3575 Pilot Knob Rd - MidAmerica Reporting Underground Storage Tank RemovalsMIDAMERICA
TECHNICAL & ENVIRONMENTAL
SERVICES, INC.
December 13, 2010
Mr. Brian Carnes
Premier Banks
2866 White Bear Avenue
Maplewood, MN 55109
RE: Removal of Three (3) Underground Storage Tanks (USTs) & Associated Environmental Reporting
Former Sixty One Stop
3575 Pilot Knob Road
Eagan, MN 55122
MidAmerica File # 10P- 1433 -A
Dear Mr. Carnes:
Enclosed, please find a copy of the report summarizing the Underground Storage Tank (UST) removals at
the subject Property, referenced above. Retain this report for your records. Also, a copy of this report has
been submitted to the City of Eagan.
Per the request of the Minnesota Pollution Control Agency (MPCA), copies of the Site Sampling Map
and Laboratory Analytical Reports (Attachments C & D) were submitted for comparison with historic
environmental reporting for /on the Property.
Should you have any questions regarding the contents of this report, or if we can be of further service,
please don't hesitate to call us at (651) 779 -1900.
Sincerely,
MIDAMERICA TECHNICAL & ENVIRONMENTAL SERVICES, INC.
Alyssa Boock, P.G.
Project Manager
Enclosure
Cc: �x
Bringing technical expertise to your environmental needs.
6989 N. 55th Street Ste. C2 • Oakdale, Minnesota 55128 • Office: 651- 779 -1900 • Fax: 651- 779 -9786
TECHNICAL & ENVIRONMENTAL
SERVICES, INC.
MIDAMERICA
UNDERGROUND STORAGE TANK REMOVAL
FORMER SIXTY ONE STOP
3575 PILOT KNOB ROAD
EAGAN, MN 55122
REPORTED TO
MR. BRIAN CARNES
PREMIER BANKS
2866 WHITE BEAR AVENUE
MAPLEWOOD, MN 55109
UST REMOVAL, REPORTING & ENVIRONMENTAL WORK CONDUCTED BY:
MIDAMERICA TECHNICAL &
ENVIRONMENTAL SERVICES, INC.
6989 NORTH 55TH STREET — SUTTE C2
OAKDALE, NHNNESOTA 55128
Project #10P- 1433 -A
December 13, 2010
Bringing technical expertise to your environmental needs.
6989 N. 55th Street Ste. C2 • Oakdale, Minnesota 55128 • Office: 651 - 779 - 1900 • Fax: 651
Certification of Underground Storage Tank Removal
Former Sixty One Stop
3575 Pilot Knob Road
Eagan, MN 55122
MidAmerica Project #10P- 1433 -A
INTRODUCTION
MidAmerica Technical & Environmental Services, Inc., (MidAmerica) was contracted by Mr.
Brian Carnes of Premier Banks to perform the removal of one (1) 10,000 -gallon Premium Gasoline
Fuel Underground Storage Tank (UST), one (1) 12,000 -gallon Gasoline Fuel UST, one (1) 12,000 -
gallon Diesel Fuel UST and six (6) Dispenser Islands located at 3575 Pilot Knob Road, in Eagan,
MN 55122 (Property). The Property is the location of closed MPCA Leak Site #15548. Premier
Banks obtained ownership of the Property through foreclosure and is not a responsible party
according to Minnesota Statute 115C.021, subd. 4 (2008). Premier Banks joined the Petroleum
Brownfields Program in September 2009 and was granted a Petroleum Storage Tank Release
Liability Letter for the Property on October 8, 2009.
Companies Involved in the Removal of the UST
MidAmerica Technical & Environmental Services Inc., 6989 North 55 Street, Suite C2, Oakdale,
Minnesota 55128 performed the product pumping, tank cleaning, field screening, laboratory
sampling, and field management/site supervision. MPCA Contractor #688, MPCA Site Supervisor
#8391
Landwehr Construction, P.O. Box 1086 St. Cloud, MN 56302 performed the excavation and
removal of the USTs.
Pace Analytical Services, Inc. 1700 Elm Street S.E., Minneapolis, MN 55414 provided Laboratory
Analytical Services for Fixed Soil Sample Analysis. MDH Laboratory Certification #027 - 053 -137.
Minnesota Petroleum, 682 39 Avenue, Columbia Heights, MN 55421, processed the petroleum-
impacted water and sludge that were removed from the tanks. EPA ID# MND004595694
RESULTS OF THE UST REMOVAL & EXCAVATION OBSERVATIONS
Methodology
The USTs were initially pumped of gasoline and diesel for processing. The gasoline and diesel
were pumped prior to the removal of the UST, to minimize the potential for environmental impacts,
in the event that the UST would leak or rupture during excavation. Following tank pump -out
procedures, the USTs were removed. Upon verifying that environmental conditions within the
tanks were below the lower explosive limit, an access hole was cut into an end of the tank for
purposes of cleaning. The tanks were slip -3 with a fiberglass coating (clad USTs). No pinholes or
evidence of excessive pitting were observed in the tanks.
No petroleum odors or stains were observed directly around or below the USTs or UST basin. A
slight petroleum odor was noticed under dispensers D -5 and D -11. All soil samples were field
screened with a MiniRae Photo Ionization Detector (PID) containing a 10.6 e.V. lamp. Soil
samples were collected from the clean backfill material at a depth of 14' from the end of each tank
and results from field screening yielded up to 14.7 parts per million (ppm) of organic vapors. Soil
samples from under the dispensers were collected at a depth of 5' and results from field screening
yielded up to 15.9 ppm of organic vapors. A total twelve (12) soil samples from under the UST
basin and pump islands were submitted for laboratory analysis to confirm field observations. A site
map with sampling locations is included as Attachment C.
The soil samples were sent to a fixed laboratory (Pace Analytical Services, Inc.) to be analyzed for
Diesel Range Organics (DRO) or Gasoline Range Organics (GRO), and Benzene, Toluene, Ethyl
Benzene and Xylenes (BTEX). Laboratory analysis yielded concentrations of the aforementioned
parameters below the applicable method detection limit, i.e. non - detect, with the exception of D -11.
Soils from D - 11 yielded detections of DRO up to 3,200 milligrams per kilogram (mg/kg).
The release was called in to the Minnesota State Duty Officer and reported as likely residual
petroleum impacts from previous leak site # 15548 (MPCA report number 116027). MidAmerica
discussed tank removal activities and sampling with MPCA representative Kate Lewison, including
field screening results and observations. Ms. Lewison requested a site map showing sample locations
and a copy of the final lab reports for the MPCA to compare with historic documents. The requested
documents were sent and are awaiting a final determination.
Findings
The tank removals were performed on November 23, 2010.
• At the time of tank removals, approximately 1,075 gallons of gasoline/gasoline- impacted water
and 395 gallons of diesel were removed for processing;
• Soils field screened at two (2) feet below the tank excavation and five (5) feet below the
dispenser islands were up to 15.9 ppm;
• No pitting or pinholes were observed in the tank structure;
• No petroleum odors or stains were observed directly in or below the tank basin or dispenser
islands. However, a slight petroleum odor was noticed under dispensers D -5 and D -11; and
• Laboratory analysis of all twelve (12) soil samples submitted yielded results of Non Detect (ND
mg/kg) for DRO and/or GRO/BTEX, except D -11, which yielded detections of DRO at 3,200
mg/kg;
DISCUSSION AND CONCLUSIONS
MidAmerica performed the removal of the USTs in accordance with the City of Eagan, the MPCA
and State Fire Marshal guidelines. A copy of the City of Eagan Inspections Permit is included as
Attachment A. A copy of the MPCA's Change of Status Form is included as Attachment B.
Copies of the manifests are included in Attachment E.
Final inspection of the USTs, after removal and cleaning, yielded no visual signs of pitting or
pinholes in the USTs. Visual and olfactory observations of the soils directly around the USTs, in
addition to field screening, did not indicate the existence of petroleum impacts. Laboratory
analysis of DRO and/or GRO/BTEX for the UST system samples submitted yielded Non-
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Detections, confirming field observations. Laboratory analysis of DRO and/or GRO/BTEX for
the dispensers yielded a detection of DRO at 3,200 mg/kg under dispenser D -11. A copy of the
analytical report is included as Attachment D.
The Property is the location of closed MPCA Leak Site #15548. Premier Banks obtained
ownership of the Property through foreclosure and is not a responsible party according to
Minnesota Statute 115C.021, subd. 4 (2008). Premier Banks joined the Petroleum Brownfields
Program in September 2009 and was granted a Petroleum Storage Tank Release Liability Letter for
the Property on October 8, 2009.
On behalf of Premier Banks, MidAmerica requested an additional General Liability Letter be issued
to the Buyer of the Property as an assurance that the Buyer will not be named a Responsible Party.
Minnesota Statute 115C.021, subd. 1 (2010) states that if a person comes into possession of a
property after the tanks have been removed, that person is not a responsible party and cannot be
ordered to take corrective action. As the tanks have been removed from the Property prior to the
transfer of ownership to the Buyer, the Buyer is not Responsible Party and will not be required to
perform corrective action on the Property. However, the Buyer is required to cooperate with
corrective actions issued to the Responsible Party, as stated in Minnesota Statue 115C.03, subd 1.
MidAmerica believes that neither Premier Banks, nor the Buyer, will be targeted as the Responsible
Party for releases from tanks on the Property.
MidAmerica understands that development is planned for the Property. The Buyer should be aware
that Minnesota Law requires contaminated soils and water uncovered or disturbed to be properly
managed. Contaminated soils are likely to be encountered on this Property related to one or more
historic releases. MidAmerica recommends the Buyer hire a qualified environmental consultant to
assist them with a Development Response Action Plan (DRAP) for the management of
contaminated soils or groundwater, should they be encountered during development. The MPCA's
Petroleum Brownfields Program can assist with the review and approval of the DRAP.
Based on field observations, field screening and fixed laboratory results, MidAmerica does not
recommend any further investigation with respect to the former fuel dispensing system.
MidAmerica recommends awaiting the final MPCA determination of the property prior to any
subsurface investigation or development of the Property.
STANDARD OF CARE
Our recommendations contained in this report represent our professional opinions, which were
arrived at in accordance with currently accepted local hydrogeological and engineering practices as
they pertain to the site conditions at the time of the UST removals. No other warranty is implied or
intended.
MIDAMERICA TECHNICAL & ENVIRONMENTAL SERVICES, INC
Alyssa Boock, P.G.
Project Manager
1
City of Eagan
I 3830 Pilot Knob Rd
Eagan, MN 55122
(651) 675 -5675
www.ci.eagan.mn.us
I Site Address: 3575 Pilot Knob Rd
Lot: 1 Block: 1 Addition: George W Giles
PID: 10- 28990 - 010 -01
1 Use: Sixty One Stop
Sub Type: Underground Tank
Work Type: Remove
I Description: Removal of 3 underground storage tanks
INSPECTION RECORD
Permit Type: Mechanical
Permit Number: EA097010
Date Issued: 11/15/2010
Mid America Technical & Environmental
(651) 779 -1900
0 * Contractor is responsible for erosion control.
* House #s required for final inspection.
* 4 -hour notice for permanent water turn -on for new building: 651- 675 -5200.
1. Tank number
See Guidance - page 4
001
002
003
2. Install new tank
3. Install new piping
4. Install new tank and piping
5. Install new dispenser(s)
6. Change site information
7. Change owner information
8. Change tank information
9. Change piping, pump, or
dispenser information
10. Current tank status
See Guidance — page 4
Status: Removed
Date: 11/23/2010
Status: Removed
Date: 11/23/2010
Status: Removed
Date: 11/23/2010
Status:
Date:
11. If tank has been removed,
list tank sludge disposal
company and Hazardous
Waste Generator ID#
MN Petroeleum
MND0045956943
MN Petroeleum
MND0045956943
MN Petroeleum
MND0045956943
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Minnesota Pollution
Control Agency
520 Lafayette Road North
St. Paul, MN 551554194
Notify the Minnesota Pollution Control Agency (MPCA) within 30 days after bringing tank system into use or making a change in
status or information. Keep a copy for your records. Unsigned and incomplete forms will be returned. Guidance on page 4.
Questions: Call 651 - 757 -2429 or 1- 800 - 657 -3864 during normal business hours.
Use this form for:
• Installation or replacement of tank, piping, or dispensers
• Change in information, such as site name, address, owner,
or tank contents
• Change in tank status
Ways to notify:
• Fax: 651 -297 -2343 or 651 - 297 -8683, Attn: Joann Henry
• Mail: Attn: Joann Henry at above address
Site Information
Site name: Sixty One Stop
Address: 3575 Pilot Knob Road
City: Eagan
Contact name:
Is this site located on Native American lands? ❑ Yes ® No Is this the initial notification for this site? ❑ Yes ® No
Type of facility: ® Service station ❑ Govemment ❑ Education ❑ Industry/Factory ❑ Auto dealer ❑ Utility
❑ Bulk plant ❑ Resort ❑ Office building ❑ Other (specify):
Owner Information
Name: Premier Banks
Address: 2866 White Bear Ave.
City: Maplewood
Brian Carnes
Contact name: Brian Carnes
State: MN
Notification of Installation or Change in Status
Installation, New Information, Closure
Tanks, Piping, Dispensers
State: MN
A. Action (Enter date [MM/DD/YYYY] of action under tank number)
Underground Storage Tanks
MPCA Use Only
Site #:
County:
Date rec'd:
Site # (if known): 14974
55122 -
Zip code: 1314 County: Dakota
Phone: 651- 855 -1111
Phone: 651 - 855 -1111
Zip code: 55109
www.pca.state_mn.us • 651-296-6300 • 800 - 657 -3864 • TTY 651- 282 -5332 or 800 - 657 -3864 • Available in alternative formats
t -u5 -04 • 12/3/08
Page 1 of 5
1. Tank number
See Guidance — page 4
001
002
003
003
2. Capacity
Gallons: 10,000
Gallons: 12,000
Gallons: 12,000
Gallons:
3. Stored substance
See Guidance — page 4
Type: Gasoline, E10
Specify:: Premium
Type: Gasoline, E10
Specify Regular
Type: Diesel, Petroleum
Specify.
Type:
Specify:
4. Compartmental tank only
See Guidance — page 4
Compartment 1
Gallons:
Type:
Specify
Gallons:
Type:
Specify.:
Gallons:
Type:
Specify.
Gallons:
Type:
Specify:
Compartment 2
Gallons:
Type:
Specify.
Gallons:
Type:
Specify:
Gallons:
Type:
Specify:
Gallons:
Type:
Specify:
Compartment 3
Gallons:
Type:
Specify:
Gallons:
Type:
Specify.
Gallons:
Type:
Specify
Gallons:
Type:
Specify:
5. Special use (check either or
both if applicable)
❑ Heating
❑ Heating
❑ Generator fuel
❑ Heating
❑ Heating
❑ Generator fuel
■ Generator fuel
• Generator fuel
6. Tank type
See Guidance — page 4
Type: Other (specify)
Specify. STIP3 Coated
With Fiberglass on
Exterior
Type: Other (specify)
Specify: STIP3 Coated
With Fiberglass on
Exterior
Type: Other (specify)
Specify STIP3 Coated
With Fiberglass on
Exterior
Type:
Specify:
7. Tank corrosion protection
See Guidance — page 4
Sacrificial Anode
Sacrificial Anode
Sacrificial Anode
8. Fill pipe spill containment
(spill bucket)
0 Yes ❑ No
® Yes • No
0 Yes ❑ No
• Yes ❑ No
9. Overfill prevention type
See Guidance — page 4
Vent pipe ball float
Vent pipe ball float
Vent pipe ball float
10. Stage 1 vapor recovery for
gasoline tanks
• Yes ® No
• Yes 0 No
• Yes 0 No
❑ Yes • No
11. Primary method of tank
release detection
See Guidance — page 4
Auto tank gauging(ATG)
Auto tank gauging(ATG)
Auto tank gauging(ATG)
C. Piping, Pump, and Dispenser Information:
1. Tank number
See Guidance — page 4
001
002
003
2. Piping type
See Guidance — page 4
Type: Fiberglass,SW
Specify.
Type: Fiberglass,SW
Specify:
Type: Fiberglass,SW
Specify:
Type:
Specify::
3. Piping corrosion protection
See Guidance — page 4
Not needed
Not needed
Not needed
4. Primary method of piping
release detection
See Guidance — page 4
Auto line -leak detector
Auto line -leak detector
Auto line -leak detector
5 . Dispensing type
See Guidance — page 4
Submersible pump
Submersible pump
Submersible pump
6. Submersible pump
containment
See Guidance — page 4
Type: Synthetic
Specify:
Type: Synthetic
Specify:
Type: Synthetic
Specify:
Type:
Specify:
7. How many dispensers
serve this tank?
6
6
4
8. Dispenser containment
See Guidance — page 4
Type: Synthetic
Specify:
Type: Synthetic
Specify:
Type: Synthetic
Specify:
Type:
Specify:
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B. Tank Information
Comments:
www.pca.state.mn.us • 651 - 296 -6300 • 800-657-3864 • TTY 651- 282 -5332 or 800- 657 -3864 • Available in altemative formats
Page 2 of 5
t -u5 -04 • 12/3/08
Certification:
Tank Owner
/ certify that the information submitted is accurate and complete to the best of my knowledge; that installation of tanks, piping, and
dispensers is according to Minn. R. ch. 7150.0100 and 7150.0205, including secondary containment of new and replacement tanks,
piping, and dispensers; and that all tanks and piping have release detection according to Minn. R. ch. 7150. 0300 to 7150.0340.
(For owners purchasing tanks after March 1, 2008, only) 1 certify that all tank operators, including lessees, have read this chapter
and have sufficient knowledge in the operation and maintenance of underground storage tank systems.
Name of owner or
owner's authorized representati (print): � Its r( �(Y� � 2� " ;t✓�
Title: V i (, k i c.11 6L` Date: /f-96-0
9
Signature:
Tank Contractor
1 certify that all work was performed as specified by the manufacturer's instructions; that all work was performed according to the
applicable codes of practice in Minn. R. ch. 7150.0205; that all work was performed according to applicable state and federal
regulations, including this chapter, and that 1 am in compliance with contractor certification requirements imposed by Minn. R. ch.
7105.
Licensed tank supervisor
on site during tank work (print): Jim Harms
Title: Project Manager
Signature:
Licensed Tank contractor or
authorized representative (print): MidAmerica - Jim Harms
Title: President
Signature:
Date: 10 -Z4.-10
MPCA Supervisor #: 8391
Date: 10- ?s.•10
MPCA Contractor #: 688
www.pca.state.mn.us • 651-296-6300 • 800 - 657 -3864 TTY 651- 282 -5332 or 800 - 657 -3864 • Available in altemative formats
t -u5 -04 • 1213/08 Page 3 of 5
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December 03, 2010
Ms. Alyssa Boock
Midamerica Technical
6989 N. 55th Street
Suite C2
Oakdale, MN 55128
RE: Project: 1OP-1433-A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Dear Ms. Boock:
Enclosed are the analytical results for sample(s) received by the laboratory on November 27, 2010.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Paul Kirchberg
paul.kirchberg@pacelabs.com
Project Manager
Enclosures
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
REPORT OF LABORATORY ANALYSIS Page 1 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ke
1 of 26
aceAnaiytical
www.paceiabacom
Project: 1 OP- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Minnesota Certification IDs
1700 Elm Street SE Suite 200, Minneapolis, MN
Alaska Certification #: UST -078
Alaska Certification #MN00064
Arizona Certification #: AZ -0014
Arkansas Certification #: 88 -0680
Califomia Certification #: 01155CA
EPA Region 8 Certification #: Pace
Florida/NELAP Certification #: E87605
Georgia Certification #: 959
Idaho Certification #: MN00064
Illinois Certification #: 200011
Iowa Certification #: 368
Kansas Certification #: E -10167
Louisiana Certification #: 03086
Louisiana Certification #: LA080009
Maine Certification #: 2007029
Maryland Certification #: 322
Michigan DEG Certification #: 9909
Minnesota Certification #: 027- 053 -137
Mississippi Certification #: Pace
CERTIFICATIONS
55414 Montana Certification #: MT CERT0092
Nevada Certification #: MN_00064
Nebraska Certification #: Pace
New Jersey Certification #: MN -002
New Mexico Certification #: Pace
New York Certification #: 11647
North Carolina Certification #: 530
North Dakota Certification #: R -036
North Dakota Certification #: R-036A
Ohio VAP Certification #: CL101
Oklahoma Certification #: D9921
Oklahoma Certification #: 9507
Oregon Certification #: MN200001
Pennsylvania Certification #: 68 -00563
Puerto Rico Certification
Tennessee Certification #: 02818
Texas Certification #: T104704192
Washington Certification #: C754
Wisconsin Certification #: 999407970
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
2 of 26
Page 2 of 23
Project: 10P- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Lab ID Sample ID
10144082001 Trip Blank
10144082002 B -1
10144082003 B -2
10144082004 B -3
10144082005 B-4
10144082006 B -5
10144082007 B -6
10144082008 D -1
10144082009 D -3
10144082010 D -5
10144082011 D -7
10144082012 D -9
10144082013 D -11
SAMPLE SUMMARY
Matrix Date Collected Date Received
Solid 11/23/10 08:00 11/27/10 10:50
Solid 11/23/10 10:00 11/27/10 10:50
Solid 11/23/10 10:15 11/27/1010:50
Solid 11/23/10 13:45 11/27/1010:50
Solid 11/23/10 14:05 11/27/10 10:50
Solid 11/23/10 16:00 11/27/10 10:50
Solid 11/23/10 16:10 11/27/1010:50
Solid 11/24/10 16 :00 11/27/10 10:50
Solid 11/24/10 15:50 11/27/10 10:50
Solid 11/24/1015:40 11/27/1010:50
Solid 11/24/10 15:30 11/27/1010:50
Solid 11/24/10 16:10 11/27/1010:50
Solid 11/24/10 16:05 11/27/10 10:50
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
REPORT OF LABORATORY ANALYSIS Page 3 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
CCO4
0
3 of 26
Project 10P- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Lab ID Sample ID
10144082001 Trip Blank
10144082002 B-1
10144082003 B -2
10144082004 B -3
10144082005 B-4
10144082006 B -5
10144082007 B -6
10144082008 D -1
10144082009 D -3
10144082010 D -5
10144082011 D -7
10144082012 D -9
10144082013 D -11
SAMPLE ANALYTE COUNT
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytes
Method Analysts Reported
WI MOD GRO MJH 6
WI MOD GRO MJH 6
% Moisture JDL 1
WI MOD GRO MJH 6
% Moisture JDL 1
WI MOD GRO MJH 6
% Moisture JDL 1
WI MOD GRO MJH 6
% Moisture JDL 1
WI MOD DRO KL1 2
% Moisture JDL 1
WI MOD DRO KL1 2
% Moisture JDL 1
WI MOD GRO MJH 6
% Moisture JDL 1
WI MOD GRO MJH 6
% Moisture JDL 1
WI MOD DRO KL1 2
WI MOD GRO MJH 6
% Moisture JDL 1
WI MOD DRO KL1 2
WI MOD GRO MJH 6
% Moisture JDL 1
WI MOD DRO KL1 2
WI MOD GRO MJH 6
% Moisture JDL 1
WI MOD DRO KL1 2
WI MOD GRO MJH 5
% Moisture JDL 1
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
4 of 26
Page 4 of 23
Project 10P- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Sample: Trip Blank
Results reported on a "wet- weight" basis
WIGRO GCV
Parameters
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
Date: 12/03/2010 02:58 PM
Lab ID: 10144082001 Collected: 11/23/10 08:00
Results
ANALYTICAL RESULTS
Units Report Limit DF Prepared
Analytical Method: WI MOD GRO Preparation Method: TPH GRO /PVOC WI ext
ND mg/kg 0.050
ND mg /kg 0.050
ND mg /kg 5.0
ND mg/kg 0.050
ND mg/kg 0.15
99 % 80-125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Received: 11/27/10 10:50 Matrix: Solid
11/30/10 14:55 12/02/10 00:55 71 -43 -2
11/30/10 14:55 12/02/10 00:55 100 -41-4
11/30/10 14:55 12/02/10 00:55
11/30/10 14:55 12/02/10 00:55 108 -88-3
11/30/10 14:55 12/02/10 00:55 1330 -20 -7
11/30/10 14:55 12/02/10 00:55 98 -08-8
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
Analyzed CAS No. Qual
5 of 26
Page 5 of 23
aceAnalytical
www.pacelabs.corn
Project 1 OP- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Sample: B -1
Results reported on a 'dry- weight" basis
Parameters Results
WIGRO GCV
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
Dry Weight
Percent Moisture
Date: 12/03/2010 02:58 PM
Lab ID: 10144082002 Collected: 11/23/10 10:00 Received: 11/27/10 10:50
Analytical Method: WI MOD GRO
ND mg /kg
ND mg /kg
ND mg/kg
ND mg /kg
ND mg /kg
100 %
Analytical Method: % Moisture
3.4 %
ANALYTICAL RESULTS
Units Report Limit DF
Preparation Method: TPH GRO /PVOC WI ext.
0.052
0.052
5.2
0.052
0.16
80-125
0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Prepared Analyzed CAS No.
11/30/10 14:55
11/30/10 14:55
11/30/10 14:55
11/30/10 14:55
11/30/10 14:55
11/30/10 14:55
12/02/10 05:38 71 -43 -2
12/02/10 05:38 100 -41-4
12/02/10 05:38
12/02/10 05:38 108 -88-3
12/02/10 05:38 1330 -20 -7
12/02/10 05:38 98 -08 -8
12/02/10 00:00
Pace Analytical Services, Inc.
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Minneapolis, MN 55414
(612)607 -1700
Matrix: Solid
6 of 26
Quaff
Page 6 of 23
17 ,aceAnalytical
www.pace/abscom
Project: 10P- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Sample: B -2 Lab ID: 10144082003
Results reported on a "dry-weight" basis
Parameters Results Units
WIGRO GCV
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
Dry Weight
Percent Moisture
Date: 12/03/2010 02:58 PM
Analytical Method: WI MOD GRO
ND mg/kg
ND mg/kg
ND mg/kg
ND mg /kg
ND mg/kg
101 %
Analytical Method: % Moisture
ANALYTICAL RESULTS
Collected: 11/23/10 10:15
Report Limit DF Prepared
4.7 % 0.10 1
Preparation Method: TPH GRO /PVOC WI ext.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
eireti
0.052 1 11/30/10 14:55
0.052 1 11/30/10 14:55
5.2 1 11/30/1014:55
0.052 1 11/30/10 14:55
0.16 1 11/30/1014:55
80-125 1 11/30/10 14:55
Received: 11/27/10 10:50 Matrix: Solid
Analyzed CAS No. Quaff
12/02/10 06:02 71 -43 -2
12/02/10 06:02 100 -41-4
12/02/10 06:02
12/02/10 06:02 108 -88-3
12/02/10 06:02 1330 -20 -7
12/02/10 06:02 98 -08 -8
12/02/10 00:00
Pace Analytical Services, Inc.
1700 Elm Street- Suite 200
Minneapolis, MN 55414
(612)607 -1700
7 of 26
Page 7 of 23
Project 1 OP- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Date: 12/03/2010 02:58 PM
ANALYTICAL RESULTS
Sample: B -3 Lab ID: 10144082004 Collected: 11/23/10 13:45 Received: 11/27/10 10:50 Matrix: Solid
Results reported on a 'dry- weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method: WI MOD GRO Preparation Method: TPH GRO /PVOC WI ext.
Benzene ND mg /kg 0.052 1 11/30/10 14:55 12/02/10 06:25 71 -43 -2
Ethylbenzene ND mg /kg 0.052 1 11/30/10 14:55 12/02/10 06:25 100 -41-4
Gasoline Range Organics ND mg /kg 5.2 1 11/30/10 14:55 12/02/10 06:25
Toluene ND mg /kg 0.052 1 11/30/10 14:55 12/02/10 06:25 108 -88-3
Xylene (Total) ND mg /kg 0.16 1 11/30/10 14:55 12/02/10 06:25 1330 -20 -7
a,a,a- Trifluorotoluene (S) 99 % 80-125 1 11/30/10 14:55 12/02/10 06:25 98 -08 -8
Dry Weight Analytical Method: % Moisture
Percent Moisture 4.5 % 0.10 1 12/02/10 00:00
REPORT OF LABORATORY ANALYSIS Page 8 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
8 of 26
aceAnai tical
wrrw.pacelabscom
Project: 10P- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Sample: B-4 Lab ID: 10144082005
Results reported on a 'dry- weight" basis
Parameters Results Units
WIGRO GCV
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
Dry Weight
Percent Moisture
Date: 12/03/2010 02:58 PM
Analytical Method: WI MOD GRO
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
100 %
Analytical Method: % Moisture
ANALYTICAL RESULTS
Collected: 11/23/10 14:05 Received: 11/27/10 10:50 Matrix: Solid
Report Limit DF Prepared
Preparation Method: TPH GRO /PVOC WI ext.
0.052 1
0.052 1
5.2 1
0.052 1
0.15 1
80-125 1
3.8 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
11/30/10 14:55 12/02/10 06:49 71 -43 -2
11/30/10 14:55 12/02/10 06:49 100 -414
11/30/10 14:55 12/02/10 06:49
11/30/10 14:55 12/02/10 06:49 108 -88-3
11/30/10 14:55 12/02/10 06:49 1330 -20 -7
11/30/10 14:55 12/02/10 06:49 98 -08 -8
12/02/10 00:00
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
Analyzed CAS No. Qual
9 of 26
Page 9 of 23
ace•nalytica!
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Project 1 OP- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
ANALYTICAL RESULTS
Sample: B -5 Lab ID: 10144082006 Collected: 11/23/10 16:00 Received: 11/27/10 10:50 Matrix: Solid
Results reported on a dry. weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIDRO GCS
Diesel Range Organics
n- Triacontane (S)
Dry Weight
Percent Moisture
Date: 12/03/2010 02:58 PM
Analytical Method: WI MOD DRO Preparation Method: WI MOD DRO
ND mg/kg
67 %
Analytical Method: % Moisture
3.7 %
6.5 1 11/29/10 07:28 12/01/10 22:18
50-150 1 11/29/10 07:28 12/01/10 22:18
0.10 1 12/02/10 00:00
Pace Analytical Services, Inc.
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REPORT OF LABORATORY ANALYSIS Page 10 of 23
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10 of 26
Project: 1 OP- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
WIDRO GCS
Diesel Range Organics
n- Triacontane (S)
Dry Weight
Percent Moisture
Date: 12/03/2010 02:58 PM
ND mg/kg
63 %
Analytical Method: % Moisture
3.9 %
ANALYTICAL RESULTS
Sample: B -6 Lab ID: 10144082007 Collected: 11/23/10 16:10 Received: 11/27/10 10:50 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: WI MOD DRO Preparation Method: WI MOD DRO
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
7.1 1 11/29/10 07:28 12/01/10 22:25
50-150 1 11/29/10 07:28 12/01/10 22:25
0.10 1 12/02/10 00:00
REPORT OF LABORATORY ANALYSIS Page 11 of 23
11 of 26
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
Project: 10P- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Sample: D -1
Results reported on a "dry- weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIGRO GCV Analytical Method: WI MOD GRO Preparation Method: TPH GRO /PVOC WI ext.
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
Dry Weight
Date: 12/03/2010 02:58 PM
Lab ID: 10144082008 Collected: 11/24/10 16:00 Received: 11/27/10 10:50 Matrix: Solid
ND mg /kg
ND mg /kg
ND mg /kg
ND mg /kg
ND mg /kg
102 %
Percent Moisture 9.5 %
Analytical Method: % Moisture
ANALYTICAL RESULTS
0.057 1 11/29/10 10:07 11/30/10 08:53 71 -43 -2
0.057 1 11/29/10 10:07 11/30/10 08:53 100 -41-4
5.7 1 11/29/10 10:07 11/30/10 08:53
0.057 1 11/29/10 10:07 11/30/10 08:53 108 -88-3
0.17 1 11/29/10 10:07 11/30/10 08:53 1330 -20 -7
80-125 1 11/29/10 10:07 11/30/10 08:53 98 -08 -8
0.10 1 12/02/10 00:00
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
REPORT OF LABORATORY ANALYSIS Page 12 of 23
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without the written consent of Pace Analytical Services, Inc..
12 of 26
a eAnal.4icaI
www.pacetabs.com
Project 1 OP- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
WIGRO GCV
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
Dry Weight
Percent Moisture
Date: 12/03/2010 02:58 PM
Analytical Method: WI MOD GRO
Analytical Method: % Moisture
ANALYTICAL RESULTS
Sample: D -3 Lab ID: 10144082009- Collected: 11/24/10 15:50
Results reported on a dry- weight" basis
Parameters Results
Units Report Limit DF Prepared
ND mg/kg 0.056
ND mg/kg 0.056
ND mg/kg 5.6
ND mg/kg 0.056
ND mg/kg 0.17
99 % 80-125
Preparation Method: TPH GRO /PVOC WI ext
s„ ti C C k1
10.3 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Received: 11/27/10 10:50 Matrix: Solid
11/29/10 10:07
11/29/10 10:07
11/29/10 10:07
11/29/10 10:07
11/29/10 10:07
11/29/10 10:07
Analyzed CAS No. Qual
11/30/10 09:17 71 -43 -2
11/30/10 09:17 100 -41-4
11/30/10 09:17
11/30/10 09:17 108 -88-3
11/30/10 09:17 1330 -20-7
11/30/10 09:17 98 -08 -8
12/02/10 00:00
13 of 26
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
Page 13 of 23
aceAna/ytical
snrwpacelablwm
Project: 1 OP- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Sample: D -5 Lab ID: 10144082010
Results reported on a dry- weight" basis
Parameters Results Units
WIDRO GCS
Diesel Range Organics
n- Triaoontane (S)
WIGRO GCV
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
Dry Weight
Percent Moisture
Date: 12/03/2010 02:58 PM
Analytical Method: WI MOD DRO
ND mg /kg
72 %
Analytical Method: WI MOD GRO
ND mg /kg
ND mg /kg
ND mg /kg
ND mg /kg
ND mg /kg
98 %
Analytical Method: % Moisture
4.3 %
ANALYTICAL RESULTS
Collected: 11/24/10 15:40 Received: 11/27/10 10:50 Matrix: Solid
Report Limit DF Prepared Analyzed
Preparation Method: WI MOD DRO
6.2 1 11/29/10 07:28 12/02/1013:16
50-150 1 11/29/10 07:28 12/02/1013:16
Preparation Method: TPH GRO /PVOC WI ext.
0.051 1 11/29/10 10:07
0.051 1 11/29/10 10:07
5.1 1 11/29/10 10:07
0.051 1 11/29/1010:07
0.15 1 11/29/1010:07
80-125 1 11/29/10 10:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
11-°
11/30/10 09:41
11/30/10 09:41
11/30/10 09:41
11/30/10 09:41
11/30/10 09:41
11/30/10 09:41
0.10 1 12/02/10 00:00
Pace Analytical Services, Inc.
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14 of 26
CAS No. Qual
71 -43 -2
100 -41-4
108 -88-3
1330 -20-7
98 -08 -8
Page 14 of 23
Project: 10P- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Sample: D -7 Lab ID: 10144082011
Results reported on a dry- weight" basis
Parameters Results Units
WIDRO GCS
Diesel Range Organics
n- Triacontane (S)
WIGRO GCV
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
Dry Weight
Percent Moisture
Date: 12/03/2010 02:58 PM
Analytical Method: WI MOD DRO
ND mg/kg
70 %
Analytical Method: WI MOD GRO
ND mg /kg
ND mg /kg
ND mg /kg
ND mg/kg
ND mg/kg
97 %
ANALYTICAL RESULTS
Collected: 11/24/10 15 :30 Received: 11/27/10 10:50 Matrix: Solid
Report Limit DF Prepared Analyzed CAS No. Qual
Preparation Method: WI MOD DRO
7.0 1 11/29/10 07:28 12/01/10 22:39
50-150 1 11/29/10 07:28 12/01/10 22:39
Preparation Method: TPH GRO /PVOC WI ext.
0.052 1 11/29/10 10:07 11/30/10 10:04 71 -43-2
0.052 1 11/29/10 10:07 11/30/10 10:04 100 -41-4
5.2 1 11/29/10 10:07 11/30/10 10:04
0.052 1 11/29/10 10:07 11/30/10 10:04 108 -88-3
0.15 1 11/29/10 10:07 11/30/10 10:04 1330 -20 -7
80-125 1 11/29/10 10:07 11/30/10 10:04 98 -08 -8
Analytical Method: % Moisture
5.9 % 0.10 1 12/02/10 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
40, CCCggq
`z
15 of 26
Pace Analytical Services, Inc.
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Minneapolis, MN 55414
(612)607 -1700
Page 15 of 23
a eAnaIYticaI
xww.pacelabscom
Project 10P- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
Dry Weight
ND mg/kg
ND mg /kg
ND mg/kg
ND mg/kg
ND mg/kg
102 %
Percent Moisture 5.5 %
Date: 12/03/2010 02:58 PM
Analytical Method: % Moisture
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
Sample: D -9 Lab ID: 10144082012 Collected: 11/24/10 16:10 Received: 11/27/10 10:50 Matrix: Solid
Results reported on adry- weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
WIDRO GCS Analytical Method: WI MOD DRO Preparation Method: WI MOD DRO
Diesel Range Organics ND mg /kg 6.9 1 11/29/10 07:28 12/01/10 22:53
n- Triacontane (S) 72 % 50-150 1 11/29/10 07:28 12/01/10 22:53
WIGRO GCV Analytical Method: WI MOD GRO Preparation Method: TPH GRO /PVOC WI ext.
0.054 1 11/30/10 14:55 12/02/10 07:12 71 -43 -2
0.054 1 11/30/10 14:55 12/02/10 07:12 100 -41-4
5.4 1 11/30/10 14:55 12/02/10 07:12
0.054 1 11/30/10 14:55 12/02/10 07:12 108 -88-3
0.16 1 11/30/10 14:55 12/02/10 07:12 1330 -20 -7
80-125 1 11/30/10 14:55 12/02/10 07:12 98 -08-8
0.10 1 12/02/10 00:00
REPORT OF LABORATORY ANALYSIS Page 16 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
16 of 26
aceAnalytical
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Project: 10P- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
Sample: D -11 Lab ID: 10144082013
Results reported on a "dry-weight" basis
Parameters Results Units
WIDRO GCS
Diesel Range Organics
n- Triacontane (S)
WIGRO GCV
Benzene
Ethylbenzene
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
Dry Weight
Percent Moisture
Date: 12/03/2010 02:58 PM
Analytical Method: WI MOD DRO
3200 mg/kg
0 %
Analytical Method: WI MOD GRO
ND mg/kg
ND mg/kg
ND mg/kg
ND mg/kg
98 %
Analytical Method: % Moisture
ANALYTICAL RESULTS
Collected: 11/24/10 16:05 Received: 11/27/10 10:50 Matrix: Solid
Report Limit DF Prepared Analyzed CAS No. Qual
Preparation Method: WI MOD DRO
763 100 11/29/10 07:28 12/02/10 13:51
50-150 100 11/29/10 07:28 12/02/10 13:51
Preparation Method: TPH GRO /PVOC WI ext.
0.057
0.057
0.057
0.17
80-125
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
11/30/10 14:55
11/30/10 14:55
11/30/10 14:55
11/30/10 14:55
11/30/10 14:55
12/02/10
12/02/10
12/02/10
12/02/10
12/02/10
14.0 % 0.10 1 12/02/10 00:00
17 of 26
Pace Analytical Services, Inc.
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Minneapolis, MN 55414
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07:36 71 -43 -2
07:36 100 -41-4
07:36 108 -88-3
07:36 1330 -20-7
07:36 98 -08-8
S4
Page 17 of 23
• Pace Analytical Services, Inc.
a i
aL'�1 &t a I 1700 Elm Street -Suite 200
`7` Minneapolis, MN 55414
(612)607 -1700
QUALITY CONTROL DATA '
Project 1 OP- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082 111 QC Batch: OEXT/14338 Analysis Method: WI MOD DRO
QC Batch Method: WI MOD DRO Analysis Description: WIDRO GCS
Associated Lab Samples: 10144082006, 10144082007, 10144082010, 10144082011, 10144082012, 10144082013
METHOD BLANK: 898334 Matrix: Solid
Associated Lab Samples: 10144082006, 10144082007, 10144082010, 10144082011, 10144082012, 10144082013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Diesel Range Organics mglkg ND 5.0 12/01/10 21:15
n- Triacontane (S) % 73 50-150 12/01/10 21:15
LABORATORY CONTROL SAMPLE & LCSD: 898335 898336
Spike LCS LCSD LCS LCSD % Rec Max
I
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Diesel Range Organics mg/kg 80 64.2 67.6 80 84 70 -120 5 20
n- Triacontane (S) % 79 81 50-150
1
1 : ek
1
1
1
1
1
1
1
1
Date: 12/03/2010 02:58 PM REPORT OF LABORATORY ANALYSIS Page 18 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
18of26
1
I %2
aceilical
1 stow peeelabs coin
Project 1 OP- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
METHOD BLANK: 898337
Associated Lab Samples:
Parameter
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
LABORATORY CONTROL SAMPLE & LCSD: 898338
Parameter
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
MATRIX SPIKE SAMPLE:
Parameter
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
SAMPLE DUPLICATE: 898341
Parameter
Benzene
Ethylbenzene
Gasoline Range Organics
Toluene
Xylene (Total)
a,a,a- Trifluorotoluene (S)
Date: 12/03/2010 02:58 PM
mg/I9
m9 /k9
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
m9/k9
898340
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
Units
QUALITY CONTROL DATA
QC Batch: GCV/7630 Analysis Method:
QC Batch Method: TPH GRO/PVOC WI ext. Analysis Description:
Associated Lab Samples: 10144082008, 10144082009, 10144082010, 10144082011
Matrix: Solid
10144082008, 10144082009, 10144082010, 10144082011
Blank Reporting
Units Result Limit Analyzed Qualifiers
ND
ND
ND
ND
ND
101
898339
Spike LCS LCSD LCS LCSD % Rec
Units Conc. Result Result % Rec % Rec Limits
5 5.6 5.0 111 100 80 -120 11 20
5 5.5 5.0 111 99 80-120 11 20
50 57.2 53.8 114 108 80 -120 6 20
5 5.5 5.0 110 99 80 -120 10 20
15 16.5 14.6 110 98 80-120 12 20
100 100 80 -125
10143803001
Result
ND
ND
ND
ND
ND
10143803002 Dup
Result Result
ND .01J
ND ND
ND 1.7J
ND ND
ND ND
104 98
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
0.050 11/30/10 01:49
0.050 11/30/10 01:49
5.0 11/30/10 01:49
0.050 11/30/10 01:49
0.15 11/30/10 01:49
80-125 11/30/10 01:49
REPORT OF LABORATORY ANALYSIS
11i =! .�'
Spike MS MS % Rec
Conc. Result % Rec Limits Qualifiers
WI MOD GRO
WIGRO Solid GCV
5.3 6.1 114 80-120
5.3 6.0 113 80-120
52.9 64.8 119 80-120
5.3 6.0 113 80 -120
15.9 17.4 109 80 -120
101 80 -125
RPD
7
Max
RPD
20
20
20
20
20
19 of 26
Pace Analytical Services, Inc.
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Max
RPD RPD Qualifiers
Qualifiers
Page 19 of 23
® Pace Analytical Services, Inc. '
9lyticaleAna 1700 Elm Street -Suite 200
a Minneapolis, MN 55414
(612)607 -1700
QUALITY CONTROL DATA 1
Project: 10P- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
QC Batch: GCV/7642 Analysis Method: WI MOD GRO
QC Batch Method: TPH GRO /PVOC WI ext. Analysis Description: WIGRO Solid GCV
Associated Lab Samples: 10144082001, 10144082002, 10144082003, 10144082004, 10144082005, 10144082012, 10144082013
METHOD BLANK: 899052 Matrix: Solid
Associated Lab Samples: 10144082001, 10144082002, 10144082003, 10144082004, 10144082005, 10144082012, 10144082013
Blank Reporting
I
Parameter Units Result Limit Analyzed Qualifiers
Benzene mg/kg ND 0.050 12/01/10 23:45
Ethylbenzene mg/kg ND 0.050 12/01/10 23:45
I
Gasoline Range Organics mg/kg ND 5.0 12/01/10 23:45
Toluene mg/kg ND 0.050 12/01/10 23:45
Xylene (Total) mg/kg ND 0.15 12/01/10 23:45
a,a,a- Trifluorotoluene (S) % 95 80-125 12/01/10 23:45
LABORATORY CONTROL SAMPLE & LCSD: 899053 899054
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Benzene mg/kg 5 5.7 5.1 114 101 80 -120 12 20
Ethylbenzene mg/kg 5 5.6 5.0 111 100 80 -120 10 20
Gasoline Range Organics mg/kg 50 59.3 56.4 119 113 80 -120 5 20
Toluene mg/kg 5 5.6 5.0 112 101 80 -120 11 20
Xylene (Total) mg/kg 15 16.3 14.6 109 98 80 -120 11 20
a,a,a- Trifluorotoluene (S) % 103 102 80-125
I
MATRIX SPIKE SAMPLE: 899055
10144060001 Spike MS MS % Rec
I
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Benzene mg/kg ND 6.2 8.1 130 80-120 M1
Ethylbenzene mg/kg ND 6.2 8.1 129 80-120 M1
Gasoline Range Organics mg/kg ND 62.3 83.8 132
80-120 M1
Toluene mg/kg ND 6.2 8.1 129 80-120 M7
Xylene (Total) mg/kg ND 18.7 23.5 125 80-120 ES
a,a,a- Trifluorotoluene (S) % 103 80-125
1
SAMPLE DUPLICATE: 899056
10144060002 Dup Max
I Parameter Units Result Result RPD RPD Qualifiers
Benzene mg/kg ND ND 20
Ethylbenzene mg/kg ND ND 20
Gasoline Range Organics mg/kg ND ND 20
I
Toluene mg/kg ND ND 20
Xylene (Total) mg/kg ND ND 20
a,a,a- Trifluorotoluene (S) % 102 98 5
1
Date: 12/03/2010 02:58 PM REPORT OF LABORATORY ANALYSIS Page 20 of 23
This report shall not be reproduced, except in full,
I
without the written consent of Pace ; Analytical Services, Inc..
`c 1 20 of 26
1
1 e Pace Analytical Services, Inc.
aceAnalytical 1700 Elm Street - Suite 200
•wwpecxla Minneapolis, MN 55414
1 (612)607 -1700
1 QUALITY CONTROL DATA
Project 10P- 1433 -A Eagan Sixty 1 Stop
I Pace Project No.: 10144082
QC Batch: MPRP /23812 Analysis Method: % Moisture
QC Batch Method: % Moisture Analysis Description: Dry Weight/Percent Moisture
I Associated Lab Samples: 10144082002, 10144082003, 10144082004, 10144082005, 10144082006, 10144082007, 10144082008
SAMPLE DUPLICATE: 899965
10144199006 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 11.8 11.3 5 30
I SAMPLE DUPLICATE: 899966
10144048009 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
I Percent Moisture % 7.4 7.3 1 30
1
1
1
1
1
1
1
1
1
Date: 12/03/2010 02:58 PM REPORT OF LABORATORY ANALYSIS Page 21 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
p ,M •p pp
n
21 of 26
acelytical
wwwpaoelab&. m
Project: 1 OP- 1433 -A Eagan Sixty 1 Stop
Pace Project No.: 10144082
QUALITY CONTROL DATA
QC Batch: MPRP/23814 Analysis Method: % Moisture
QC Batch Method: % Moisture Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 10144082009, 10144082010, 10144082011, 10144082012, 10144082013
SAMPLE DUPLICATE: 899977
10143533001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 8.0 7.4 7 30
SAMPLE DUPLICATE: 899978
10143929001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 55.9 55.9 .04 30
Date: 12/03 /2010 02:58 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
22 of 26
Page 22 of 23
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Project 1OP-1433-A Eagan Sixty 1 Stop
Pace Project No.: 10144082
DEFINITIONS
www.pecebDsoom
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit
S - Surrogate
1,2- Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with,EPA guidelines, unrounded are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
U - Indicates the compound was analyzed for, but not detected.
N- Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
ANALYTE QUALIFIERS
ES The reported result is estimated because one or more of the constituent results are qualified as such.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
Date: 12/03/2010 02:58 PM
QUALIFIERS
Pace Analytical Services, Inc.
1700 Elm Street - Suite 200
Minneapolis, MN 55414
(612)607 -1700
REPORT OF LABORATORY ANALYSIS Page 23 of 23
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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A. Client Name: �� s4 yr.c,
Courier:. ❑ Fed Ex 0 UPS 0 usPS�Cltent ❑ Commercial ❑ Pace Other
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Pecking Material: ❑ Bubble Wrap
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Date: / 1//
Note: Wherever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to theme tom, Inc.
F- L213Rev.00, 05Aug2009 1100 Elm Street SE, Suite 200, Minneapolis, MN 55414
26 of 26
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Emergency Response Telephone Number: 1 (888) 314 -2042
CONTAINER
Quantity Size /Type
TOTAL (WtIVOI)
Quantity gal,Ib,ton,c /y
SHIPPING DESCRIPTION /S
Used Oil Lubricating Oil
Petroleum Grease
Open Gear Lube / Debris
Other:
Used Oil Filters Industrial
Automotive (Crushed)
Automotive (Uncrushed)
Petroleum Granular Clay
Contaminated Sorbents Granular Organic
Pads, Rags, Booms, other
Petroleum Contaminated Water
Other:
Used Antifreeze
Other:
'_n
Fuel Oil, 3, NA 1993, PGIII 4/e Je.Q
2-
ZGS Ayf+C
.QS'
54 L
Used Transformer Oil ( <49ppm)
Other: 69asol,N
/ 6'
66oALbrv4
4 iS6 0
qAL
Other:
1
1
GENERATOR
1
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MIDAMERICA
10 TECHNICAL & ENVIRONMENTAL
SERVICES, INC.
Name: CD I S4 °?
Address: 33 - 74 — Prloi- 24
Service Location:
City /State /Zip:
Contact: e,-revL Ca.rt�. Phone: 63 -77 7 -7.7 ° a
Shipping Manifest
Non - Hazardous
Recyclable Materials
Date: 1 I 9
*Generator Certification: This is to certify that the above named materials are properly classified, packaged, marked and labeled, and are in
proper condition for transportation according to the applicable regulations of the Department of Transportation.
*Generator Non- Contamination Certification (Antifreeze Only) - "I certify that, based on my knowledge of the waste antifreeze and the waste
management practices used at this facility, that this batch of waste antifreeze has not been mixed with other wastes and that this certification is
accurate, true and complete. 1 understand that significant penalties exist for improper management of solid and hazardous waste, including
the possibility of monetary penalties and imprisonment."
Name (Print):
i
Transporter "DRIVER"
Name (Print):
A+.Tdaof r k-
Receiving Facility
Name (Print):
fk(yss4 Bo
Signature: Date:
Signature:
Signature:
Date:
ail 1 0
Date:
9 4
Used oil subject to E.P.A. Regulation under 40 CFR Part 279, MN R. Chapter 7045, Et Seq. MidAmerica, Inc. certifies that oil filters will be shipped
for recycling.
Antifreeze Processing Facility Destination: Pioneer Environmental Group, Inc., 7500 Hudson Blvd., Oakdale, MN 55128.
MIDAMERICA
0 TECHNICAL & ENVIRONMENTAL
SERVICES, INC.
Bringing technical expertise to your environmental needs.
1001
1244
6989 N. 55th Street Ste. C2 • Oakdale, Minnesota 55128 • Office: 651 779 - 1900 • Fax: 651 - 779 - 9786
Emergency Response Telephone Number: 1 (888) 314-2042
CONTAINER
Quantity Size/Type
TOTAL (WtNOI)
Quantity gal,lb,ton,c/y
SHIPPING DESCRIPTION /S
Used Oil Lubricating Oil
Petroleum Grease
Open Gear Lube l Debris
Other :
_
Used Oil Filters Industrial
Automotive (Crushed)
Automotive (Uncrushed)
Petroleum Granular Clay
Contaminated Sorbents Granular Organic
Pads, Rags, Booms, other
Petroleum Contaminated Water
Other:
Used Antifreeze
Other:
Fuel Oil, 3, NA 1993, PGIII
Used Transformer Oil ( <49ppm)
Other: &ASbl+ ±A .y
/
LOr -.
/ — o
"A
Ah L
Other: aAta lr-.o Zp y v �
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MIDAMERICA Shipping Manifest
:AL & ENVIRONMENTAL Non - Hazardous
SERVICES, INC. Recyclable Materials
Name: b Flo f
Address: 3 5-7 r P%lof kno 4.
Service Location:
City /State /Zip: , /AA/
Contact: f3v/-4.1 Ct ' &.d Phone: (0S 777 -710,1
Date 1l /Z f 1 D
1001
1247
`Generator Certification: This is to certify that the above named materials are properly classified, packaged, marked and labeled, and are in
proper condition for transportation according to the applicable regulations of the Department of Transportation.
'Generator Non - Contamination Certification (Antifreeze Only) - "I certify that, based on my knowledge of the waste antifreeze and the waste
management practices used at this facility, that this batch of waste antifreeze has not been mixed with other wastes and that this certification is
accurate, true and complete. 1 understand that significant penalties exist for improper management of solid and hazardous waste, including
the possibility of monetary penalties and imprisonment."
Name (Print):
Transporter "DRIVER"
Name (Print):
wr eto""--\ (i �es6j
Receiving Facility 1
Name (Print):
Signature:
Signature:
�y Ss't �pocC�
MIDAMERICA
TECHNICAL & ENVIRONMENTAL
SERVICES, INC.
Signature: Date:
Date:
t. /z3 /z
Date:
Used oil subject to E.P.A. Regulation under 40 CFR Part 279, MN R. Chapter 7045, Et Seq. MidAmerica, Inc. certifies that oil filters will be shipped
for recycling.
Antifreeze Processing Facility Destination: Pioneer Environmental Group, Inc., 7500 Hudson Blvd., Oakdale, MN 55128.
Bringing technical expertise to your environmental needs.
6989 N. 55th Street Ste. C2 • Oakdale, Minnesota 55128 • Office: 651- 779 - 1900 • Fax: 651 779 - 978