OF LABORATORY ANALYSIS Page 3 of 7 aeeAnalytieal www.pacelabs.com Project: DRO -soil Pace Project No.: 10126869 QUALITY CONTROL DATA QC Batch: OEXT!12764 Analysis Method: WI MOD DRO QC Batch Method: WI MOD DRO Analysis Description: WIDRO GCS Associated Lab Samples: 10126869001, 10126869002 METHOD BLANK: 778264 Matrix: Solid Associated Lab Samples: 10126869001, 10126869002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diesel Range Organics n- Triacontane (S) Diesel Range Organics n- Triacontane (S) Date: 04/29/2010 05:11 PM mg/kg ND 5.0 04/26/10 13:06 °10 83 50- 150 04/26/10 13:06 mg /kg 80 65.3 64.8 82 81 70 -120 1 20 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607 -1700 LABORATORY CONTROL SAMPLE & LCSD: 778265 778266 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers ok 83 82 50 -150 REPORT OF LABORATORY ANALYSIS Page 4 of 7 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. (Math Project: DRO -soil Pace Project No.: 10126869 QC Batch: MPRP /20132 Analysis Method: % Moisture QC Batch Method: % Moisture Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 10126869001, 10126869002 SAMPLE DUPLICATE: 778864 Percent Moisture Percent Moisture Date: 04/29/2010 05:11 PM QUALITY CONTROL DATA 10127148002 Dup Parameter Units Result Result RPD Qualifiers SAMPLE DUPLICATE: 778865 ° !0 17.8 18.0 1 10127040003 Dup Parameter Units Result Result RPD Qualifiers 13.9 15.4 10 Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607 -1700 REPORT OF LABORATORY ANALYSIS Page 5 of 7 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnalytical wwwpacelabs.com Project: DRO -soil Pace Project No.: 10126869 DEFINITIONS WORKORDER QUALIFIERS QUALIFIERS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2- Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. U - Indicates the compound was analyzed for, but not detected. WO: 10126869 Et) The samples were received outside of required temperature range. Analysis was completed upon client approval. Date: 04/29/2010 05:11 PM Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607 -1700 REPORT OF LABORATORY ANALYSIS Page 6 of 7 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. L aceAnalytical wwwpacelabs.can Project: DRO -soil Pace Project No.: 10126869 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 1700 Elm Street - Suite 200 Minneapolis, MN 55414 (612)607 -1700 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 10126869001 1950 JADE LN #1 WI MOD DRO OEXT/12764 WI MOD DRO GCSV /6658 10126869002 1950 JADE LN #2 WI MOD DRO OEXT/12764 WI MOD DRO GCSV /6658 10126869001 1950 JADE LN #1 % Moisture MPRP /20132 10126869002 1950 JADE LN #2 % Moisture MPRP/20132 Date: 04/29/2010 05:11 PM REPORT OF LABORATORY ANALYSIS Page 7 of 7 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..